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    • 8. 发明授权
    • Method for stopping operation of reactor
    • 停止反应器运行的方法
    • US09200210B2
    • 2015-12-01
    • US14007473
    • 2012-03-15
    • Shinya Arai
    • Shinya Arai
    • C07C27/00C10G3/00C10G2/00
    • C10G3/60C10G2/33C10G2/342C10G2300/4031Y02P30/20
    • The method for stopping operation of a reactor is provided with a stop step of stopping supply of a synthesis gas containing a carbon monoxide gas and a hydrogen gas into the reactor; a slurry discharge step of discharging slurry from the reactor; a steam supply step of supplying steam higher in temperature than the decomposition temperatures of metal carbonyls into the reactor, thereby discharging gaseous matters inside the reactor; and a carbon monoxide gas detecting step of detecting an amount of carbon monoxide gas contained in the gaseous matters discharged from the reactor. In the steam supply step, supply of the steam is stopped when an amount of the detected carbon monoxide gas continuously declines to be lower than a predetermined reference value.
    • 停止反应器运转的方法具有停止向反应器供给包含一氧化碳气体和氢气的合成气的停止步骤; 从反应器排出浆料的浆料排出步骤; 蒸汽供给步骤,将比金属羰基化物的分解温度更高的蒸气供给到反应器中,从而将反应器内的气态物质排出; 以及一氧化碳气体检测步骤,检测从反应器排出的气态物质中所含的一氧化碳气体的量。 在蒸汽供给步骤中,当检测到的一氧化碳气体的量持续下降到低于预定的参考值时,停止供给蒸汽。