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1. 发明申请

US20050258742A1 Carbene containing metal complexes as OLEDs 有权
标题翻译：含有碳的金属络合物作为OLED
公开(公告)号：US20050258742A1
公开(公告)日：2005-11-24
申请号：US11032739
申请日：2005-01-10
申请人： Yui-Yi Tsai , Michael Barone , Arnold Tamayo , Mark Thompson
发明人： Yui-Yi Tsai , Michael Barone , Arnold Tamayo , Mark Thompson
IPC分类号： C07F15/00 , H01J1/62 , H01J63/04 , H01L51/00 , H01L51/50
CPC分类号： H01L51/0085 , C07F15/0033 , C09B57/10 , H01L51/5016
摘要： A process for preparing a compound having the formula L2IrL′ is provided. The process comprises: combining and L′ in the presence of an organic solvent to form a mixture, wherein L is a suitable carbene ligand precursor coordinated to Ir; and L′ is a bidentate ligand or two monodentate ligands, and L is different from L′; Also provided is a process for preparing a compound having the formula The process comprises: (a) combining L, a carbene ligand precursor, with an organic solvent; (b) maintaining the mixture of step (a) at a temperature from about 175° C. to less than the boiling point of the organic solvent in (a). A process for preparing a compound with the formula L3Ir is also provided. This process comprises combining and L in the presence of alcohol and a base to form a mixture, wherein L is a bidentate ligand that may form a five-membered chelate ring.
摘要翻译：提供了具有式L 2 IrL'的化合物的制备方法。该方法包括：在有机溶剂存在下将L'结合形成混合物，其中L是与Ir配位的合适的卡宾配体前体; L'是二齿配体或两个单齿配体，L不同于L'; 还提供了制备具有下式的化合物的方法。该方法包括：（a）将L，卡宾配体前体与有机溶剂组合; （b）将步骤（a）的混合物保持在约175℃至低于（a）中的有机溶剂的沸点。还提供了制备具有式L 3 Ir的化合物的方法。该方法包括在醇和碱的存在下组合L并形成混合物，其中L是可形成五元螯合环的二齿配体。

2. 发明申请

US20050260447A1 Cyclometallated iridium carbene complexes for use as hosts 有权
标题翻译：用作主体的环金属铱卡宾配合物
公开(公告)号：US20050260447A1
公开(公告)日：2005-11-24
申请号：US11032836
申请日：2005-01-10
申请人： Jason Brooks , Xiao-Chang Li , Bert Alleyne , Mark Thompson , Peter Djurovich , Arnold Tamayo
发明人： Jason Brooks , Xiao-Chang Li , Bert Alleyne , Mark Thompson , Peter Djurovich , Arnold Tamayo
IPC分类号： C09K11/06 , C25B3/00 , H01L51/00 , H01L51/30 , H01L51/50 , H05B33/14
CPC分类号： H05B33/14 , C09K11/06 , C09K2211/1044 , C09K2211/185 , H01L51/0059 , H01L51/0078 , H01L51/0081 , H01L51/0085 , H01L51/5016
摘要： An organic light emitting device is provided. The device has an anode, a cathode and an organic layer disposed between the anode and the cathode. The organic layer comprises a host and a dopant, and the host comprises a compound having at least one carbene atom coordinated to iridium, and the compound has the structure:
摘要翻译：提供有机发光装置。该器件具有阳极，阴极和设置在阳极和阴极之间的有机层。有机层包括主体和掺杂剂，并且主体包含具有与铱配位的至少一个卡宾原子的化合物，该化合物具有以下结构：

3. 发明申请

US20060024526A1 Organic light emitting devices with electron blocking layers 有权
公开(公告)号：US20060024526A1
公开(公告)日：2006-02-02
申请号：US11230851
申请日：2005-09-19
申请人： Mark Thompson , Vadim Adamovich , Xiaofan Ren , Arnold Tamayo , Peter Djurovich
发明人： Mark Thompson , Vadim Adamovich , Xiaofan Ren , Arnold Tamayo , Peter Djurovich
IPC分类号： H05B33/12
CPC分类号： H01L51/0085 , C09K11/06 , C09K2211/1044 , C09K2211/185 , H01L51/0059 , H01L51/0062 , H01L51/0077 , H01L51/0081 , H01L51/0087 , H01L51/5096 , H01L2251/308 , H05B33/14 , Y10S428/917
摘要： The present invention relates to organic light emitting devices (OLEDs), and more specifically to efficient OLEDs having electron blocking layers. The devices of the present invention comprise at least one electron blocking layer which functions to confine electrons to specific regions of the light emitting devices. The present invention also relates to materials for use as electron blockers that show increased stability when incorporated into an organic light emitting device.

4. 发明申请

US20050260448A1 Novel organometallic compounds for use in electroluminescent devices 有权
标题翻译：用于电致发光器件的新型有机金属化合物
公开(公告)号：US20050260448A1
公开(公告)日：2005-11-24
申请号：US11032885
申请日：2005-01-10
申请人： Chun Lin , Jui-Yi Tsai , Jason Brooks , Bert Alleyne , Mark Thompson , Peter Djurovich , Arnold Tamayo , Tissa Sajoto , Robert Walters
发明人： Chun Lin , Jui-Yi Tsai , Jason Brooks , Bert Alleyne , Mark Thompson , Peter Djurovich , Arnold Tamayo , Tissa Sajoto , Robert Walters
IPC分类号： C09K11/06 , H01L51/00 , H01L51/50 , H05B33/14
CPC分类号： C09K11/06 , C09K2211/1044 , C09K2211/185 , H01L51/0059 , H01L51/0078 , H01L51/0081 , H01L51/0085 , H01L51/5016 , H05B33/14 , Y10S428/917
摘要： An organic light emitting device having an anode, a cathode and an organic layer between the anode and the cathode is provided. The organic layer comprises a carbene-metal complex having the structure: where R may be halo, hydrogen, alkyl, alkenyl, alkynyl, aralkyl, aryl, heteroaryl, substituted aryl, substituted heteroaryl, or a heterocyclic group; and additionally or alternatively, two or more R groups on the same ring form independently a 5 or 6-member cyclic group, which may be cycloalkyl, cycloheteroalkyl, aryl or heteroaryl; and which may be substituted by one or more substituents J; and J may be R′, CN, CF3, C(O)OR′, C(O)R′, C(O)NR′2, NR′2, NO2, OR′, SR′, SO2, SOR′, or SO3R′, and additionally or alternatively, two J groups on adjacent ring atoms form a fused 5- or 6-membered aromatic group; each R′ may be halo, H, alkyl, alkenyl, alkynyl, heteroalkyl, aralkyl, aryl and heteroaryl.
摘要翻译：提供了一种在阳极和阴极之间具有阳极，阴极和有机层的有机发光器件。有机层包含具有以下结构的卡宾金属络合物：其中R可以是卤素，氢，烷基，烯基，炔基，芳烷基，芳基，杂芳基，取代的芳基，取代的杂芳基或杂环基; 另外或替代地，相同环上的两个或更多个R基团独立地形成5或6元环基，其可以是环烷基，环杂烷基，芳基或杂芳基; 并且其可以被一个或多个取代基J取代; 并且J可以是R'，CN，CF 3，C（O）OR'，C（O）R'，C（O）NR'2，NR' 2'，2'，OR'，SR'，SO 2，SOR'或SO 3 R' ，另外或可选地，相邻环原子上的两个J基团形成稠合的5或6元芳族基团; 每个R'可以是卤素，H，烷基，烯基，炔基，杂烷基，芳烷基，芳基和杂芳基。

5. 发明申请

US20050260441A1 Luminescent compounds with carbene ligands 有权
标题翻译：具有卡宾配体的发光化合物
公开(公告)号：US20050260441A1
公开(公告)日：2005-11-24
申请号：US10849301
申请日：2004-05-18
申请人： Mark Thompson , Arnold Tamayo , Peter Djurovich , Tissa Sajoto
发明人： Mark Thompson , Arnold Tamayo , Peter Djurovich , Tissa Sajoto
IPC分类号： C07F15/00 , C09K11/06 , H01L51/00 , H01L51/50 , H05B33/14
CPC分类号： C09K11/06 , C07F15/0033 , C09K2211/1044 , C09K2211/1088 , C09K2211/1092 , C09K2211/185 , H01L51/0085 , H01L51/5016 , H05B33/14
摘要： An organic light emitting device is provided. The device has an anode, a cathode and an organic layer disposed between the anode and the cathode. The organic layer comprises a compound further comprising one or more carbene ligands coordinated to a metal center.
摘要翻译：提供有机发光装置。该器件具有阳极，阴极和设置在阳极和阴极之间的有机层。有机层包含进一步包含与金属中心配位的一个或多个卡宾配体的化合物。

6. 发明授权

US08007926B2 Luminescent compounds with carbene ligands 有权
标题翻译：具有卡宾配体的发光化合物
公开(公告)号：US08007926B2
公开(公告)日：2011-08-30
申请号：US12131458
申请日：2008-06-02
申请人： Mark E. Thompson , Arnold Tamayo , Peter Djurovich , Tissa Sajoto
发明人： Mark E. Thompson , Arnold Tamayo , Peter Djurovich , Tissa Sajoto
IPC分类号： H01L51/54 , C09K11/06
CPC分类号： C07F15/0086 , C07F15/0033 , C09K11/06 , C09K2211/1011 , C09K2211/1029 , C09K2211/1044 , C09K2211/1048 , C09K2211/1051 , C09K2211/1059 , C09K2211/1074 , C09K2211/1088 , C09K2211/1092 , C09K2211/1096 , C09K2211/185 , H01L51/0084 , H01L51/0085 , H01L51/0087 , H01L51/0088 , H01L51/5016 , H05B33/14 , Y10S428/917
摘要： An organic light emitting device is provided. The device has an anode, a cathode and an organic layer disposed between the anode and the cathode. The organic layer comprises a compound further comprising one or more carbene ligands coordinated to a metal center.
摘要翻译：提供有机发光装置。该器件具有阳极，阴极和设置在阳极和阴极之间的有机层。有机层包含进一步包含与金属中心配位的一个或多个卡宾配体的化合物。

7. 发明授权

US07393599B2 Luminescent compounds with carbene ligands 有权
标题翻译：具有卡宾配体的发光化合物
公开(公告)号：US07393599B2
公开(公告)日：2008-07-01
申请号：US10880384
申请日：2004-06-28
申请人： Mark E. Thompson , Arnold Tamayo , Peter Djurovich , Tissa Sajoto
发明人： Mark E. Thompson , Arnold Tamayo , Peter Djurovich , Tissa Sajoto
IPC分类号： H01L51/54 , C09K11/06
CPC分类号： C07F15/0086 , C07F15/0033 , C09K11/06 , C09K2211/1011 , C09K2211/1029 , C09K2211/1044 , C09K2211/1048 , C09K2211/1051 , C09K2211/1059 , C09K2211/1074 , C09K2211/1088 , C09K2211/1092 , C09K2211/1096 , C09K2211/185 , H01L51/0084 , H01L51/0085 , H01L51/0087 , H01L51/0088 , H01L51/5016 , H05B33/14 , Y10S428/917
摘要： An organic light emitting device is provided. The device has an anode, a cathode and an organic layer disposed between the anode and the cathode. The organic layer comprises a compound further comprising one or more carbene ligands coordinated to a metal center.
摘要翻译：提供有机发光装置。该器件具有阳极，阴极和设置在阳极和阴极之间的有机层。有机层包含进一步包含与金属中心配位的一个或多个卡宾配体的化合物。

8. 发明授权

US07989090B2 Near infrared emitting organic compounds and organic devices using the same 有权
标题翻译：近红外发射有机化合物和使用相同的有机器件
公开(公告)号：US07989090B2
公开(公告)日：2011-08-02
申请号：US12546829
申请日：2009-08-25
申请人： Mark E. Thompson , Carsten Borek , Kenneth Hanson , Peter Djurovich , Yiru Sun , Stephen Forrest , Arnold Tamayo
发明人： Mark E. Thompson , Carsten Borek , Kenneth Hanson , Peter Djurovich , Yiru Sun , Stephen Forrest , Arnold Tamayo
IPC分类号： H05B33/14 , H05B33/00
CPC分类号： C07F15/0033 , C09K11/06 , C09K2211/1029 , C09K2211/1033 , C09K2211/1044 , C09K2211/1074 , C09K2211/1088 , C09K2211/185 , H01L51/0037 , H01L51/0085 , H01L51/0087 , H01L51/5016 , H05B33/14 , Y10S428/917
摘要： Certain iridium compounds which may comprise an iridium(III)-ligand complex having the general formula: (C^N)2—Ir—(N^N). (C^N) and (N^N) may each represent a ligand coordinated to an iridium atom. The iridium compounds may have a primary phosphorescent photoluminescence peak wavelength in the near-infrared (IR) range. Also, organic devices that use certain iridium compounds. The organic device may comprise an organic layer and the organic layer may comprise any of the iridium compounds disclosed herein. Also, organic devices that use certain metalloporphyrin compounds. The metalloporphyrin compounds may comprise a core porphyrin structure with four pyrrole rings. The metalloporphyrin compounds may have a primary phosphorescent photoluminescence peak wavelength in the near-IR range.
摘要翻译：某些铱化合物，其可以包含具有以下通式的铱（III）配位络合物：（C 1 N）2-Ir-（N 2 N）。（C ^ N）和（N ^ N）可以各自表示与铱原子配位的配体。铱化合物可以在近红外（IR）范围内具有初级磷光光致发光峰值波长。而且，使用某些铱化合物的有机器件。有机装置可以包括有机层，并且有机层可以包含本文公开的任何铱化合物。而且，使用某些金属卟啉化合物的有机器件。金属卟啉化合物可以包含具有四个吡咯环的核心卟啉结构。金属卟啉化合物可以在近红外范围内具有初级磷光光致发光峰值波长。

9. 发明授权

US07956192B2 Carbene containing metal complexes as OLEDs 有权
标题翻译：含有碳的金属络合物作为OLED
公开(公告)号：US07956192B2
公开(公告)日：2011-06-07
申请号：US12543057
申请日：2009-08-18
申请人： Jui-Yi Tsai , Michael S. Barone , Arnold Tamayo , Mark E. Thompson
发明人： Jui-Yi Tsai , Michael S. Barone , Arnold Tamayo , Mark E. Thompson
IPC分类号： C07F15/00 , H01J1/62
CPC分类号： H01L51/0085 , C07F15/0033 , C09B57/10 , H01L51/5016
摘要： A process for preparing a compound having the formula L2IrL′ is provided. The process comprises:combining and L′ in the presence of an organic solvent to form a mixture, wherein L is a suitable carbene ligand precursor coordinated to Ir; and L′ is a bidentate ligand or two monodentate ligands, and L is different from L′; Also provided is a process for preparing a compound having the formula The process comprises: (a) combining L, a carbene ligand precursor, with an organic solvent; (b) maintaining the mixture of step (a) at a temperature from about 175° C. to less than the boiling point of the organic solvent in (a). A process for preparing a compound with the formula L3Ir is also provided. This process comprises combining and L in the presence of alcohol and a base to form a mixture, wherein L is a bidentate ligand that may form a five-membered chelate ring.
摘要翻译：提供了具有式L2IrL'的化合物的制备方法。该方法包括：在有机溶剂存在下将L'结合形成混合物，其中L是与Ir配位的合适的卡宾配体前体; L'是二齿配体或两个单齿配体，L不同于L'; 还提供了制备具有下式的化合物的方法。该方法包括：（a）将L，卡宾配体前体与有机溶剂组合; （b）将步骤（a）的混合物保持在约175℃至低于（a）中的有机溶剂的沸点。还提供了制备具有式L3Ir的化合物的方法。该方法包括在醇和碱的存在下组合L并形成混合物，其中L是可形成五元螯合环的二齿配体。

10. 发明授权

US07553557B2 Organic light emitting devices with electron blocking layers 有权
标题翻译：具有电子阻挡层的有机发光器件
公开(公告)号：US07553557B2
公开(公告)日：2009-06-30
申请号：US11230851
申请日：2005-09-19
申请人： Mark E. Thompson , Vadim Adamovich , Xiaofan Ren , Arnold Tamayo , Peter I. Djurovich
发明人： Mark E. Thompson , Vadim Adamovich , Xiaofan Ren , Arnold Tamayo , Peter I. Djurovich
IPC分类号： H01L51/54
CPC分类号： H01L51/0085 , C09K11/06 , C09K2211/1044 , C09K2211/185 , H01L51/0059 , H01L51/0062 , H01L51/0077 , H01L51/0081 , H01L51/0087 , H01L51/5096 , H01L2251/308 , H05B33/14 , Y10S428/917
摘要： The present invention relates to organic light emitting devices (OLEDs), and more specifically to efficient OLEDs having electron blocking layers. The devices of the present invention comprise at least one electron blocking layer which functions to confine electrons to specific regions of the light emitting devices. The present invention also relates to materials for use as electron blockers that show increased stability when incorporated into an organic light emitting device.
摘要翻译：本发明涉及有机发光器件（OLED），更具体地涉及具有电子阻挡层的高效OLED。本发明的器件包括至少一个电子阻挡层，其功能是将电子限制在发光器件的特定区域。本发明还涉及用作电子阻滞剂的材料，其在结合到有机发光器件中时显示出增加的稳定性。

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