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1. 发明申请

US20100093530A1 METHOD OF PREPARING A COMPOSITION USING ARGENTATION CHROMATOGRAPHY 有权
标题翻译：使用归一化色谱法制备组合物的方法
公开(公告)号：US20100093530A1
公开(公告)日：2010-04-15
申请号：US12639137
申请日：2009-12-16
申请人： Thomas P. Binder , Doug Geier , Ahmad K. Hilaly , Robert Duane Sandage , John G. Soper
发明人： Thomas P. Binder , Doug Geier , Ahmad K. Hilaly , Robert Duane Sandage , John G. Soper
IPC分类号： B01J20/26
CPC分类号： B01D15/1828 , B01D15/20 , B01D15/362 , B01J20/0233 , B01J20/284 , B01J20/3234 , B01J20/3236 , B01J47/016 , C07C67/56 , C11B3/10 , G01N30/462 , C07C69/587 , C07C69/58
摘要： The present invention is directed to a method of preparing compositions enriched in compounds containing carbon chains of varying degrees of unsaturation using argentation chromatography. The present method utilizes an argentized cationic resin or a conditioned argentized alumina to separate compounds containing saturated or mono-unsaturated carbon chains from compounds having polyunsaturated carbon chains present in a starting composition. The invention is particularly useful for preparing a composition enriched in polyunsaturated fatty acid alkyl esters from mixtures of fatty acid esters in a starting composition derived from vegetable oils. The present invention is also directed to a method of preparing a conditioned argentized alumina adsorbent having increased selectivity for compounds containing one or more polyunsaturated carbon chains.
摘要翻译：本发明涉及使用梯度色谱法制备富集含有不同不饱和度的碳链的化合物的组合物的方法。本方法利用阳离子阳离子树脂或调节的氧化铝将起始组合物中存在的具有多不饱和碳链的化合物与饱和或单不饱和碳链分开。本发明特别可用于在源自植物油的起始组合物中由脂肪酸酯的混合物制备富含多不饱和脂肪酸烷基酯的组合物。本发明还涉及一种制备具有对含有一个或多个多不饱和碳链的化合物具有增加的选择性的调节的氧化铝吸附剂的方法。

2. 发明授权

US07828978B2 Simultaneous synthesis and purification of a fatty acid monoester biodiesel fuel 有权
标题翻译：同时合成和纯化脂肪酸单酯生物柴油
公开(公告)号：US07828978B2
公开(公告)日：2010-11-09
申请号：US11449199
申请日：2006-06-08
申请人： Doug Geier , John G. Soper
发明人： Doug Geier , John G. Soper
IPC分类号： B01D15/08 , C07C51/00 , C02F1/28 , C07C51/43
CPC分类号： B01D15/1857 , B01J8/0457 , C10G2300/1011 , C10L1/026 , C11C3/003 , Y02E50/13 , Y02P30/20
摘要： Simultaneous synthesis and purification of a fatty acid monoester biodiesel fuel from a triacylglycerol feedstock is described. In an exemplary method, the triacylglycerol feedstock is continuously contacted with a catalytic chromatographic bed comprising a first (solid phase) basic catalyst through a first port of a simulated moving bed chromatographic apparatus. A monohydric alcohol and optional second (mobile phase) basic catalyst is continuously contacted with the catalytic chromatographic bed through a second port and pumped in a first direction toward the triacylglycerol feedstock to contact the triacylglycerol in a reaction zone of the catalytic chromatographic bed where the fatty acid monoester and glycerol coproduct are formed. The fatty acid monoester is removed from the reaction zone through a product port of the simulated moving bed apparatus. Segments of the catalytic chromatographic bed are incrementally moved in a second direction, opposite the first direction, and the glycerol is removed from a raffinate port located opposite the product port of the apparatus.
摘要翻译：描述了从三酰基甘油原料同时合成和纯化脂肪酸单酯生物柴油燃料。在示例性方法中，三酰基甘油原料通过模拟移动床层析装置的第一端口与包含第一（固相）碱性催化剂的催化色谱床连续接触。一元醇和任选的第二（流动相）碱性催化剂通过第二端口与催化色谱床连续接触并沿着第一方向朝向三酰基甘油原料泵送，以在催化色谱床的反应区中与三酰基甘油接触，其中脂肪形成酸单酯和甘油副产物。脂肪酸单酯通过模拟移动床装置的产品端口从反应区域中除去。催化色谱层的分段沿与第一方向相反的第二方向递增移动，并且甘油从位于装置的产品端口的抽出物端口移除。

3. 发明授权

US08088710B2 Method of preparing a composition using argentation chromatography 有权
标题翻译：使用梯度色谱法制备组合物的方法
公开(公告)号：US08088710B2
公开(公告)日：2012-01-03
申请号：US12639137
申请日：2009-12-16
申请人： Thomas P. Binder , Doug Geier , Ahmad K. Hilaly , Robert D. Sandage , John G. Soper
发明人： Thomas P. Binder , Doug Geier , Ahmad K. Hilaly , Robert D. Sandage , John G. Soper
IPC分类号： B01J20/00
CPC分类号： B01D15/1828 , B01D15/20 , B01D15/362 , B01J20/0233 , B01J20/284 , B01J20/3234 , B01J20/3236 , B01J47/016 , C07C67/56 , C11B3/10 , G01N30/462 , C07C69/587 , C07C69/58
摘要： The present invention is directed to a method of preparing compositions enriched in compounds containing carbon chains of varying degrees of unsaturation using argentation chromatography. The present method utilizes an argentized cationic resin or a conditioned argentized alumina to separate compounds containing saturated or mono-unsaturated carbon chains from compounds having polyunsaturated carbon chains present in a starting composition. The invention is particularly useful for preparing a composition enriched in polyunsaturated fatty acid alkyl esters from mixtures of fatty acid esters in a starting composition derived from vegetable oils. The present invention is also directed to a method of preparing a conditioned argentized alumina adsorbent having increased selectivity for compounds containing one or more polyunsaturated carbon chains.
摘要翻译：本发明涉及使用梯度色谱法制备富集含有不同不饱和度的碳链的化合物的组合物的方法。本方法利用阳离子阳离子树脂或调节的氧化铝将起始组合物中存在的具有多不饱和碳链的化合物与饱和或单不饱和碳链分开。本发明特别可用于在源自植物油的起始组合物中由脂肪酸酯的混合物制备富含多不饱和脂肪酸烷基酯的组合物。本发明还涉及一种制备具有对含有一个或多个多不饱和碳链的化合物具有增加的选择性的调节的氧化铝吸附剂的方法。

4. 发明申请

US20070158270A1 Simultaneous synthesis and purification of a fatty acid monoester biodiesel fuel 有权
标题翻译：同时合成和纯化脂肪酸单酯生物柴油
公开(公告)号：US20070158270A1
公开(公告)日：2007-07-12
申请号：US11449199
申请日：2006-06-08
申请人： Doug Geier , John G. Soper
发明人： Doug Geier , John G. Soper
IPC分类号： B01D15/08
CPC分类号： B01D15/1857 , B01J8/0457 , C10G2300/1011 , C10L1/026 , C11C3/003 , Y02E50/13 , Y02P30/20
摘要： Simultaneous synthesis and purification of a fatty acid monoester biodiesel fuel from a triacylglycerol feedstock is described. In an exemplary method, the triacylglycerol feedstock is continuously contacted with a catalytic chromatographic bed comprising a first (solid phase) basic catalyst through a first port of a simulated moving bed chromatographic apparatus. A monohydric alcohol and optional second (mobile phase) basic catalyst is continuously contacted with the catalytic chromatographic bed through a second port and pumped in a first direction toward the triacylglycerol feedstock to contact the triacylglycerol in a reaction zone of the catalytic chromatographic bed where the fatty acid monoester and glycerol coproduct are formed. The fatty acid monoester is removed from the reaction zone through a product port of the simulated moving bed apparatus. Segments of the catalytic chromatographic bed are incrementally moved in a second direction, opposite the first direction, and the glycerol is removed from a raffinate port located opposite the product port of the apparatus.
摘要翻译：描述了从三酰基甘油原料同时合成和纯化脂肪酸单酯生物柴油燃料。在示例性方法中，三酰基甘油原料通过模拟移动床层析装置的第一端口与包含第一（固相）碱性催化剂的催化色谱床连续接触。一元醇和任选的第二（流动相）碱性催化剂通过第二端口与催化色谱床连续接触并沿着第一方向朝向三酰基甘油原料泵送，以在催化色谱床的反应区域中与三酰基甘油接触，其中脂肪形成酸单酯和甘油副产物。脂肪酸单酯通过模拟移动床装置的产品端口从反应区域中除去。催化色谱层的分段沿与第一方向相反的第二方向递增移动，并且甘油从位于装置的产品端口的抽出物端口移除。

5. 发明授权

US07667061B2 Method of preparing a composition using argentation chromatography 有权
标题翻译：使用梯度色谱法制备组合物的方法
公开(公告)号：US07667061B2
公开(公告)日：2010-02-23
申请号：US11612250
申请日：2006-12-18
申请人： Thomas P. Binder , Doug Geier , Ahmad K. Hilaly , Robert Duane Sandage , John G. Soper
发明人： Thomas P. Binder , Doug Geier , Ahmad K. Hilaly , Robert Duane Sandage , John G. Soper
IPC分类号： C11B7/00 , B01D15/00
CPC分类号： B01D15/1828 , B01D15/20 , B01D15/362 , B01J20/0233 , B01J20/284 , B01J20/3234 , B01J20/3236 , B01J47/016 , C07C67/56 , C11B3/10 , G01N30/462 , C07C69/587 , C07C69/58
摘要： The present invention is directed to a method of preparing compositions enriched in compounds containing carbon chains of varying degrees of unsaturation using argentation chromatography. The present method utilizes an argentized cationic resin or a conditioned argentized alumina to separate compounds containing saturated or mono-unsaturated carbon chains from compounds having polyunsaturated carbon chains present in a starting composition. The invention is particularly useful for preparing a composition enriched in polyunsaturated fatty acid alkyl esters from mixtures of fatty acid esters in a starting composition derived from vegetable oils. The present invention is also directed to a method of preparing a conditioned argentized alumina adsorbent having increased selectivity for compounds containing one or more polyunsaturated carbon chains.
摘要翻译：本发明涉及使用梯度色谱法制备富集含有不同不饱和度的碳链的化合物的组合物的方法。本方法利用阳离子阳离子树脂或调节的氧化铝将起始组合物中存在的具有多不饱和碳链的化合物与饱和或单不饱和碳链分开。本发明特别可用于在源自植物油的起始组合物中由脂肪酸酯的混合物制备富含多不饱和脂肪酸烷基酯的组合物。本发明还涉及一种制备具有对含有一个或多个多不饱和碳链的化合物具有增加的选择性的调节的氧化铝吸附剂的方法。

6. 发明申请

US20070181504A1 Method of Preparing a Composition Using Argentation Chromatography 有权
标题翻译：使用阿根廷色谱法制备组合物的方法
公开(公告)号：US20070181504A1
公开(公告)日：2007-08-09
申请号：US11612250
申请日：2006-12-18
申请人： Thomas Binder , Doug Geier , Ahmad Hilaly , Robert Sandage , John Soper
发明人： Thomas Binder , Doug Geier , Ahmad Hilaly , Robert Sandage , John Soper
IPC分类号： B01D15/08
CPC分类号： B01D15/1828 , B01D15/20 , B01D15/362 , B01J20/0233 , B01J20/284 , B01J20/3234 , B01J20/3236 , B01J47/016 , C07C67/56 , C11B3/10 , G01N30/462 , C07C69/587 , C07C69/58
摘要： The present invention is directed to a method of preparing compositions enriched in compounds containing carbon chains of varying degrees of unsaturation using argentation chromatography. The present method utilizes an argentized cationic resin or a conditioned argentized alumina to separate compounds containing saturated or mono-unsaturated carbon chains from compounds having polyunsaturated carbon chains present in a starting composition. The invention is particularly useful for preparing a composition enriched in polyunsaturated fatty acid alkyl esters from mixtures of fatty acid esters in a starting composition derived from vegetable oils. The present invention is also directed to a method of preparing a conditioned argentized alumina adsorbent having increased selectivity for compounds containing one or more polyunsaturated carbon chains.
摘要翻译：本发明涉及使用梯度色谱法制备富集含有不同不饱和度的碳链的化合物的组合物的方法。本方法利用阳离子阳离子树脂或调节的氧化铝将起始组合物中存在的具有多不饱和碳链的化合物与饱和或单不饱和碳链分开。本发明特别可用于在源自植物油的起始组合物中由脂肪酸酯的混合物制备富含多不饱和脂肪酸烷基酯的组合物。本发明还涉及一种制备具有对含有一个或多个多不饱和碳链的化合物具有增加的选择性的调节的氧化铝吸附剂的方法。

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