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1. 发明授权

US07244478B2 Recording medium having ink-receiving layer and method of manufacturing the same 失效
标题翻译：具有油墨接收层的记录介质及其制造方法
公开(公告)号：US07244478B2
公开(公告)日：2007-07-17
申请号：US10664872
申请日：2003-09-22
申请人： Yuji Kondo , Shigehira Iida , Tsuyoshi Santo , Motoaki Sato , Kenichi Yamaguchi
发明人： Yuji Kondo , Shigehira Iida , Tsuyoshi Santo , Motoaki Sato , Kenichi Yamaguchi
IPC分类号： B41M5/40
CPC分类号： B41M5/52 , B41M5/508 , B41M5/5218 , B41M5/5254
摘要： A method of manufacturing a recording medium with an excellent productivity is provided. The method provides a recording medium having excellent ink absorbency and coloring property and includes an ink-receiving layer in which a binder is restricted and controlled. The present invention provides a method of manufacturing a recording medium including the steps of: performing a surface treatment on a substrate; and forming an ink-receiving layer using at least a pigment, polyvinyl alcohol, and a coating liquid that contains at least one selected from the group consisting of boric acid and borate. In this method, the surface-treatment step includes a first surface treatment and a second surface treatment. In the first surface treatment, a coating liquid that contains at least one selected from the group consisting of boric acid and borate is applied followed by being dried and solidified. In the second surface treatment, after the first surface treatment, a coating liquid that contains at least one selected from the group consisting of boric acid and borate is applied on the substrate. While the substrate is in a state of being wet by the coating liquid applied in the second surface treatment, the substrate is further coated with a coating liquid for forming the ink-receiving layer.
摘要翻译：提供了一种制造具有优异生产率的记录介质的方法。该方法提供了具有优异的油墨吸收性和着色性的记录介质，并且包括其中粘合剂被限制和控制的油墨接收层。本发明提供一种制造记录介质的方法，包括以下步骤：对基底进行表面处理; 以及使用至少含有选自硼酸和硼酸盐中的至少一种的颜料，聚乙烯醇和涂布液形成油墨接收层。在该方法中，表面处理步骤包括第一表面处理和第二表面处理。在第一表面处理中，涂布含有选自硼酸和硼酸盐中的至少一种的涂布液，然后进行干燥固化。在第二表面处理中，在第一表面处理之后，在基板上涂布含有选自硼酸和硼酸盐中的至少一种的涂布液。当基板处于被第二表面处理中施加的涂布液湿润的状态时，基板进一步涂覆有用于形成油墨接收层的涂布液。

2. 发明授权

US07255901B2 Recording medium for ink and method for producing the same 有权
标题翻译：油墨记录介质及其制造方法
公开(公告)号：US07255901B2
公开(公告)日：2007-08-14
申请号：US10678143
申请日：2003-10-06
申请人： Kenichi Yamaguchi , Shigehira Iida , Tsuyoshi Santo , Yuji Kondo , Motoaki Sato
发明人： Kenichi Yamaguchi , Shigehira Iida , Tsuyoshi Santo , Yuji Kondo , Motoaki Sato
IPC分类号： B41M5/50
CPC分类号： B41M5/506 , B41M5/5218 , B41M5/5236 , B41M5/5245 , B41M5/5254
摘要： A recording medium for ink, capable of rapidly absorbing large amounts of ink, showing excellent color forming ability and capable of suppressing image deterioration caused by dye displacement that occurs when an image is stored in humid conditions and image deterioration caused by light when a printed image is displayed, and providing a printed image showing excellent long-term stability. The invention also provides a recording medium for ink having at least one layer provided on a substrate, and an ink receiving layer containing alumina hydrate as an outermost layer. A surface of the substrate at least on the side of the ink receiving layer is subjected to a cationizing treatment. An undercoat layer is provided on the same side as the cationizing treatment, to obtain cations in a predetermined distribution. The outermost ink receiving layer is provided on the undercoat layer.
摘要翻译：一种用于油墨的记录介质，能够快速吸收大量的油墨，显示出优良的成色能力，并且能够抑制当在潮湿条件下存储图像时发生的染料位移引起的图像劣化，以及当打印图像时由光引起的图像劣化并且提供显示出优异的长期稳定性的打印图像。本发明还提供了一种用于油墨的记录介质，其具有设置在基板上的至少一层，以及含有氧化铝水合物作为最外层的油墨接收层。至少在油墨接收层一侧的基材表面进行阳离子化处理。在与阳离子化处理相同的一侧设置底涂层，以获得预定分布的阳离子。最外层的油墨接收层设置在底涂层上。

3. 发明申请

US20070166487A1 RECORDING MEDIUM FOR INK AND METHOD FOR PRODUCING THE SAME 有权
标题翻译：油墨记录介质及其制造方法
公开(公告)号：US20070166487A1
公开(公告)日：2007-07-19
申请号：US11687906
申请日：2007-03-19
申请人： Kenichi Yamaguchi , Shigehira Iida , Tsuyoshi Santo , Yuji Kondo , Motoaki Sato
发明人： Kenichi Yamaguchi , Shigehira Iida , Tsuyoshi Santo , Yuji Kondo , Motoaki Sato
IPC分类号： B41M5/50 , B41M5/40
CPC分类号： B41M5/506 , B41M5/5218 , B41M5/5236 , B41M5/5245 , B41M5/5254
摘要： The invention provides a recording medium for ink having an ink absorbing ability capable of absorbing ink of a large amount at a high speed, showing an excellent color forming ability and capable of suppressing an image deterioration by a dye displacement which tends to appear particularly in an image storage under a high humidity condition, and an image deterioration caused by light when a printed image is displayed, and showing an excellent stability with time of the printed image, and a method for producing such recording medium for ink. The invention also provides a recording medium for ink having at least one layer laminated on a substrate and including an ink receiving layer containing alumina hydrate as an outermost layer, in which a surface of the substrate at least on the side of the ink receiving layer is subjected to a cationizing treatment, further having an undercoat layer on the side of such cationizing treatment to obtain cations in a predetermined distribution, and having an outermost ink receiving layer laminated on said undercoat layer, and a producing method for such recording medium for ink.
摘要翻译：本发明提供了具有能够高速吸收大量油墨的油墨吸收能力的油墨记录介质，显示出优良的成色能力并且能够抑制特别是在在高湿度条件下的图像存储，以及当显示打印图像时由光引起的图像劣化，并且显示出打印图像的时间优异的稳定性，以及用于制造这种油墨记录介质的方法。本发明还提供了一种用于油墨的记录介质，其具有层压在基材上的至少一层，并且包括含有氧化铝水合物作为最外层的油墨接收层，其中至少在油墨接收层侧的基材的表面是进行阳离子化处理，在该阳离子化处理侧进一步具有底涂层以获得预定分布的阳离子，并且具有层压在所述底涂层上的最外层油墨接收层，以及这种用于油墨的记录介质的制备方法。

4. 发明授权

US07790223B2 Recording medium for ink and method for producing the same 有权
标题翻译：油墨记录介质及其制造方法
公开(公告)号：US07790223B2
公开(公告)日：2010-09-07
申请号：US11687906
申请日：2007-03-19
申请人： Kenichi Yamaguchi , Shigehira Iida , Tsuyoshi Santo , Yuji Kondo , Motoaki Sato
发明人： Kenichi Yamaguchi , Shigehira Iida , Tsuyoshi Santo , Yuji Kondo , Motoaki Sato
IPC分类号： B41M5/50
CPC分类号： B41M5/506 , B41M5/5218 , B41M5/5236 , B41M5/5245 , B41M5/5254
摘要： The invention provides a recording medium for ink having an ink absorbing ability capable of absorbing ink of a large amount at a high speed, showing an excellent color forming ability and capable of suppressing an image deterioration by a dye displacement which tends to appear particularly in an image storage under a high humidity condition, and an image deterioration caused by light when a printed image is displayed, and showing an excellent stability with time of the printed image, and a method for producing such recording medium for ink.The invention also provides a recording medium for ink having at least one layer laminated on a substrate and including an ink receiving layer containing alumina hydrate as an outermost layer, in which a surface of the substrate at least on the side of the ink receiving layer is subjected to a cationizing treatment, further having an undercoat layer on the side of such cationizing treatment to obtain cations in a predetermined distribution, and having an outermost ink receiving layer laminated on said undercoat layer, and a producing method for such recording medium for ink.
摘要翻译：本发明提供了具有能够高速吸收大量油墨的油墨吸收能力的油墨记录介质，显示出优良的成色能力并且能够抑制特别是在在高湿度条件下的图像存储，以及当显示打印图像时由光引起的图像劣化，并且显示出打印图像的时间优异的稳定性，以及用于制造这种油墨记录介质的方法。本发明还提供了一种用于油墨的记录介质，其具有层压在基材上的至少一层，并且包括含有氧化铝水合物作为最外层的油墨接收层，其中至少在油墨接收层侧的基材的表面是进行阳离子化处理，在该阳离子化处理侧进一步具有底涂层以获得预定分布的阳离子，并且具有层压在所述底涂层上的最外层油墨接收层，以及这种用于油墨的记录介质的制备方法。

5. 发明申请

US20060141176A1 Recording medium having ink-receiving layer and method of manufacturing the same 审中-公开
标题翻译：具有油墨接收层的记录介质及其制造方法
公开(公告)号：US20060141176A1
公开(公告)日：2006-06-29
申请号：US11356382
申请日：2006-02-17
申请人： Yuji Kondo , Shigehira Iida , Tsuyoshi Santo , Motoaki Sato , Kenichi Yamaguchi
发明人： Yuji Kondo , Shigehira Iida , Tsuyoshi Santo , Motoaki Sato , Kenichi Yamaguchi
IPC分类号： B41M5/00
CPC分类号： B41M5/52 , B41M5/508 , B41M5/5218 , B41M5/5254
摘要： A method of manufacturing a recording medium with an excellent productivity is provided. The method provides a recording medium having excellent ink absorbency and coloring property and includes an ink-receiving layer in which a binder is restricted and controlled. The present invention provides a method of manufacturing a recording medium including the steps of: performing a surface treatment on a substrate; and forming an ink-receiving layer using at least a pigment, polyvinyl alcohol, and a coating liquid that contains at least one selected from the group consisting of boric acid and borate. In this method, the surface-treatment step includes a first surface treatment and a second surface treatment. In the first surface treatment, a coating liquid that contains at least one selected from the group consisting of boric acid and borate is applied followed by being dried and solidified. In the second surface treatment, after the first surface treatment, a coating liquid that contains at least one selected from the group consisting of boric-acid and borate is applied on the substrate. While the substrate is in a state of being wet by the coating liquid applied in the second surface treatment, the substrate is further coated with a coating liquid for forming the ink-receiving layer.
摘要翻译：提供了一种制造具有优异生产率的记录介质的方法。该方法提供了具有优异的油墨吸收性和着色性的记录介质，并且包括其中粘合剂被限制和控制的油墨接收层。本发明提供一种制造记录介质的方法，包括以下步骤：对基底进行表面处理; 以及使用至少含有选自硼酸和硼酸盐中的至少一种的颜料，聚乙烯醇和涂布液形成油墨接收层。在该方法中，表面处理步骤包括第一表面处理和第二表面处理。在第一表面处理中，涂布含有选自硼酸和硼酸盐中的至少一种的涂布液，然后进行干燥固化。在第二表面处理中，在第一表面处理之后，在基板上涂布含有选自硼酸和硼酸盐中的至少一种的涂布液。当基板处于被第二表面处理中施加的涂布液湿润的状态时，基板进一步涂覆有用于形成油墨接收层的涂布液。

6. 发明授权

US4953498A Microwave plasma CVD apparatus having substrate shielding member 失效
标题翻译：具有基板屏蔽部件的微波等离子体CVD装置
公开(公告)号：US4953498A
公开(公告)日：1990-09-04
申请号：US477123
申请日：1990-02-07
申请人： Junichiro Hashizume , Tetsuya Takei , Shigehira Iida , Keishi Saitoh , Takayoshi Arai
发明人： Junichiro Hashizume , Tetsuya Takei , Shigehira Iida , Keishi Saitoh , Takayoshi Arai
IPC分类号： C23C16/50 , C23C16/44 , C23C16/455 , C23C16/511 , G03G5/08 , H01J37/32 , H01L21/205 , H01L31/04
CPC分类号： H01J37/32623 , C23C16/511 , H01J37/32633
摘要： An improved MW-PCVD apparatus, characterized in that in the MW-CVD apparatus having a substrate onto which a deposited film to be formed and a space near the substrate for the decomposition of a raw material gas with the action of microwave energy, a shielding member is provided between said substrate and said space, which has an opening to allow part of the decomposed raw material gas species to be passed toward the substrate.
摘要翻译：一种改进的MW-PCVD装置，其特征在于，在具有基板的MW-CVD装置中，其上形成有沉积膜和在基板附近的空间，用于利用微波能量分解原料气体，屏蔽构件设置在所述基板和所述空间之间，所述空间具有允许部分分解的原料气体种类向基板通过的开口。

7. 发明授权

US4897281A Process for the formation of a functional deposited film by way of microwave plasma CVD method 失效
标题翻译：通过微波等离子体CVD法形成功能沉积膜的工艺
公开(公告)号：US4897281A
公开(公告)日：1990-01-30
申请号：US198746
申请日：1988-05-25
申请人： Takayoshi Arai , Shigehira Iida , Keishi Saitoh , Junichiro Hashizume , Tetsuya Takei
发明人： Takayoshi Arai , Shigehira Iida , Keishi Saitoh , Junichiro Hashizume , Tetsuya Takei
IPC分类号： C23C16/50 , B01J19/12 , C23C16/511 , C23C16/52 , H01J37/32 , H01L21/205 , H01L31/0248
CPC分类号： H01J37/32935 , B01J19/126 , C23C16/511 , H01L21/02425 , H01L21/02532 , H01L21/0262 , B01J2219/0894
摘要： According to the present invention, there is provided an improved process for the formation of a deposited film by way of a microwave plasma CVD method, the improvement comprising monitoring an effective power of a microwave to be introduced into a reaction chamber, leading to a control means an output signal indicative of the effective power corresponding a plasma intensity, and automatically controlling the matching between the reaction chamber and the microwave to be introduced into the reaction chamber according to an output signal from the control means. According to the above process, even after a long discharge time has elapsed, the plasma intensity in the reaction chamber may be maintained constant, and the effective power of the microwave to be introduced into the reaction chamber may be therefore maintained constant. Because of this, it becomes possible to repeatedly and stably prepare a desired deposited film excelling in the uniformity of the thickness and that of the quality at a high deposition rate.
摘要翻译：根据本发明，提供了一种通过微波等离子体CVD法形成沉积膜的改进方法，其改进包括监测要引入反应室的微波的有效功率，从而进行控制表示表示与等离子体强度相对应的有效功率的输出信号，并且根据来自控制装置的输出信号自动控制反应室与微波之间的匹配以引入反应室。根据上述处理，即使经过长时间的放电时间，反应室内的等离子体强度也可以保持恒定，因此可以将导入反应室的微波的有效功率保持恒定。因此，能够以高的沉积速度重复且稳定地制备在厚度均匀性和质量均匀性方面优异的所需沉积膜。

8. 发明授权

US4957772A Method for forming functional deposited films by means of microwave plasma chemical vapor deposition method 失效
标题翻译：通过微波等离子体化学气相沉积法形成功能性沉积膜的方法
公开(公告)号：US4957772A
公开(公告)日：1990-09-18
申请号：US287666
申请日：1988-12-21
申请人： Keishi Saitoh , Junichiro Hashizume , Shigehira Iida , Tetsuya Takei , Takayoshi Arai
发明人： Keishi Saitoh , Junichiro Hashizume , Shigehira Iida , Tetsuya Takei , Takayoshi Arai
IPC分类号： C23C16/511
CPC分类号： C23C16/511 , Y10S148/045 , Y10S148/065
摘要： An improved method for forming a functional deposited film by introducing a raw material gas into a substantially enclosed reaction chamber containing a substrate onto which the functional deposited film is to be deposited and coupling microwave energy from a source of microwave energy thereinto to thereby form a glow discharge plasma causing decomposition of the raw material gas whereby forming the functional deposited film on the substrate, the improvement comprising supplying microwave of a power equivalent to 1.1 times or more over that of microwave with which the deposition rate for the decomposed products from the raw material gas being deposited onto the substrate to be saturated to the raw material gas in the reaction chamber and regulating the inner pressure of the reaction chamber to a vacuum of 10 m Torr or less.According to the method of this invention, there can be formed a desired functional deposited film having a wealth of many practically applicable characteristics and having an improved response speed against photocurrent at an improved deposition rate with a raw material gas utilization efficiency of hundred percent or nearly hundred percent. And the method of this invention makes it possible to mass-produce various functional elements comprising such deposited film usable in electrophotographic photosensitive member, photosensor, thin-film transistor, solar cell, etc. on an industrial scale thereby enabling low cost production.
摘要翻译：通过将原料气体引入包含要沉积功能性沉积膜的基板的基本封闭的反应室中，并将来自微波能量的微波能量耦合到其中形成发光，从而形成功能沉积膜的改进方法放电等离子体引起原料气体分解，由此在基板上形成功能沉积膜，其改进在于提供微波功率相当于来自原料的分解产物沉积速率的微波的1.1倍或更多倍将沉积在基板上的气体饱和到反应室中的原料气体中，并将反应室的内部压力调节至10mTorr以下的真空。根据本发明的方法，可以形成具有许多实际应用特性的期望的功能性沉积膜，并且在提高的沉积速率下具有改善的光电流响应速度，原料气体利用效率为百分之百或几乎百分之百。并且本发明的方法使得可以在工业规模上大量生产包括可用于电子照相感光构件，光电传感器，薄膜晶体管，太阳能电池等的这种沉积膜的各种功能元件，从而能够实现低成本生产。

9. 发明授权

US4897284A Process for forming a deposited film on each of a plurality of substrates by way of microwave plasma chemical vapor deposition method 失效
标题翻译：通过微波等离子体化学气相沉积法在多个基板上形成沉积膜的工艺
公开(公告)号：US4897284A
公开(公告)日：1990-01-30
申请号：US166553
申请日：1988-03-10
申请人： Takayoshi Arai , Shigehira Iida , Junichiro Hashizume , Tetsuya Takei , Keishi Saitoh
发明人： Takayoshi Arai , Shigehira Iida , Junichiro Hashizume , Tetsuya Takei , Keishi Saitoh
IPC分类号： C23C16/44 , C23C16/24 , C23C16/455 , C23C16/511 , G03G5/08 , G03G5/082 , H01L21/205 , H01L31/0248
CPC分类号： C23C16/24 , C23C16/511 , G03G5/08278
摘要： An improvement in the known MW-PCVD process for forming a deposited film on each of a plurality of cylindrical substrates being so arranged as to surround the discharging space in a substantially enclosed reaction space of a deposition chamber by the glow discharge of raw material gas to generate plasmas containing reactive gaseous materials causing the formation of said deposited film in the discharging space while rotating said plurality of substrates, which comprises providing a gas feed pipe provided with a plurality of gas liberation holes opening into the discharging space in every space between every two of the substrates so as to form an encircled discharging space and an open non-discharging space by said plurality of cylindrical substrates and a plurality of gas feed pipes and regulating the deposit thickness to be deposited per a rotation cycle of the substrate passing through the discharging space and the non-discharging space to a 1000 .ANG. or less.
摘要翻译：用于在多个圆柱形基板中的每一个上形成沉积膜的已知的MW-PCVD工艺的改进被布置成通过原料气体的辉光放电在沉积室的基本封闭的反应空间中包围放电空间，产生包含反应性气体材料的等离子体，导致在排出空间中形成所述沉积膜，同时旋转所述多个基板，其包括提供气体供给管，该气体供给管设置有在每两个空间之间的每个空间中通向排放空间的多个气体释放孔以便通过所述多个圆柱形基底和多个气体供给管形成环绕的排出空间和开放的非排放空间，并且每个循环通过放电的衬底的旋转周期来调节沉积物的沉积厚度空间和不排放空间达到1000安格或以下。

10. 发明授权

US5061511A Method for forming functional deposited films by means of microwave plasma chemical vapor deposition method 失效
标题翻译：通过微波等离子体蒸发沉积方法形成功能性沉积膜的方法
公开(公告)号：US5061511A
公开(公告)日：1991-10-29
申请号：US551081
申请日：1990-07-11
申请人： Keishi Saitoh , Junichiro Hashizume , Shigehira Iida , Tetsuya Takei , Takayoshi Arai
发明人： Keishi Saitoh , Junichiro Hashizume , Shigehira Iida , Tetsuya Takei , Takayoshi Arai
IPC分类号： C23C16/511
CPC分类号： C23C16/511 , Y10S148/045 , Y10S148/065
摘要： An improved method for forming a functional deposited film by introducing a raw material gas into a substantially enclosed reaction chamber containing a substrate onto which the functional deposited film is to be deposited and coupling microwave energy from a source of microwave energy thereinto to thereby form a glow discharge plasma causing decomposition of the raw material gas whereby forming the functional deposited film on the substrate, the improvement comprising supplying microwave of a power equivalent of 1.1 times or more over that of microwave with which the deposition rate for the decomposed products from the raw material gas being deposited onto the substrate to be saturated to the raw material gas in the reaction chamber and regulating the inner pressure of the reaction chamber to a vacuum of 10 m Torr or less.According to the method of this invention, there can be formed a desired functional deposited film having a wealth of many practically applicable characteristics and having an improved response speed against photocurrent at an improved deposition rate with a raw material gas utilization efficiency of hundred percent or nearly hundred percent. And the method of this invention makes it possible to mass-produce various functional elements comprising such deposited film usable in electrophotographic photosensitive member, photosensor, thin-film transistor, solar cell, etc. on an industrial scale thereby enabling low cost production.

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