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1. 发明申请

US20100230341A1 APPARATUS FOR THE SEMI-CONTINUOUS CHROMATOGRAPHIC SEPARATION OF BINARY AND MULTI-COMPONENT MIXTURES 审中-公开
标题翻译：二元和多组分混合物的半连续色谱分离装置
公开(公告)号：US20100230341A1
公开(公告)日：2010-09-16
申请号：US12763547
申请日：2010-04-20
申请人： Abdelaziz Toumi
发明人： Abdelaziz Toumi
IPC分类号： B01D15/08
CPC分类号： G01N30/44 , B01D15/1828 , B01D15/1842 , B01D15/1857 , G01N30/463
摘要： The invention relates to a semi-continuous chromatographic method for the separation of binary and multi-component mixtures and corresponding devices.
摘要翻译：本发明涉及用于分离二元和多组分混合物和相应装置的半连续色谱方法。

2. 发明申请

US20070158270A1 Simultaneous synthesis and purification of a fatty acid monoester biodiesel fuel 有权
标题翻译：同时合成和纯化脂肪酸单酯生物柴油
公开(公告)号：US20070158270A1
公开(公告)日：2007-07-12
申请号：US11449199
申请日：2006-06-08
申请人： Doug Geier , John G. Soper
发明人： Doug Geier , John G. Soper
IPC分类号： B01D15/08
CPC分类号： B01D15/1857 , B01J8/0457 , C10G2300/1011 , C10L1/026 , C11C3/003 , Y02E50/13 , Y02P30/20
摘要： Simultaneous synthesis and purification of a fatty acid monoester biodiesel fuel from a triacylglycerol feedstock is described. In an exemplary method, the triacylglycerol feedstock is continuously contacted with a catalytic chromatographic bed comprising a first (solid phase) basic catalyst through a first port of a simulated moving bed chromatographic apparatus. A monohydric alcohol and optional second (mobile phase) basic catalyst is continuously contacted with the catalytic chromatographic bed through a second port and pumped in a first direction toward the triacylglycerol feedstock to contact the triacylglycerol in a reaction zone of the catalytic chromatographic bed where the fatty acid monoester and glycerol coproduct are formed. The fatty acid monoester is removed from the reaction zone through a product port of the simulated moving bed apparatus. Segments of the catalytic chromatographic bed are incrementally moved in a second direction, opposite the first direction, and the glycerol is removed from a raffinate port located opposite the product port of the apparatus.
摘要翻译：描述了从三酰基甘油原料同时合成和纯化脂肪酸单酯生物柴油燃料。在示例性方法中，三酰基甘油原料通过模拟移动床层析装置的第一端口与包含第一（固相）碱性催化剂的催化色谱床连续接触。一元醇和任选的第二（流动相）碱性催化剂通过第二端口与催化色谱床连续接触并沿着第一方向朝向三酰基甘油原料泵送，以在催化色谱床的反应区域中与三酰基甘油接触，其中脂肪形成酸单酯和甘油副产物。脂肪酸单酯通过模拟移动床装置的产品端口从反应区域中除去。催化色谱层的分段沿与第一方向相反的第二方向递增移动，并且甘油从位于装置的产品端口的抽出物端口移除。

3. 发明申请

US20160145167A1 REACTIVE CHROMATOGRAPHY PROCESS FOR EQUILIBRIUM-LIMITED REACTIONS 有权
标题翻译：平衡有限反应的反应色谱法
公开(公告)号：US20160145167A1
公开(公告)日：2016-05-26
申请号：US14888512
申请日：2014-05-02
申请人： DOW GLOBAL TECHNOLOGIES, LLC
发明人： Timothy C. FRANK , Megan E. DONALDSON
IPC分类号： C07B41/12 , B01D15/18 , C07B41/02 , C07C67/03 , C07C29/128
CPC分类号： C07B41/12 , B01D15/1821 , B01D15/1857 , B01D15/363 , B01D15/3857 , C07B41/02 , C07C29/1285 , C07C67/03 , Y02P20/127 , C07C69/14
摘要： The present disclosure provides for a process for an equilibrium limited reaction using reactive chromatography unit (RCU) in which a first organic donor reactant (FODR) and a second organic acceptor reactant (SOAR) react to form a product mixture of a first acceptor product (FAP) and a second donor co-product (SDCP). The equilibrium-limited reaction does not produce water. The RCU has separation media to separate the product mixture into a raffmate and an extract. The FODR is in a stoichiometric deficit relative to the SOAR for the equilibrium limited reaction, so that the SOAR acts as the eluent for both the raffmate and the extract, and so as not to produce an azeotrope of FODR and the SDCP in the extract.
摘要翻译：本公开提供使用反应性色谱单元（RCU）的平衡限制反应的方法，其中第一有机供体反应物（FODR）和第二有机受体反应物（SOAR）反应以形成第一受体产物（ FAP）和第二供体共同产物（SDCP）。平衡有限的反应不产生水。 RCU具有分离介质，以将产物混合物分离成拉夫特和提取物。 FODR相对于SOAR为平衡有限反应的化学计量缺口，使得SOAR作为萃取物和萃取物的洗脱液，并且不产生FODR的共沸物和萃取物中的SDCP。

4. 发明申请

US20120108841A1 SIMULATED MOVING BED MEMBRANE REACTOR, NEW HYBRID SEPARATION PROCESS AND USES THEREOF 审中-公开
标题翻译：模拟移动床膜反应器，新型混合分离方法及其用途
公开(公告)号：US20120108841A1
公开(公告)日：2012-05-03
申请号：US13263828
申请日：2010-04-07
申请人： Viviana Manuela Tenedório Matos Da Silva , Carla Sofia Marques Pereira , Alírio Egídio Rodrigues
发明人： Viviana Manuela Tenedório Matos Da Silva , Carla Sofia Marques Pereira , Alírio Egídio Rodrigues
IPC分类号： C07C69/68 , C07C43/303 , B01J8/06
CPC分类号： B01D15/1842 , B01D15/1857 , B01D61/362
摘要： The presently disclosed subject matter is a new technology, related to a simulated moving bed membrane reactor. This novel technology includes a reactor with two different separation techniques: i) chromatography (simulated moving bed—SMB); ii) selective permeable membrane (namely, pervaporation and permeation, among others) into a single device, allowing a significant increase in the unity productivity and considerable reduction of solvent consumption and consequently lowers downstream costs associated to the following separation units, for the same product purity and reactants conversion criteria. It has its main applications in the chemical industry, particularly, in the continuous production of oxygenated compounds as esters, acetals, ethers, carbonates, among others.
摘要翻译：目前公开的主题是与模拟移动床膜反应器相关的新技术。这种新技术包括具有两种不同分离技术的反应器：i）色谱法（模拟移动床SMB）; ii）选择性渗透膜（即，渗透蒸发和渗透等）成单个装置，允许显着提高单位生产率并显着降低溶剂消耗，并因此降低与以下分离单元相关的下游成本，同一产品纯度和反应物转化标准。其主要应用于化学工业，特别是连续生产作为酯，缩醛，醚，碳酸酯等的含氧化合物。

5. 发明申请

US20110168632A1 Method and device for separating fractions of a mixture 有权
$Method and device for separating fractions of a mixture$
标题翻译：用于分离混合物馏分的方法和装置
公开(公告)号：US20110168632A1
公开(公告)日：2011-07-14
申请号：US11996840
申请日：2006-07-25
申请人： Eric Valery , Olivier Ludemann-Hombourger
发明人： Eric Valery , Olivier Ludemann-Hombourger
IPC分类号： B01D15/10 , B01D15/18
CPC分类号： B01D15/18 , B01D15/1857 , B01D15/1864 , B01D15/1871 , G01N30/461
摘要： The invention concerns a method for separating fractions of a mixture to be separated, in a device (1) comprising: several chromatography columns (21, 22, 23,) mounted in series; an open separation loop comprising in input a point for injecting (6) eluent in one of the columns and in output a point for drawing (8) a fraction of the mixture. The method includes the following steps: batch injection of the mixture to be separated in the open separation loop (4); collecting at least two fractions; offsetting at least one column of the eluent injecting and fraction drawing points (6, 8) of the separation loop (4). The invention also concerns a device for separating fractions of a mixture to be separated.
摘要翻译：本发明涉及一种在装置（1）中分离待分离的混合物的级分的方法，包括：串联安装的几个色谱柱（21,22,23）; 一个开放的分离回路，包括输入一个点，用于在一个柱中注入（6）洗脱液，并输出一个点用于拉伸（8）一部分混合物。该方法包括以下步骤：在开放分离回路（4）中分批注入要分离的混合物; 收集至少两个馏分; 抵消分离回路（4）的洗脱液注入和分馏点（6,8）的至少一列。本发明还涉及用于分离要分离的混合物的馏分的装置。

6. 发明申请

US20040063992A1 High performance continuous reaction/separation process using a continuous liquid-solid contactor 有权
公开(公告)号：US20040063992A1
公开(公告)日：2004-04-01
申请号：US10412502
申请日：2003-04-11
发明人： Chen-Chou Chiang , David L. Fair
IPC分类号： C07C069/74
CPC分类号： C07C37/20 , B01D15/1857 , B01D15/1864 , B01D2215/023 , B01D2215/028 , C07C39/16
摘要： A process for reaction and separation which comprises inputting a process material into at least one column of a plurality of columns wherein each column has at least one inlet for accepting flow from another column or group of columns, an external feed stream, an external eluent stream or a combination thereof, and each column has at least one outlet for connecting to another column, a group of columns, an external product stream or a combination thereof. Each column is independently operable in an up-flow or down-flow mode and connected independently to one of the group comprising another column, an external feed stream, an external eluent stream, an external product stream and combinations thereof.

7. 发明申请

US20160145184A1 PROCESS FOR EQUILIBRIUM-LIMITED REACTIONS 有权
标题翻译：平衡有限反应的方法
公开(公告)号：US20160145184A1
公开(公告)日：2016-05-26
申请号：US14888535
申请日：2014-05-02
申请人： Georgia Tech Research Corporation , Dow Global Technologies LLC
发明人： Yoshiaki Kawajiri , Andreas Sebastian Bommarius , Timothy C. Frank , Mega E. Donaldson , Jungmin Oh , Gaurav Agrawal
IPC分类号： C07C51/48
CPC分类号： C07C51/48 , B01D15/1857 , B01D15/362 , B01D15/3857 , C07C67/08 , C07C67/56 , Y02P20/127 , C07C69/14
摘要： A process for conducting equilibrium-limited chemical reactions that produce water as a reaction product. Specifically, a process that uses a reactive chromatography unit (RCU) to improve the efficiency of equilibrium-limited reactions, such as a process for reacting glycol ether (GE) and carboxylic acid (CA) to form water and glycol ether ester (GEE). The process includes supplying GE and CA to the RCU, where one of either the CA or the GE is in a stoichiometric deficit relative to the other reactant. The reactant in the stoichiometric deficit reacts in the presence of the catalyst in the RCU to form a mixture of GEE and water. A raffinate is separated from the mixture using the separation media of the RCU contains at least the GEE. An extract separated from the mixture using the separation media of the RCU contains at least the water.
摘要翻译：一种产生水作为反应产物的平衡限制化学反应的方法。具体地，使用反应性色谱单元（RCU）来提高平衡有限反应的效率的方法，例如使二醇醚（GE）和羧酸（CA）反应形成水和二醇醚酯（GEE）的方法，。该方法包括向RCU提供GE和CA，其中CA或GE中的一个相对于其他反应物为化学计量的赤字。化学计量缺口中的反应物在RCU中的催化剂存在下反应以形成GEE和水的混合物。使用RCU的分离介质至少含有GEE，将萃余液与混合物分离。使用RCU的分离介质与混合物分离的提取物至少含有水。

8. 发明申请

US20130186832A1 SEPARATING COMPONENTS OF MIXED FLUID USING A FUNCTIONALLY GRADED MATERIAL 审中-公开
标题翻译：使用功能分级材料分离混合流体的组分
公开(公告)号：US20130186832A1
公开(公告)日：2013-07-25
申请号：US13744270
申请日：2013-01-17
申请人： Lawrence Livermore National Security, LLC
发明人： Andrew J. Pascall , George R. Farquar , Christopher M. Spadaccini , Sarah C. Chinn
IPC分类号： B01D15/18
CPC分类号： B01D15/18 , B01D15/1821 , B01D15/1828 , B01D15/1842 , B01D15/1857 , B01D15/1864 , B01D15/1885 , B01D15/22
摘要： A system for separating components of a fluid containing at least a first component and a second component includes a device having an inlet for introducing the fluid into the device, a first outlet for directing the first component of the fluid from the device, and a second outlet for directing the second component of the fluid from the device. A material that has a gradient in properties is located in the device between the inlet and the first and second outlets. The material has a first portion with an affinity for the first fluid component and a second portion with an affinity for the second fluid component. The first portion is positioned with relation to the first outlet such that the first component is directed from said device through the first outlet. The second portion is positioned with relation to the second outlet such that the second component is directed from the device through the second outlet.
摘要翻译：用于分离至少包含第一组分和第二组分的流体的组分的系统包括具有用于将流体引入装置的入口的装置，用于引导来自装置的流体的第一组分的第一出口，以及第二用于从装置引导流体的第二部件的出口。具有属性梯度的材料位于入口与第一和第二出口之间的装置中。该材料具有对第一流体组分具有亲和性的第一部分和对第二流体组分具有亲和力的第二部分。第一部分相对于第一出口定位，使得第一部件从所述装置通过第一出口引导。第二部分相对于第二出口定位，使得第二部件从装置通过第二出口引导。

9. 发明申请

US20110000853A1 PROCESS AND DEVICE FOR SEPARATING FRACTIONS OF A MIXTURE 有权
标题翻译：用于分离混合物的部分的方法和装置
公开(公告)号：US20110000853A1
公开(公告)日：2011-01-06
申请号：US12281170
申请日：2007-03-07
申请人： Eric Valery , Céline Morey
发明人： Eric Valery , Céline Morey
IPC分类号： B01D15/18 , B01D15/08 , B01D15/10
CPC分类号： B01D15/1828 , B01D15/1857
摘要： The invention concerns a method for separating fractions of a mixture using a chromatography device. The method includes the following steps: controlling in one node of the device, the history of a specific variable of the fractions of the mixture to be separated; detecting one characteristic point of the history, the characteristic point being between two successive steps of fraction collecting; comparing the position of the characteristic point relative to a target position; adjusting the amount of mobile phase modifying the position of the characteristic point to cause the position of the characteristic point to coincide with the target position. The invention also concerns a device for implementing the method. The method enables the operation of the device to be automatically set.
摘要翻译：本发明涉及使用色谱装置分离混合物的馏分的方法。该方法包括以下步骤：在设备的一个节点中控制要分离的混合物的分数的特定变量的历史; 检测历史的一个特征点，特征点在分级收集的两个连续步骤之间; 比较特征点相对于目标位置的位置; 调整移动相位的量，改变特征点的位置，使得特征点的位置与目标位置一致。本发明还涉及一种用于实现该方法的装置。该方法使得能够自动设置设备的操作。

10. 发明申请

US20040099605A1 High performance continuous reaction/separation process using a continuous liquid-solid contactor 审中-公开
标题翻译：使用连续液固接触器的高性能连续反应/分离过程
公开(公告)号：US20040099605A1
公开(公告)日：2004-05-27
申请号：US10207585
申请日：2002-07-29
发明人： Chen-Chou Chiang , David L. Fair
IPC分类号： C02F001/28 , C07C069/00
CPC分类号： B01D15/1857 , B01D15/1864 , B01D2215/023 , B01D2215/028 , C07C37/20 , C07C39/16
摘要： A process for reaction and separation which comprises inputting a process material into at least one column of a plurality of columns wherein each column has at least one inlet for accepting flow from another column or group of columns, an external feed stream, an external eluent stream or a combination thereof, and each column has at least one outlet for connecting to another column, a group of columns, an external product stream or a combination thereof. Each column is independently operable in an up-flow or down-flow mode and connected independently to one of the group comprising another column, an external feed stream, an external eluent stream, an external product stream and combinations thereof.
摘要翻译：一种用于反应和分离的方法，其包括将工艺材料输入到多个塔的至少一个塔中，其中每个塔具有至少一个入口，用于接受来自另一个塔或一组塔的流，外部进料流，外部洗脱液流或其组合，并且每个柱具有至少一个用于连接到另一个柱，一组柱，外部产物流或其组合的出口。每列可独立地在上流或下流模式下操作，并且独立地与包括另一柱，外部进料流，外部洗脱液流，外部产物流及其组合的组之一独立连接。

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