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    • 1. 发明授权
    • Ink jet inks, inks, and other compositions containing colored pigments
    • 喷墨油墨,油墨和含有着色颜料的其它组合物
    • US06506245B1
    • 2003-01-14
    • US09698328
    • 2000-10-27
    • Thomas A. KinneyFriedrich K. von GottbergYuan YuJohn F. Welch
    • Thomas A. KinneyFriedrich K. von GottbergYuan YuJohn F. Welch
    • C09B6700
    • C09D11/34C09B67/0004C09D11/037C09D11/322
    • Colored pigments having one or more desired parameters and/or properties are described. These parameters and/or properties include: a) a particles size of from about 10 nm to about 300 nm; b) an accusizer number of less than 1010 particles/ml of dispersion at 15% solids which are greater than 0.5 micron; c) a filterability such that when in a liquid medium, 100 ml having 10% solids of the colored pigment filters through a 3 micron nylon absolute filter; d) a colored pigment purity of greater than about 80%, based on extractable material; and/or e) a stability such that the above-described properties do not change by more than 50% at 25 degrees C for at least one week. Colored pigments having at least one organic group and having one or more of the above-described characteristics is also described as well as a process for preparing surface-modified colored pigments. The process involves combining at least one treating agent and at least one type of colored pigment(s) in a container to form a mixture and subjecting the mixture to high shearing and introducing at least one diazotizing agent to the mixture at least for a portion of time while the high shearing is taking place, and preferably during the entire time that high shearing is taking place, such that a reaction product is formed and contains surface-modified colored pigment(s).
    • 描述具有一个或多个所需参数和/或性质的有色颜料。 这些参数和/或性质包括:a)约10nm至约300nm的粒度; b)大于0.5微米的15%固体的小于1010个/ ml分散体的指示剂数; c)过滤性,使得当在液体介质中,具有10%固体的着色颜料的100ml通过3微米尼龙绝对过滤器过滤; d)基于可萃取材料的有色颜料纯度大于约80%; 和/或e)稳定性,使得上述性质在25℃下至少不超过50%变化至少一周。 还描述了具有至少一个有机基团并具有一种或多种上述特征的着色颜料以及制备表面改性着色颜料的方法。 该方法包括将至少一种处理剂和至少一种类型的有色颜料混合在容器中以形成混合物,并使混合物经受高剪切,并将至少一种重氮化试剂至少引入至少一部分 并且优选在高剪切发生的整个时间内形成反应产物并含有表面改性的着色颜料。
    • 3. 发明授权
    • Liquid dyestuff compositions
    • 液体染料组合物
    • US06221113B1
    • 2001-04-24
    • US09006149
    • 1998-01-13
    • Jürgen Geiwiz
    • Jürgen Geiwiz
    • C09B6700
    • D21H21/28C09B67/0076Y10S8/919
    • A liquid dyestuff composition comprising from 4 to 50 wt % of a basic or cationic water soluble dyestuff, an organic or inorganic acid and 0.1 to 15.0 wt % of a phenolic derivative, the dyestuff having a solubility in water in the presence or absence of a phenolic derivative of at least 1 g/liter at a temperature of 25° C. and the composition being made up to 100 wt % by water and optionally a water-miscible solvent and/or a dissolving auxiliary; a process of dyeing a substrate like paper with such composition; a powder or granulate form of such composition and the use of such a composition or powder or granulate thereof in a dyeing process.
    • 一种液体染料组合物,其包含4至50重量%的碱性或阳离子水溶性染料,有机或无机酸和0.1至15.0重量%的酚衍生物,所述染料在有或没有 酚衍生物在25℃的温度下为至少1g / l,并​​且组合物由水和任选的水混溶性溶剂和/或溶解助剂构成至100重量%; 用这种组合物染色基材如纸的方法; 这种组合物的粉末或颗粒形式,以及这种组合物或粉末或其颗粒在染色过程中的用途。
    • 5. 发明授权
    • Granular compacts
    • 颗粒状压块
    • US06632255B2
    • 2003-10-14
    • US09932733
    • 2001-08-17
    • Walter DümlerPaolo Balliello
    • Walter DümlerPaolo Balliello
    • C09B6700
    • C09B67/0092C09B67/0072C09B67/0075C09B67/0094
    • The invention relates to the compacted granular products of a mixture of (A) at least one water-soluble dye, (B) at least one extender, and (C) at least one compound of formula:  wherein R is a saturated or unsaturated aliphatic residue with 12 to 22 carbon atoms, R1, R2, R3 and R4 independently of one another are each hydrogen or a residue of formula—(OCH2CH2)nH in which n is a number from 20 to 100, and B and B1 independently of one another are each C1-C4alkylene, and optionally (D) a dust-binding oil and/or (E) further additives, their production and their use.
    • 本发明涉及至少一种水溶性染料,(B)至少一种增量剂和(C)至少一种(A)的混合物的压实颗粒状产品。 式的化合物:其中R是具有12至22个碳原子的饱和或不饱和脂族残基,其中R > PDAT > 2 ,R 3 和R 4 彼此独立地为氢或 式的残基(OCH 2 CH 2 n 其中n为20至100的数,且彼此独立的 B和B 1 分别为C (D)粉尘结合油和/或其它添加剂,(P) 他们的生产和使用。
    • 8. 发明授权
    • Aqueous dispersions, their production and use
    • 水分散体,其生产和使用
    • US06736865B1
    • 2004-05-18
    • US09720065
    • 2000-12-18
    • Bernard DannerFrancis Palacin
    • Bernard DannerFrancis Palacin
    • C09B6700
    • D06P1/65162D06M7/00D06M13/02D06M15/21D06M15/227D06M15/263D06M15/285D06M2200/40D06P1/0036D06P1/5221D06P1/5242D06P1/525D06P1/5257
    • Aqueous dispersions (L) comprising: (a) a wax which is (a1) a carboxyl-containing hydrocarbon wax or a mixture of such waxes or a mixture of (a1) and (a2) at least one unmodified hydrocarbon wax, (b) a (co)poly(meth)acrylamide or (co)poly-(meth)acrylamide mixture which is (b1) at least one macro(co)poly-(meth)acrylamide, which optionally contains carboxyl-containing comonomers, having an average molecular weight {overscore (M)}W=n·106, where n≧10, or a mixture of (b1) and (b2) at least one (co)poly(meth)-acrylamide, which optionally contains carboxyl-containing comonomers, having an average molecular weight {overscore (M)}W
    • 水分散体(L),其包含:(a)蜡,其是(a1)含羧基的烃蜡或这种蜡的混合物或(a1)和(a2)的至少一种未改性烃蜡的混合物,(b) (共)聚(甲基)丙烯酰胺或(共)聚(甲基)丙烯酰胺混合物,其是(b1)至少一种宏(共)聚(甲基)丙烯酰胺,其任选地含有含羧基的共聚单体, 分子量(MW = n.10 <6>,其中n≥10,或(b1)和(b2)至少一种(共)聚(甲基)丙烯酰胺的混合物,其任选地含有含羧基 具有平均分子量(超过(MW <10.10 6)和(d)由两性,阴离子和/或非离子表面活性剂组成的分散剂体系的共聚单体令人惊奇地用作具有极高冲击效应的高效折痕标记抑制剂, 也适用于特别短的液体,例如在绞车和喷染机中。
    • 10. 发明授权
    • Process for preparing colored pigments
    • 制备有色颜料的方法
    • US06398858B1
    • 2002-06-04
    • US09517857
    • 2000-03-03
    • Yuan YuRonald J. GambaleRobert M. Amici
    • Yuan YuRonald J. GambaleRobert M. Amici
    • C09B6700
    • B82Y30/00C01P2004/50C01P2004/51C01P2004/62C01P2004/64C01P2004/80C01P2006/10C01P2006/12C01P2006/60C01P2006/80C09B67/0004C09C1/20C09C1/3669C09D11/322
    • The present invention relates to a process for preparing surface-modified colored pigments. The process includes the steps of: preparing a reaction batch comprising a treating agent and a diazotizing agent; adding a colored pigment to the batch; and mixing the colored pigment and the batch under high shear conditions to form a reaction product comprising a surface-modified colored pigment. The treating agent has an organic group which comprises at least one diazotizable group. In a preferred embodiment the diazotizable group comprises a) at least one aromatic group or at least one C1-C20 alkyl group, and b) at least one ionic group, ionizable group, nonionic group, or a mixture thereof. The surface-modified colored pigments prepared by the process of the present invention have been found useful in aqueous or solvent based compositions and particularly in ink jet ink compositions.
    • 本发明涉及一种制备表面改性着色颜料的方法。 该方法包括以下步骤:制备包含处理剂和重氮化试剂的反应批料; 向批料中加入有色颜料; 并在高剪切条件下混合着色颜料和批料以形成包含表面改性着色颜料的反应产物。 处理剂具有包含至少一个可重氮化基团的有机基团。 在优选的实施方案中,重氮化基团包括a)至少一个芳族基团或至少一个C 1 -C 20烷基,和b)至少一个离子基团,可离子基团,非离子基团或其混合物。 已经发现通过本发明的方法制备的表面改性的着色颜料可用于水性或溶剂基组合物,特别是在喷墨油墨组合物中。