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    • 3. 发明授权
    • Decaffeinating coffee and tea
    • 减肥咖啡和茶
    • US5153015A
    • 1992-10-06
    • US815895
    • 1991-12-31
    • Peter TheissingPeter SaamerJorg-Peter Korner
    • Peter TheissingPeter SaamerJorg-Peter Korner
    • A23F3/36A23F5/20B01D11/02C07D473/12C07G99/00C11B9/02
    • B01D11/0203A23F3/366A23F5/206C07D473/12
    • A process and apparatus for extracting ingredient substances from natural products by means of a pressurized fluid, particularly for decaffeinating tea leaves by means of carbon dioxide, wherein the ingredient substances are bound by an adsorbent, preferably activated carbon. The fluid is conducted through a product layer, the thickness of which in flow direction is small in comparision with that transversely of the flow direction and the fluid is passed through the product layer with changing, especially increasing, velocity. The apparatus includes a cylindrical high-pressure vessel with annular cylindrical baskets for accommodating the natural product and/or the adsorbent, and the gas flows from a cylindrical outer range to a cylindrical inner range. The time required for the treatment of leafy natural product is reduced, the flow paths of the fluid are shortened, thus diminishing the risk of clogging, and the fluid flow velocity is reduced.
    • 一种通过加压流体,特别是通过二氧化碳去除咖啡因的茶叶从天然产物中提取成分物质的方法和装置,其中成分物质被吸附剂,优选活性炭结合。 流体通过产品层传导,其厚度与流动方向的横向相比在流动方向上较小,并且流体以改变,特别是增加的速度通过产品层。 该装置包括一圆柱形高压容器,其具有用于容纳天然产物和/或吸附剂的环形圆柱形篮,并且气体从圆柱形外部范围流动到圆柱形内部范围。 减少叶片天然产物处理所需的时间,流体的流动路径缩短,从而降低堵塞的风险,降低流体流动速度。
    • 4. 发明授权
    • Process for decaffinating green coffee beans
    • 去除绿咖啡豆的方法
    • US5089280A
    • 1992-02-18
    • US63372
    • 1987-06-18
    • Hedi Ben-NasrFriedrich W. H. Coenen
    • Hedi Ben-NasrFriedrich W. H. Coenen
    • A23F5/02A23F5/20
    • A23F5/206A23F5/02
    • A simple, reliable process for decaffeinating green coffee beans to a high degree while avoiding denaturation of the green coffee beans includes wetting the green coffee beans to a high water content of 35-50%-wt.; compressing the beans in a pressure chamber for a period of a few minutes to several hours in an atmosphere comprised of a supercritical fluid which is a gas at STP, at a temperature ranging from 20.degree. to 80.degree. C. under a critical pressure ranging from 75 to 300 bar; decompressing the wetted beans from critical pressure p.sub.c to a pressure p for which p.sub.c .ltoreq.p.ltoreq.1 bar abruptly or in the space of a few minutes, while avoiding freezing the green coffee beans; washing with water or with the supercritical fluid for selective extraction of the caffeine; repeating the process one or more times; centrifuging; drying; and roasting the beans. Further, caffeine is recovered in a known manner from the washing medium.
    • 一个简单,可靠的方法,以高度脱咖啡因的绿咖啡豆,同时避免绿色咖啡豆的变性包括将绿色咖啡豆润湿至35-50%重量级的高含水量; 在压力室内压缩豆类在几分钟至数小时的时间内,在由STP中的气体制成的超临界流体气氛中,温度为20℃至80℃,临界压力范围为 75到300巴; 将湿豆从临界压力pc减压到突然间或几分钟的空间中的p p的压力p,同时避免冷冻生咖啡豆; 用水或与超临界流体一起洗涤以选择性地提取咖啡因; 重复一次或多次; 离心; 烘干; 并烘烤豆类。 此外,咖啡因以已知的方式从洗涤介质中回收。