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1. 发明授权

US06627047B1 Method for preventing polymerization in thin-film type evaporating device 有权
标题翻译：薄膜型蒸发装置防止聚合的方法
公开(公告)号：US06627047B1
公开(公告)日：2003-09-30
申请号：US09556754
申请日：2000-04-21
申请人： Yuichi Ijiri , Takeshi Nishimura , Yukihiro Matsumoto
发明人： Yuichi Ijiri , Takeshi Nishimura , Yukihiro Matsumoto
IPC分类号： B01D122
CPC分类号： B01D3/343 , B01D1/225 , Y10S203/22
摘要： A method is provided for preventing an easily polymerizable substance from being polymerized in a thin-film type evaporating device by supplying a solution of the substance to the evaporating heating surface of the device by the centrifugal force of a stirring rotary shaft, characterized by mixing a distilled vapor of the substance with a molecular oxygen-containing gas and supplying the extracted liquid or a solution having lower viscosity than the extracted liquid to a feed raw material inlet thereby adjusting the quantity of a wetting liquid per unit length of the surface in the range of 0.02-2 m3/mHr. In the evaporation of the substance by the use of the device, a method for preventing the substance from polymerization is provided.
摘要翻译：提供了一种通过利用搅拌旋转轴的离心力将物质溶液供给到该装置的蒸发加热面上来防止在薄膜型蒸发装置中聚合易于聚合的物质的方法，其特征在于将将具有分子含氧气体的物质的蒸馏蒸气，并将萃取的液体或具有比萃取液体的粘度低的溶液供给到进料原料入口，从而将表面的每单位长度的润湿液体的量调节在该范围内为0.02-2m 3 / mHr。在通过使用该装置的物质的蒸发中，提供了防止物质聚合的方法。

2. 发明授权

US06588450B2 Storage tank for viscous oil containing easily polymerizable compounds 有权
标题翻译：含有容易聚合的化合物的粘性油储罐
公开(公告)号：US06588450B2
公开(公告)日：2003-07-08
申请号：US09788598
申请日：2001-02-21
申请人： Yuichi Ijiri , Yukihiro Matsumoto , Sei Nakahara , Fumio Munechika
发明人： Yuichi Ijiri , Yukihiro Matsumoto , Sei Nakahara , Fumio Munechika
IPC分类号： F17D114
CPC分类号： B65D88/10 , Y10T137/8342 , Y10T137/85954
摘要： This invention relates to a storage tank for a viscous oil containing easily polymerizable compounds. The storage tank of the present invention for storing viscous oil containing easily polymerizable compounds comprises a bottom plate, a side wall, a draw-off pipe and an inlet pipe. The bottom plate slopes downwardly toward the draw-off pipe, and an angle of downward inclination of the bottom plate is a gradient of at least 1/200. It becomes possible because of the storage tank to effectively prevent polymerization of easily polymerizable compounds contained in waste oil within the storage tank, and clogging of a pipe is suppressed considerably.
摘要翻译：本发明涉及一种含有容易聚合的化合物的粘稠油储罐。用于储存容易聚合的化合物的粘性油的本发明的储罐包括底板，侧壁，抽出管和入口管。底板朝向排出管向下倾斜，底板的向下倾斜角度为至少1/200的坡度。由于储罐能够有效地防止储罐内的废油中容易聚合的化合物的聚合，因此可以大幅度地抑制管堵塞。

3. 发明申请

US20070003460A1 Reactor filled with solid particle and gas-phase catalytic oxidation with the reactor 有权
标题翻译：反应器用反应器填充固体颗粒和气相催化氧化
公开(公告)号：US20070003460A1
公开(公告)日：2007-01-04
申请号：US11498426
申请日：2006-08-03
申请人： Yukihiro Matsumoto , Takeshi Nishimura , Sei Nakahara , Naoto Kasaya
发明人： Yukihiro Matsumoto , Takeshi Nishimura , Sei Nakahara , Naoto Kasaya
IPC分类号： B01J8/04 , B01J8/08 , B01J10/00
CPC分类号： B01J8/067 , B01J8/001 , B01J2208/00044 , B01J2208/00061 , B01J2208/00212 , B01J2208/00513 , B01J2208/00539 , B01J2208/021 , B01J2208/025 , B01J2219/00777
摘要： A shell-and tube reactor including at least one reaction tube with a measuring means, substantially same solid particles being filled in the reaction tubes with or without the measuring means, a length of the filled solid particle layer, and a pressure drop thereof while passing a gas through the reaction tube, per each reaction tube, being substantially the same, respectively. By measuring the temperature of the catalyst particle layer, such a temperature as a representative can be gasped.
摘要翻译：包括具有测量装置的至少一个反应管的管壳式反应器，在具有或不具有测量装置的反应管中填充基本相同的固体颗粒，填充的固体颗粒层的长度及其通过时的压降通过反应管的每个反应管的气体分别基本相同。通过测量催化剂颗粒层的温度，可以将诸如代表性的温度气化。

4. 发明授权

US06525216B1 Method of manufacturing (meth)acrylic acid 有权
标题翻译：制造（甲基）丙烯酸的方法
公开(公告)号：US06525216B1
公开(公告)日：2003-02-25
申请号：US09588834
申请日：2000-06-07
申请人： Takeshi Nishimura , Yukihiro Matsumoto
发明人： Takeshi Nishimura , Yukihiro Matsumoto
IPC分类号： C07C5142
CPC分类号： C07C51/252 , B01D3/009 , B01D3/143 , B01D53/1487 , B01J2219/00006 , C07C51/44 , Y02P20/127 , C07C57/04
摘要： A method of manufacturing (meth)acrylic acid includes: a reaction step of carrying out a catalytic gas-phase oxidation reaction; an absorbing step of absorbing (meth)acrylic acid from a (meth)acrylic-acid-containing mixed gas prepared in the reaction step; a refinement step of separating, refining, and recovering (meth)acrylic acid from a (meth)acrylic-acid-containing liquid prepared in the absorbing step; and a recirculation step of recirculating (meth)acrylic acid contained in a vent gas produced in the refinement step to the absorbing step and/or the refinement step.
摘要翻译：制备（甲基）丙烯酸的方法包括：进行催化气相氧化反应的反应步骤;从（甲基）丙烯酸混合气体中吸收（甲基）丙烯酸的吸收步骤反应步骤;从在吸收步骤中制备的（甲基）丙烯酸的液体中分离，精制和回收（甲基）丙烯酸的精制步骤; 以及将在精炼步骤中产生的排气中包含的（甲基）丙烯酸再循环到吸收步骤和/或精制步骤的再循环步骤。

5. 发明授权

US06436245B1 Apparatus for the purification of organic compounds containing readily-blocking substances and process thereof 有权
标题翻译：用于纯化含有易阻塞物质的有机化合物的装置及其方法
公开(公告)号：US06436245B1
公开(公告)日：2002-08-20
申请号：US09585617
申请日：2000-06-02
申请人： Takeshi Nishimura , Yukihiro Matsumoto
发明人： Takeshi Nishimura , Yukihiro Matsumoto
IPC分类号： B01D320
CPC分类号： B01D3/225 , B01D3/22 , B01D3/24 , Y10S203/11 , Y10S203/22
摘要： A purification tower for purifying liquid by contacting the liquid with gas, the purification tower including: (a) a shell; and (b) a plurality of baffles, each of which is fixed to an internal surface of the shell, (i) said each baffle having a flat upper surface and a plurality of openings are formed in each of the baffle so that the liquid and the gas pass through the openings; (ii) any adjacent pair of the baffles are arranged so that a bottom of the shell is covered by the pair of the baffles viewing in an longitudinal direction of the shell. The present invention thus configured can provide a process and an apparatus for the purification of even an organic compound containing a readily-blocking substances, which are capable of continuously purifying such an organic substance over the long time without discontinuing operations.
摘要翻译： 1.一种用于通过使液体与气体接触来净化液体的净化塔，所述净化塔包括：（a）壳; 和（b）多个挡板，每个挡板固定在外壳的内表面上，（i）所述每个隔板具有平坦的上表面，并且在每个挡板中形成多个开口，使得液体和气体通过开口;（ii）任何相邻的挡板对被布置成使得壳体的底部被沿着壳体的纵向方向观察的一对挡板覆盖。由此构造的本发明可以提供一种方法和用于纯化甚至含有易阻塞物质的有机化合物的装置，其能够在不中断操作的情况下长时间地连续净化这种有机物质。

6. 发明授权

US07205429B2 Method for disposal of waste from acrylic acid process and acrylic ester process 有权
标题翻译：从丙烯酸工艺和丙烯酸酯工艺处理废物的方法
公开(公告)号：US07205429B2
公开(公告)日：2007-04-17
申请号：US10664237
申请日：2003-09-17
申请人： Yukihiro Matsumoto , Takeshi Nishimura , Kenji Sanada , Harunori Hirao
发明人： Yukihiro Matsumoto , Takeshi Nishimura , Kenji Sanada , Harunori Hirao
IPC分类号： C07C67/48 , C07C57/02
CPC分类号： C02F1/727 , B01D53/75 , C02F1/04 , C02F1/20 , C02F11/08 , C02F2103/18 , C07C67/08 , C07C69/54
摘要： This invention is providing a method for efficient treatment of the waste material from a process for production of acrylic acid and an acrylic ester. This is a method for the disposal of waste material, which at least one waste material selected from the group consisting of waste oil, waste water, and waste gas emitted from a process for production of acrylic acid is/are purified with at least one waste material selected from the group consisting of waste oil, waste water, and waste gas emitted from a process for production of an acrylic ester jointly. The efficiency of the treatment is enhanced by simultaneously treating the waste material.
摘要翻译：本发明提供了一种从丙烯酸和丙烯酸酯的生产方法对废料进行有效处理的方法。这是一种用于处理废物的方法，其中至少一种从由废油，废水和从生产丙烯酸的方法排出的废气中的废气中选出的废料被至少一种废物净化从由废丙烯酸酯的制造方法排出的废油，废水和废气组成的组中选择的材料。通过同时处理废料来提高处理效率。

7. 发明申请

US20060009655A1 Method for starting up reactor and reactor system 有权
标题翻译：启动反应堆和反应堆系统的方法
公开(公告)号：US20060009655A1
公开(公告)日：2006-01-12
申请号：US11221213
申请日：2005-09-07
申请人： Yukihiro Matsumoto , Takeshi Nishimura , Hideki Sogabe , Kazuhiko Sakamoto , Osamu Dodo
发明人： Yukihiro Matsumoto , Takeshi Nishimura , Hideki Sogabe , Kazuhiko Sakamoto , Osamu Dodo
IPC分类号： C07C51/16 , B01J10/00
CPC分类号： F28D7/0066 , B01J8/067 , B01J2208/00212 , B01J2208/00256 , B01J2208/00716 , B01J2219/00006 , C07C45/35 , C07C51/252 , C07C47/22 , C07C57/04
摘要： A method for quickly starting up a reactor and a reactor system therefor are provided. A shell-and-tube reactor in the system is adapted to circulate a heat medium having a solid point in the range of 50-250° C. to the outside of the reaction tubes and characterized by initiating temperature elevation of the reactor by introducing a gas of a temperature in the range of 100-400° C. to the reaction tubes' side and then circulating the heat medium in a heated state to the outside of the reaction tubes. By introducing a gas of an elevated temperature preparatorily to the reaction tubes, it is made possible to prevent the heat medium after circulation from being solidified again and enable the reactor to be quickly started up.
摘要翻译：提供了一种用于快速启动反应器及其反应器系统的方法。系统中的管壳式反应器适于将具有在50-250℃范围内的固点的热介质循环到反应管的外部，并且其特征在于通过引入反应器的温度升高将温度在100-400℃范围内的气体加到反应管侧，然后将加热的热介质循环到反应管的外部。通过将升温的气体预先引入反应管，可以防止循环后的热介质再次固化，使反应器快速启动。

8. 发明授权

US06888025B2 Method for absorbing acrylic acid and method for purifying acrylic acid 有权
标题翻译：丙烯酸的吸收方法和丙烯酸的净化方法
公开(公告)号：US06888025B2
公开(公告)日：2005-05-03
申请号：US10211040
申请日：2002-08-02
申请人： Harunori Hirao , Yoshitake Ishii , Yukihiro Matsumoto , Takeshi Nishimura
发明人： Harunori Hirao , Yoshitake Ishii , Yukihiro Matsumoto , Takeshi Nishimura
IPC分类号： C07C51/44 , C07C51/48 , C07C51/42
CPC分类号： C07C51/44 , B01D3/225 , C07C51/48 , C07C57/04
摘要： This invention concerns a method for absorbing acrylic acid, characterized by supplying an acrylic acid-containing reaction gas component obtained by the reaction of catalytic gas phase oxidation to an acrylic acid absorption column and advancing a high boiling inert hydrophobic organic liquid into counter-flow contact with said reaction gas in said acrylic acid absorption column with the mass flow rate of the organic liquid fixed in the range of 0.2-7.0 times the mass flow rate of the acrylic acid in the reaction gas thereby absorbing acrylic acid in said organic liquid and obtaining an acrylic acid-containing solution including a low boiling substance in the range of 0.7-7.5 wt % based on the weight of bottom liquid of absorption column.
摘要翻译：本发明涉及一种吸收丙烯酸的方法，其特征在于将通过催化气相氧化反应获得的含丙烯酸的反应气体组分供给丙烯酸吸收塔，并将高沸点惰性疏水性有机液体推入逆流接触所述丙烯酸吸收塔中的所述反应气体的有机液体的质量流量固定在反应气体中丙烯酸的质量流量的0.2-7.0倍的范围内，从而吸收所述有机液体中的丙烯酸，并获得含有丙烯酸的溶液，其包含基于吸收塔底液重量的0.7-7.5重量％的低沸点物质。

9. 发明授权

US06755943B1 Perforated tray without downcomer, perforated tray tower without downcomer 有权
标题翻译：穿孔托盘无降液管，多孔塔塔无降液管
公开(公告)号：US06755943B1
公开(公告)日：2004-06-29
申请号：US09506713
申请日：2000-02-18
申请人： Noriaki Mizutani , Takeshi Nishimura , Yukihiro Matsumoto
发明人： Noriaki Mizutani , Takeshi Nishimura , Yukihiro Matsumoto
IPC分类号： B01D332
CPC分类号： B01D3/225 , B01D3/22 , B01D3/324 , Y10S203/11 , Y10S203/22
摘要： A perforated tray without downcomer in accordance with the present invention satisfies following conditions: (a) The hole has a diameter of 10 mm to 25 mm. (b) Two adjacent holes are spaced by a distance of 1.2 d to 3 d, measured between the two centers. (c) The tray thickness is 2 mm to 8 mm. (d) The opening ratio is 10% to 30%. A perforated tray tower without downcomer fitted with two or more such perforated trays without downcomer in accordance with the present invention satisfies following conditions: (g) Perforated trays are spaced by a distance of 0.1 D to 0.5 D (D denotes the tower diameter). (h) The levelness of each perforated tray is 8 mm or less. (i) If a plurality of perforated trays are used at the same stage, the two most closely located holes that respectively belong to adjacent perforated trays are spaced by a distance of 50 mm to 150 mm, measured between the two centers. By using the perforated tray tower without downcomer, an easily polymerizable compound, such as an (meth)acrylic acid, or a liquid containing such an easily polymerizable compound can be distilled in a stable manner over an extended period of time with the formation of polymers being effectively prevented.
摘要翻译：根据本发明的无降液管的多孔板满足以下条件：（a）孔的直径为10mm〜25mm。（b）在两个中心之间测量，两个相邻的孔间隔1.2至3 d的距离。（c）托盘厚度为2mm至8mm。（d）开口率为10％〜30％。根据本发明的没有装有两个或更多个这样的没有降液管的多孔板的下降管的多孔塔塔塔满足以下条件：（g）穿孔托盘间隔0.1D至0.5D的距离（D表示塔架直径）。（h）每个多孔板的平整度为8mm或更小。（i）如果在相同的阶段使用多个多孔板，则分别属于相邻的多孔板的两个最接近定位的孔在两个中心之间测量的距离为50mm至150mm。通过使用没有降液管的多孔塔塔，可以在长时间内以稳定的方式蒸馏容易聚合的化合物如（甲基）丙烯酸或含有这种易聚合化合物的液体，同时形成聚合物有效防范。

10. 发明授权

US06566551B2 Method for preventing effluent gas pipe from blocking 有权
标题翻译：防止排气管阻塞的方法
公开(公告)号：US06566551B2
公开(公告)日：2003-05-20
申请号：US09724468
申请日：2000-11-29
申请人： Takeshi Nishimura , Yukihiro Matsumoto , Sei Nakahara , Misao Inada , Harunori Hirao , Mamoru Takamura
发明人： Takeshi Nishimura , Yukihiro Matsumoto , Sei Nakahara , Misao Inada , Harunori Hirao , Mamoru Takamura
IPC分类号： C07C5116
CPC分类号： C07C51/252 , C07C57/04
摘要： For use in a process for the production of (meth)acrylic acid comprising at least a step for the reaction of (meth)acrylic acid by catalytic gas phase oxidation and a step for the absorption thereof, a method for preventing an effluent gas pipe from blocking is disclosed, which method is characterized by causing part or the whole of the gas discharged from the step for absorption, while being circulated via the effluent gas pipe to the step for the reaction or being discarded, to be subjected to temperature elevation and application of pressure and/or mist separation. Particularly by setting the temperature of the waste gas from the absorption column at a level in the range of 30-70° C., it is made possible to decrease the contents of water, low boiling substances, and subliming substances entrained by the waste gas and, coupled with the temperature elevation and the application of pressure implemented in the effluent gas pipe, attain effective prevention of the interior of the effluent gas pipe from blockage and corrosion.
摘要翻译：为了用于生产（甲基）丙烯酸的方法，至少包括通过催化气相氧化反应（甲基）丙烯酸的步骤和用于吸收的步骤，用于防止流出气体管道的方法公开了这种方法，其特征在于，使得从步骤吸收的气体的一部分或全部通过废气管循环到用于反应或被丢弃的步骤中，以进行升温和施加的压力和/或雾分离。特别是通过将来自吸收塔的废气的温度设定在30〜70℃的范围内，能够降低水，低沸点物质和由废气夹带的升华物质的含量再加上在排气管道中实施的温度升高和施加压力，有效防止排气管内部堵塞和腐蚀。

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