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    • 3. 发明申请
    • METHOD FOR PREPARING UREA WATER, METHOD FOR REMOVING TRIURET FROM UREA WATER AND METHOD FOR COLLECTING TRIURET FROM AQUEOUS SOLUTION
    • 用于制备尿素水的方法,从尿素水中除去三氯乙烯的方法和从水溶液中收集三水合物的方法
    • US20160175739A1
    • 2016-06-23
    • US14375254
    • 2013-12-06
    • OPTY CO. , LTD.
    • Eiichi INO
    • B01D15/36B01D53/92
    • B01D15/361B01D53/92B01D2251/2067C07C273/14C07C275/00
    • Provided is a method of efficiently removing triuret from urea water, a method of producing urea water of high purity and a method of collecting triuret from aqueous solution. Thus, a method of producing urea water comprises a step of preparing urea water by dissolving urea water in water, a step of making the urea water cloudy in a temperature range of −5° C. or more and 17° C. or less and a step of passing the urea water in a cloudy state through an ion exchange resin. Moreover, a method of removing triuret from urea water comprises a step of precipitating the triuret by cooling the urea water including urea and triuret as impurity in a temperature range of −5° C. or more and 17° C. or less and a step of passing the urea water in the temperature range through an ion exchange resin and capturing the precipitated triuret within the ion exchange resin.
    • 提供了一种从尿素水中有效去除三脲的方法,一种制备高纯度尿素水的方法以及从水溶液中收集三脲的方法。 因此,生产尿素水的方法包括通过将尿素水溶解在水中来制备尿素水的步骤,使尿素水在-5℃以上17℃以下的温度范围内变得混浊, 使浑浊状态的尿素水通过离子交换树脂的步骤。 此外,从尿素水中除去三脲的方法包括通过在-5℃或更高和17℃或更低的温度范围内冷却包括尿素和三联效应剂的尿素水作为杂质来沉淀三联效应的步骤,并且步骤 使所述温度范围内的尿素水通过离子交换树脂,并将沉淀的三联体捕获在离子交换树脂内。
    • 7. 发明授权
    • Process for preparing granular urea
    • 颗粒状尿素的制备方法
    • US5965071A
    • 1999-10-12
    • US913871
    • 1997-09-05
    • Hidetsugu FujiiHaruyuki Morikawa
    • Hidetsugu FujiiHaruyuki Morikawa
    • B01J2/02B01J2/04B01J2/16C05C9/00C05C9/02C07C273/02C07C273/14C07C275/00B29B9/10
    • B01J2/16B01J2/04C05C9/005C07C273/02C07C273/14
    • The present invention provides a process for preparing granular urea, which solves the problem of removing moisture in a prilling tower method and the problem of concentrating diluted formaldehyde in granulation by a fluidized, spouted bed method when urea is granulated in the presence of formaldehyde. That is, the present invention provides a process for preparing granular urea from liquid drops or sprayed drops of a urea solution, wherein the urea solution is divided into two portions of a urea solution A and a urea solution B, and a urea solution prepared by mixing an aqueous formaldehyde solution with the urea solution A, concentrating the above mixed solution and then mixing it with the urea solution B is used.
    • PCT No.PCT / JP97 / 00108 Sec。 371日期:1997年9月5日 102(e)1997年9月5日PCT 1997年1月21日PCT PCT。 公开号WO97 / 28100 PCT 日期:1997年8月7日本发明提供了一种制备颗粒状尿素的方法,其解决了造粒塔法中除去水分的问题,以及当尿素成粒时,通过流化喷雾床方法将稀释的甲醛浓缩成粒状的问题 存在甲醛。 也就是说,本发明提供了一种从尿液溶液的液滴或喷雾液滴制备颗粒状尿素的方法,其中将尿素溶液分成尿素溶液A和尿素溶液B两部分,尿素溶液由 将甲醛水溶液与尿素溶液A混合,浓缩上述混合溶液,然后与尿素溶液B混合。
    • 8. 发明授权
    • Process for the preparation of urea
    • 制备尿素的方法
    • US5686647A
    • 1997-11-11
    • US529602
    • 1995-09-18
    • Jan Chys
    • Jan Chys
    • C07C273/04C07C273/14C07C273/16C07D487/18
    • C07D487/18C07C273/04C07C273/14C07C273/16
    • Process for the preparation of urea, wherein in a first step ammonia and carbon dioxide react in suitable conditions so as to form a first mixture containing a quantity of urea, wherein in one or more subsequent steps ammonia and carbon dioxide are removed from the first mixture and the obtained urea is concentrated until a urea concentration has been reached suitable to be granulated in a gas stream, whereby apart from urea granules a second mixture containing air, gaseous ammonia and urea dust is formed which subsequently is washed, and wherein before or during the washing an amount of formaldehyde is added to the second mixture of air, ammonia and urea under circumstances wherein the ammonia can react with the formaldehyde in order to form hexamethylenetetramine (HMTA) whereupon the so formed HMTA is separated from the gas stream and is returned into the process before the granulation step.
    • 制备尿素的方法,其中在第一步骤中,氨和二氧化碳在合适的条件下反应,以形成含有一定量尿素的第一混合物,其中在一个或多个后续步骤中,从第一混合物中除去氨和二氧化碳 将得到的尿素浓缩直到达到适合于在气流中造粒的尿素浓度,由此除了尿素颗粒之外,形成含有空气,气态氨和尿素粉末的第二混合物,其随后被洗涤,并且其中在之前或期间 在氨与甲醛反应以形成六亚甲基四胺(HMTA)的情况下,向空气,氨和尿素的第二混合物中加入一定量的甲醛,由此形成的HMTA与气流分离并返回 进入造粒步骤之前的过程。