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    • 1. 发明授权
    • Ink jet inks, inks, and other compositions containing colored pigments
    • 喷墨油墨,油墨和含有着色颜料的其它组合物
    • US06494943B1
    • 2002-12-17
    • US09698468
    • 2000-10-27
    • Yuan YuFriedrich K. von GottbergRobert M. AmiciPaul S. Palumbo
    • Yuan YuFriedrich K. von GottbergRobert M. AmiciPaul S. Palumbo
    • C09D1100
    • C09D11/34C09B67/0004C09B68/24C09D11/322
    • Colored pigments having one or more desired parameters and/or properties are described. These parameters and/or properties include: a) a particles size of from about 10 nm to about 300 nm; b) an accusizer number of less than 1010 particles/ml of dispersion at 15% solids which are greater than 0.5 micron; c) a filterability such that when in a liquid medium, 100 ml having 10% solids of the colored pigment filters through a 3 micron nylon absolute filter; d) a colored pigment purity of greater than about 80%, based on extractable material; and/or e) a stability such that the above-described properties do not change by more than 50% at 25 degrees C. for at least one week. Colored pigments having at least one organic group and having one or more of the above-described characteristics is also described as well as a process for preparing surface-modified colored pigments. The process involves combining at least one treating agent and at least one type of colored pigment(s) in a container to form a mixture and subjecting the mixture to high shearing and introducing at least one diazotizing agent to the mixture at least for a portion of time while the high shearing is taking place, and preferably during the entire time that high shearing is taking place, such that a reaction product is formed and contains surface-modified colored pigment(s).
    • 描述具有一个或多个所需参数和/或性质的有色颜料。 这些参数和/或性质包括:a)约10nm至约300nm的粒度; b)大于0.5微米的15%固体的小于1010个/ ml分散体的指示剂数; c)过滤性,使得当在液体介质中,具有10%固体的着色颜料的100ml通过3微米尼龙绝对过滤器过滤; d)基于可萃取材料的有色颜料纯度大于约80%; 和/或e)稳定性,使得上述性质在25摄氏度下不会改变超过50%至少一周。 还描述了具有至少一个有机基团并且具有一种或多种上述特征的着色颜料以及制备表面改性着色颜料的方法。 该方法包括将至少一种处理剂和至少一种类型的有色颜料混合在容器中以形成混合物,并使混合物经受高剪切,并将至少一种重氮化试剂至少引入至少一部分 并且优选在高剪切发生的整个时间内形成反应产物并含有表面改性的着色颜料。
    • 3. 发明授权
    • Ink jet inks, inks, and other compositions containing colored pigments
    • 喷墨油墨,油墨和含有着色颜料的其它组合物
    • US06506245B1
    • 2003-01-14
    • US09698328
    • 2000-10-27
    • Thomas A. KinneyFriedrich K. von GottbergYuan YuJohn F. Welch
    • Thomas A. KinneyFriedrich K. von GottbergYuan YuJohn F. Welch
    • C09B6700
    • C09D11/34C09B67/0004C09D11/037C09D11/322
    • Colored pigments having one or more desired parameters and/or properties are described. These parameters and/or properties include: a) a particles size of from about 10 nm to about 300 nm; b) an accusizer number of less than 1010 particles/ml of dispersion at 15% solids which are greater than 0.5 micron; c) a filterability such that when in a liquid medium, 100 ml having 10% solids of the colored pigment filters through a 3 micron nylon absolute filter; d) a colored pigment purity of greater than about 80%, based on extractable material; and/or e) a stability such that the above-described properties do not change by more than 50% at 25 degrees C for at least one week. Colored pigments having at least one organic group and having one or more of the above-described characteristics is also described as well as a process for preparing surface-modified colored pigments. The process involves combining at least one treating agent and at least one type of colored pigment(s) in a container to form a mixture and subjecting the mixture to high shearing and introducing at least one diazotizing agent to the mixture at least for a portion of time while the high shearing is taking place, and preferably during the entire time that high shearing is taking place, such that a reaction product is formed and contains surface-modified colored pigment(s).
    • 描述具有一个或多个所需参数和/或性质的有色颜料。 这些参数和/或性质包括:a)约10nm至约300nm的粒度; b)大于0.5微米的15%固体的小于1010个/ ml分散体的指示剂数; c)过滤性,使得当在液体介质中,具有10%固体的着色颜料的100ml通过3微米尼龙绝对过滤器过滤; d)基于可萃取材料的有色颜料纯度大于约80%; 和/或e)稳定性,使得上述性质在25℃下至少不超过50%变化至少一周。 还描述了具有至少一个有机基团并具有一种或多种上述特征的着色颜料以及制备表面改性着色颜料的方法。 该方法包括将至少一种处理剂和至少一种类型的有色颜料混合在容器中以形成混合物,并使混合物经受高剪切,并将至少一种重氮化试剂至少引入至少一部分 并且优选在高剪切发生的整个时间内形成反应产物并含有表面改性的着色颜料。
    • 4. 发明授权
    • Processes of purifying a dispersion and making inkjet inks
    • 纯化分散体和制备喷墨油墨的方法
    • US06328894B1
    • 2001-12-11
    • US09240291
    • 1999-01-29
    • Michael K. ChanJoseph E. JohnsonJohn MathewFriedrich K. von Gottberg
    • Michael K. ChanJoseph E. JohnsonJohn MathewFriedrich K. von Gottberg
    • B01D2126
    • C09D11/324Y10S516/921
    • A process to purify and classify a dispersion containing stabilized particles having counterions and ions as well as free species is disclosed. The solution may comprise an aqueous media, a solvent media, or a combination of both and can include more than one type of aqueous and/or solvent solutions. The process includes at least the steps, in any order, of substantially removing the particles having sizes above about 1 micron, preferably above 0.5 micron; substantially removing the free species; and exchanging at least a portion of the counterions that are a part of the stabilized particles. The process disclosed is especially useful in purifying dispersions where the ionic stabilized colloidal particles are carbon black having attached organic groups comprising at least one ionic group, or at least one ionizable group, or mixtures thereof.
    • 公开了一种纯化和分类含有具有抗衡离子和离子的稳定化颗粒以及游离物质的分散体的方法。 溶液可以包含水性介质,溶剂介质或两者的组合,并且可以包括多于一种类型的水和/或溶剂溶液。 该方法至少包括以任何顺序的基本上除去具有大于约1微米,优选高于0.5微米的尺寸的颗粒的步骤; 基本上除去游离物种; 并交换作为稳定化颗粒的一部分的至少一部分抗衡离子。 所公开的方法特别可用于纯化分散体,其中离子稳定化胶体颗粒是具有连接的包含至少一个离子基团的有机基团或至少一个可离子化基团的炭黑或其混合物。