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1. 发明授权

US07470348B2 Separator for producing aromatic carboxylic acids 有权
标题翻译：用于生产芳族羧酸的分离器
公开(公告)号：US07470348B2
公开(公告)日：2008-12-30
申请号：US10525971
申请日：2003-08-29
申请人： Yoshio Seiki , Kazuto Kobayashi , Yoshiyuki Takeuchi , Hiroyuki Osora , Keiichi Akimoto , Noritaka Matsumoto , Motoki Numata , Hiroaki Shimazu
发明人： Yoshio Seiki , Kazuto Kobayashi , Yoshiyuki Takeuchi , Hiroyuki Osora , Keiichi Akimoto , Noritaka Matsumoto , Motoki Numata , Hiroaki Shimazu
IPC分类号： B01D3/32 , B01D71/02
CPC分类号： B01J8/009 , B01D3/14 , B01D3/143 , B01D3/4205 , B01D53/268 , B01J2219/00006 , C07C51/265 , C07C51/44 , C07C51/47 , Y10S159/03 , Y10S159/27 , Y10S159/28 , C07C63/26
摘要： A separation system has a distillation column, an overhead vapor supply pipe connected to the top of the distillation column, first and second branch pipes branching from the overhead vapor supply pipe and a superheater connected to the first branch pipe. A separator downstream of the superheater has a separation membrane for separating overhead vapor from the top of the distillation column into permeable vapor and nonpermeable vapor by allowing only a selected portion of the overhead vapor to permeate the separation membrane. A reflux unit has a condenser connected to the second branch pipe for cooling a portion of the overhead vapor into a liquid and a gas-liquid separator for separating gas from the liquid produced by cooling and returning the separated liquid into the top of the distillation column.
摘要翻译：分离系统具有蒸馏塔，连接到蒸馏塔的顶部的塔顶蒸气供给管，从塔顶蒸气供应管分支的第一和第二分支管和连接到第一分支管的过热器。过热器下游的分离器具有分离膜，用于通过仅允许顶部蒸气的选定部分渗透到分离膜中，将塔顶蒸气从蒸馏塔的顶部分离成可渗透的蒸气和不可渗透的蒸汽。回流单元具有连接到第二分支管的冷凝器，用于将塔顶蒸气的一部分冷却成液体;以及气液分离器，用于从通过冷却产生的液体中分离气体，并将分离的液体返回到蒸馏塔的顶部。

2. 发明申请

US20070213557A1 Separator, reactor, and method for producing aromatic carboxylic acids 审中-公开
标题翻译：分离器，反应器及芳香族羧酸的制造方法
公开(公告)号：US20070213557A1
公开(公告)日：2007-09-13
申请号：US11797983
申请日：2007-05-09
申请人： Yoshio Seiki , Kazuto Kobayashi , Yoshiyuki Takeuchi , Hiroyuki Osora , Keiichi Akimoto , Noritaka Matsumoto , Motoki Numata , Hiroaki Shimazu
发明人： Yoshio Seiki , Kazuto Kobayashi , Yoshiyuki Takeuchi , Hiroyuki Osora , Keiichi Akimoto , Noritaka Matsumoto , Motoki Numata , Hiroaki Shimazu
IPC分类号： C07C51/16 , B01D1/28
CPC分类号： B01J8/009 , B01D3/14 , B01D3/143 , B01D3/4205 , B01D53/268 , B01J2219/00006 , C07C51/265 , C07C51/44 , C07C51/47 , Y10S159/03 , Y10S159/27 , Y10S159/28 , C07C63/26
摘要： In a process for producing an aromatic carboxylic acid, it is a dehydrating process which can achieve compactification of a step for removing water from a mixture of acetic acid and water produced in the production process, and which can reduce the consumed energy. In a production process of an aromatic carboxylic acid having an oxidation reaction step for producing a slurry of an aromatic carboxylic acid by carrying out liquid-phase oxidation reaction of an alkyl aromatic compound with an oxygen-containing gas in a solvent containing acetic acid in the presence of an oxidation catalyst, at least a portion of a mixture containing acetic acid and water produced in the production steps is separated into a permeable gas mainly comprising water and nonpermeable substances mainly comprising acetic acid, using a separation membrane having water selectivity.
摘要翻译：在芳香族羧酸的制造方法中，能够实现从生产过程中生成的乙酸和水的混合物中除去水分的步骤的压实，从而可以降低消耗能量的脱水方法。在具有氧化反应步骤的芳族羧酸的制造方法中，通过在含有乙酸的溶剂中进行烷基芳族化合物与含氧气体的液相氧化反应，生成芳香族羧酸的浆料存在氧化催化剂，使用具有水选择性的分离膜将至少一部分在制备步骤中生产的含有乙酸和水的混合物分离成主要包含水和主要包含乙酸的不渗透物质的渗透气体。

3. 发明申请

US20060014979A1 Process for producing terephthalic acid 审中-公开
标题翻译：对苯二甲酸生产方法
公开(公告)号：US20060014979A1
公开(公告)日：2006-01-19
申请号：US10534913
申请日：2003-11-14
申请人： Motoki Numata , Takayuki Isogai , Tomohiko Ogata
发明人： Motoki Numata , Takayuki Isogai , Tomohiko Ogata
IPC分类号： C07C63/26
CPC分类号： C07C51/43 , C07C63/26
摘要： In order to provide a method for producing a high-purity aromatic dicarboxylic acid such as terephthalic acid with high energy efficiency using a simplified process, in the method for producing terephthalic acid according to the present invention, solid-liquid separation and cleaning steps are carried out using a single device, and in a step for removing any liquid adhered to terephthalic cakes by evaporation, internal energy stored in the terephthalic acid cakes and/or the liquid adhered thereto is used at least part of the energy for evaporating the liquid adhered to the cakes.
摘要翻译：为了提供使用简单的方法以高能量生产高纯度芳族二羧酸如对苯二甲酸的方法，在根据本发明的对苯二甲酸的制造方法中，进行固液分离和清洗步骤在使用单一装置的情况下，在通过蒸发除去附着在对苯二甲酸饼上的任何液体的步骤中，存储在对苯二甲酸饼和/或粘附于其上的液体的内部能量被使用至少部分能量以蒸发粘附到蛋糕。

4. 发明授权

US5341577A Drying method of and drying apparatus for powder and granular material 失效
标题翻译：粉末和颗粒材料的干燥方法和干燥装置
公开(公告)号：US5341577A
公开(公告)日：1994-08-30
申请号：US94437
申请日：1993-07-21
申请人： Iori Hashimoto , Motoki Numata , Jun Nishizawa , Tomiyuki Kamada
发明人： Iori Hashimoto , Motoki Numata , Jun Nishizawa , Tomiyuki Kamada
IPC分类号： F26B17/00 , F26B3/00 , F26B11/02 , F26B21/10 , F26B23/02 , F26B25/22
CPC分类号： F26B11/028 , F26B23/02 , F26B25/22 , F26B3/00
摘要： Carbon black is introduced into a granulating machine 3 through an inlet 1 and water is introduced into the same through an inlet 2 to prepare granulated carbon black, which is fed to a cylindrical rotary type dryer 5 through a line 4 and is dried. A product of carbon black is discharged through a line 6. Temperature in the dryer 5 is measured by a plurality of thermometers 10. A combustion control device performs the arithmetical processing of temperature data to obtain the initial point at which the state of the carbon black is changed from the constant rate of drying to the falling rate of drying. The control device controls each flow rate of fuel supplied from each line 7 or 8 to burners 9 for the front and rear half portions of the dryer by using the critical point and the temperature of the carbon black at the outlet of the dryer, whereby a temperature profile for the carbon black in the dryer 5 can be made stable for a long time.
摘要翻译：将炭黑通过入口1引入造粒机3中，并通过入口2将水引入其中，以制备造粒炭黑，其通过管线4供给到圆筒形旋转式干燥器5中并干燥。炭黑的产物通过管线6排出。干燥机5中的温度由多个温度计10测量。燃烧控制装置进行温度数据的算术处理以获得碳黑状态的初始点从恒定的干燥速率变化到干燥的下降率。控制装置通过使用干燥器出口处的炭黑的临界点和温度来控制从每条管线7或8向干燥机的前半部分和后半部分的燃烧器9供应的燃料的每个流量，由此干燥机5中的炭黑的温度曲线可以长时间稳定。

5. 发明申请

US20090018361A1 PROCESS OF PRODUCING HIGH PURITY TEREPHTHALIC ACID 审中-公开
标题翻译：生产高纯度过敏酸的方法
公开(公告)号：US20090018361A1
公开(公告)日：2009-01-15
申请号：US11909369
申请日：2006-03-14
申请人： Motoki Numata , Isao Takahashi
发明人： Motoki Numata , Isao Takahashi
IPC分类号： C07C51/16
CPC分类号： C07C51/47 , C07C51/265 , C07C63/26 , C07C63/04
摘要： A problem of the invention is to provide a process of producing high purity terephthalic acid by selectively recovering p-toluic acid in wastewater which has hitherto been discarded and using it as a raw material of terephthalic acid.The invention is concerned with a process of producing high purity terephthalic acid, which is characterized in that a p-toluic acid recovery step of recovering p-toluic acid from a primary mother liquor and feeding it into an oxidation reaction step includes the following respective steps of: (I) an adsorption step of feeding, as a liquid to be treated, the primary mother liquor or a secondary mother liquor obtained by subjecting the primary mother liquor as cooled to solid-liquid separation into an adsorption tower filled with an adsorbing agent in which the breakthrough time of p-toluic acid is longer than the breakthrough time of benzoic acid to adsorb p-toluic acid and benzoic acid in the liquid to be treated to the adsorbing agent, (II) a feed stopping step of stopping the feed of the liquid to be treated into the adsorption tower at an arbitrary point of time of exceeding the breakthrough time of benzoic acid, (III) a desorption step of feeding a desorbing agent into the adsorption tower to desorb adsorbed p-toluic acid, and (IV) a circulation step of feeding p-toluic acid contained in the desorbing agent flown out from the adsorption tower into the oxidation reaction step.
摘要翻译：本发明的一个问题是提供一种通过选择性回收废弃物中的对甲苯甲酸来生产高纯度对苯二甲酸的方法，该方法迄今已被丢弃并将其用作对苯二甲酸的原料。本发明涉及生产高纯度对苯二甲酸的方法，其特征在于从初级母液中回收对甲苯甲酸并将其送入氧化反应步骤的对甲苯甲酸回收步骤包括以下各步骤（I）作为待处理液体的原料母液或二次母液进行吸附的吸附工序，所述初级母液或二次母液通过将初级母液冷却至固液分离得到填充有吸附剂的吸附塔其中对甲苯甲酸的突破时间长于苯甲酸在待处理液体中吸附对甲苯甲酸和苯甲酸至吸附剂的穿透时间，（II）停止进料的进料停止步骤在超过苯甲酸穿透时间的任意时间点待处理的液体进入吸附塔，（III）将解吸剂加入吸附剂的解吸步骤离子塔以脱附吸附的对甲苯甲酸，以及（IV）将从吸附塔出来的脱附剂中所含的对甲苯甲酸进料到氧化反应步骤的循环步骤。

6. 发明授权

US07140494B2 Centrifugal machine 有权
公开(公告)号：US07140494B2
公开(公告)日：2006-11-28
申请号：US10540472
申请日：2003-12-26
申请人： Koji Fujimoto , Atsushi Onodera , Jun Ohashi , Motoki Numata , Takayuki Isogai , Katsunori Fukuda
发明人： Koji Fujimoto , Atsushi Onodera , Jun Ohashi , Motoki Numata , Takayuki Isogai , Katsunori Fukuda
IPC分类号： B04B3/04 , B01D33/06 , B01D33/50
CPC分类号： B04B15/12 , B04B3/04
摘要： A screen bowl type centrifugal separator which can not only eliminate the problem of the productivity being lowered resulting from the occurrence of clogging with the crystals in the screen part, but also minimize the amount of leakage of the object to be treated in the screen part. Inside of the hub (41) of the screw conveyor (40), a cleaning liquid receiving part (43) which receives the cleaning liquid for the cleaning nozzle (45) is provided, and further, in the cleaning liquid receiving part (43), a residual layer crystal cleaning liquid receiving part (46) which receives the cleaning liquid for cleaning the residual layer object to be treated in the screen part (30) is provided, being partitioned independently of the inside of the cleaning liquid receiving part (43). The cleaning liquid which has been supplied to the inside of the residual layer crystal cleaning liquid receiving part (46) is jet spouted directly toward the residual layer object to be treated from the outer circumferential edge of the flight (42) through the residual layer crystal cleaning liquid path provided along the direction of the helix of the flight (42), with no relation to said cleaning liquid receiving part (43).

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