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1. 发明授权

US06174955B1 Water-based fluorine-containing paint 失效
标题翻译：水性含氟涂料
公开(公告)号：US06174955B1
公开(公告)日：2001-01-16
申请号：US09139272
申请日：1998-08-25
申请人： Yoshi Hirashima , Kazuhiko Maeda , Satoru Kobayashi , Kentaro Tsutsumi
发明人： Yoshi Hirashima , Kazuhiko Maeda , Satoru Kobayashi , Kentaro Tsutsumi
IPC分类号： C08L2712
CPC分类号： C09D127/12 , C08G18/6279 , C08G18/706 , C08G18/718 , C08L75/04 , C08L2666/28 , C08L2666/14
摘要： The invention provides a first water-based fluorine-containing paint including a water-based emulsion containing a fluorine-containing copolymer dispersed therein, and 1-50 parts by weight of a hardener per 100 parts by weight of the copolymer. The copolymer is prepared by copolymerizing 30-65 mol % of a fluoroolefin, 14-69 mol % of a copolymerizable vinyl-containing compound, and 1-30 mol % of a hydroxyl-containing compound and/or a polymerizable carboxyl-containing compound. The hardener is prepared by mixing 1 part by weight of a self-emulsifiable polyisocyanate with 0.01-1 part by weight of a compound containing in the molecule an oxyethylene unit and an alkoxysilyl group. When mixed with the emulsion, the hardener becomes well dispersed therein. The invention further provides a second water-based fluorine-containing paint including a water-based emulsion containing a fluorine-containing copolymer dispersed therein, and a hardener which is a compound containing in the molecule at least two hydrazino groups. The fluorine-containing copolymer is prepared by emulsion polymerization of 30-65 mol % of a fluoroolefin, 0.1-20 mol % of a polymerizable unsaturated carboxylic acid, 1-30 mol % of a polymerizable acetoacetylallyl compound, and 20-65 mol % of one of a vinyl ester and a vinyl ether. The second paint does not cure at ambient temperature, even after the hardener has been added thereto, and thus is usable as a one-package paint.
摘要翻译：本发明提供第一种水性含氟涂料，其包含含有分散在其中的含氟共聚物的水性乳液和每100份重量共聚物1-50份重量的硬化剂。该共聚物通过使30-65mol％的氟烯烃，14-69mol％的可共聚的含乙烯基化合物和1-30mol％的含羟基化合物和/或可聚合的含羧基化合物共聚而制备。通过将1重量份的自乳化多异氰酸酯与0.01-1重量份在分子中含有氧化乙烯单元和烷氧基甲硅烷基的化合物混合来制备固化剂。当与乳液混合时，固化剂变得很好地分散在其中。本发明还提供了包含分散在其中的含有含氟共聚物的水性乳液的第二水性含氟涂料，以及分子中含有至少两个肼基的化合物的固化剂。含氟共聚物通过30-65mol％的氟代烯烃，0.1-20mol％的可聚合不饱和羧酸，1-30mol％的可聚合乙酰乙烯基化合物和20-65mol％的可聚合乙酰乙烯基化合物的乳液聚合制备，乙烯基酯和乙烯基醚之一。第二种涂料即使在加入固化剂之后也不能在环境温度下固化，因此可用作单组分涂料。

2. 发明授权

US5856394A Water-based fluorine-containing paint 失效
标题翻译：水性含氟涂料
公开(公告)号：US5856394A
公开(公告)日：1999-01-05
申请号：US647853
申请日：1996-05-15
申请人： Yoshi Hirashima , Kazuhiko Maeda , Satoru Kobayashi , Kentaro Tsutsumi
发明人： Yoshi Hirashima , Kazuhiko Maeda , Satoru Kobayashi , Kentaro Tsutsumi
IPC分类号： C08G18/62 , C08G18/70 , C08G18/71 , C08L75/04 , C09D127/12 , C08L27/12
CPC分类号： C09D127/12 , C08G18/6279 , C08G18/706 , C08G18/718 , C08L75/04
摘要： The invention provides a first water-based fluorine-containing paint including a water-based emulsion containing a fluorine-containing copolymer dispersed therein, and 1-50 parts by weight of a hardener per 100 parts by weight of the copolymer. The copolymer is prepared by copolymerizing 30-65 mol % of a fluoroolefin, 14-69 mol % of a copolymerizable vinyl-containing compound, and 1-30 mol % of a hydroxyl-containing compound and/or a polymerizable carboxyl-containing compound. The hardener is prepared by mixing 1 part by weight of a self-emulsifiable polyisocyanate with 0.01-1 part by weight of a compound containing in the molecule an oxyethylene unit and an alkoxysilyl group. When mixed with the emulsion, the hardener becomes well dispersed therein. The invention further provides a second water-based fluorine-containing paint including a water-based emulsion containing a fluorine-containing copolymer dispersed therein, and a hardener which is a compound containing in the molecule at least two hydrazino groups. The fluorine-containing copolymer is prepared by emulsion polymerization of 30-65 mol % of a fluoroolefin, 0.1-20 mol % of a polymerizable unsaturated carboxylic acid, 1-30 mol % of a polymerizable acetoacetylallyl compound, and 20-65 mol % of one of a vinyl ester and a vinyl ether. The second paint does not cure at ambient temperature, even after the hardener has been added thereto, and thus is usable as a one-package paint.
摘要翻译：本发明提供第一种水性含氟涂料，其包含含有分散在其中的含氟共聚物的水性乳液和每100份重量共聚物1-50份重量的硬化剂。该共聚物通过使30-65mol％的氟烯烃，14-69mol％的可共聚的含乙烯基化合物和1-30mol％的含羟基化合物和/或可聚合的含羧基化合物共聚而制备。通过将1重量份自乳化多异氰酸酯与0.01-1重量份在分子中含有氧化乙烯单元和烷氧基甲硅烷基的化合物混合来制备固化剂。当与乳液混合时，固化剂变得很好地分散在其中。本发明还提供了包含分散在其中的含有含氟共聚物的水性乳液的第二水性含氟涂料，以及分子中含有至少两个肼基的化合物的固化剂。含氟共聚物通过30-65mol％的氟代烯烃，0.1-20mol％的可聚合不饱和羧酸，1-30mol％的可聚合乙酰乙烯基化合物和20-65mol％的可聚合乙酰乙烯基化合物的乳液聚合制备，乙烯基酯和乙烯基醚之一。第二种涂料即使在加入固化剂之后也不能在环境温度下固化，因此可用作单组分涂料。

3. 发明授权

US5859123A Water-based fluorine-containing emulsion 失效
标题翻译：水性含氟乳液
公开(公告)号：US5859123A
公开(公告)日：1999-01-12
申请号：US749698
申请日：1996-11-15
申请人： Satoru Kobayashi , Kazuhiko Maeda , Yoshi Hirashima , Seiji Hasegawa , Kentaro Tsutsumi
发明人： Satoru Kobayashi , Kazuhiko Maeda , Yoshi Hirashima , Seiji Hasegawa , Kentaro Tsutsumi
IPC分类号： C08F214/18 , C08F214/24 , C08F214/26 , C09D143/04 , C08L27/12
CPC分类号： C08F214/18 , C08F214/245 , C08F214/265 , C09D143/04 , C08L2201/52
摘要： The present invention relates to a water-based fluorine-containing emulsion. This emulsion contains a fluorine-containing copolymer in a disperse phase thereof This copolymer is prepared by copolymerizing: (A) a fluoroolefin, (B) an organosilicon compound containing an olefinic unsaturated bond and an alkoxysilyl group, (C) an unsaturated carboxylic acid represented by a general formula of CH.sub.2 .dbd.CH--(CH.sub.2).sub.n --COOH where n is an integer of from 3 to 15, and (D) at least one other copolymerizable monomer. A paint prepared from the emulsion is superior in storage stability and mechanical stability, although this paint belongs to a one-package paint. A coated film formed by applying the paint is superior in water resistance in its early stages, stain resistance, and weather resistance.
摘要翻译：本发明涉及水性含氟乳液。该乳液在分散相中含有含氟共聚物。该共聚物通过共聚以下物质制备：（A）氟烯烃，（B）含有烯属不饱和键的有机硅化合物和烷氧基甲硅烷基，（C）不饱和羧酸通式为CH 2 = CH-（CH 2）n -COOH，其中n为3至15的整数，和（D）至少一种其它可共聚单体。由乳液制备的油漆在储存稳定性和机械稳定性方面是优异的，尽管这种油漆属于单组分涂料。通过涂覆涂料形成的涂膜在其早期的耐水性，耐污染性和耐候性方面都是优异的。

4. 发明授权

US07781602B2 Fluorinated cyclic compound, polymerizable fluoromonomer, fluoropolymer, resist material comprising the same, and method of forming pattern with the same 有权
标题翻译：含氟环状化合物，可聚合的含氟单体，含氟聚合物，包含它们的抗蚀剂材料，以及与其形成图案的方法
公开(公告)号：US07781602B2
公开(公告)日：2010-08-24
申请号：US11941433
申请日：2007-11-16
申请人： Haruhiko Komoriya , Shinichi Sumida , Katsunori Kawamura , Satoru Kobayashi , Satoru Miyazawa , Kazuhiko Maeda
发明人： Haruhiko Komoriya , Shinichi Sumida , Katsunori Kawamura , Satoru Kobayashi , Satoru Miyazawa , Kazuhiko Maeda
IPC分类号： C07D313/00 , C08F214/26 , C08F18/20
CPC分类号： G03F7/0397 , C07D307/93 , G03F7/0046 , G03F7/0392
摘要： The present invention relates to a novel fluorine-containing cyclic compound that is derived from a norbornadiene and hexafluoroacetone and has an oxacyclopentane structure. This compound may be represented by the following formula (1) or (2). Furthermore, the present invention relates to a fluorine-containing polymer compound prepared by a polymerization or copolymerization using this fluorine-containing cyclic compound or its derivative. By using such fluorine-containing polymer compound, it is possible to provide a superior resist material and a fine pattern forming process using the same.
摘要翻译：本发明涉及一种衍生自降冰片二烯和六氟丙酮并具有氧环戊烷结构的新型含氟环状化合物。该化合物可以由下式（1）或（2）表示。此外，本发明涉及通过使用该含氟环状化合物或其衍生物的聚合或共聚制备的含氟聚合物。通过使用这样的含氟聚合物化合物，可以提供优异的抗蚀剂材料和使用其的精细图案形成方法。

5. 发明申请

US20090272295A1 Coating Materials Consisting of Low- or Medium-Molecular Organic Compounds 有权
标题翻译：包含低分子或中等分子有机化合物的涂料
公开(公告)号：US20090272295A1
公开(公告)日：2009-11-05
申请号：US12088455
申请日：2006-09-05
申请人： Satoru Miyazawa , Satoru Kobayashi , Kazuhiko Maeda
发明人： Satoru Miyazawa , Satoru Kobayashi , Kazuhiko Maeda
IPC分类号： C09D5/00 , C07D407/12 , C07C69/757
CPC分类号： C09D4/00 , G03F7/0046 , G03F7/0397 , G03F7/091 , Y10S430/106 , Y10S430/109
摘要： A coating material including a low-molecular or medium-molecular organic compound represented by general formula (1). (In the formula, R1 is a single bond, methylene, ethylene or oxygen; and R2 is a hydrogen atom, or a hydrocarbon group, a fluorine-containing alkyl group, a cyclic form containing an aromatic group or aliphatic group, which may contain hydroxy group, carboxyl group, amino group, amide group, imide group, glycidyl group, cyano group, fluorocarbinol group, sulfonic group or sulfonylamide group, and a complex thereof, and may contain a fluorine atom, oxygen atom, nitrogen atom, silicon atom or sulfur atom, and R2's of the same type or different type may be connected by an ester bond, amide bond, ether bond, thioether bond, thioester bond or urethane bond.). This compound can be derived from a diol compound and bicyclo[2.2.2]octane-2,3:5,6-tetracarboxylic anhydride.
摘要翻译：一种包含由通式（1）表示的低分子或中分子有机化合物的涂料。（式中，R 1为单键，亚甲基，亚乙基或氧，R 2为氢原子或烃基，含氟烷基，含有芳香族基团或脂肪族基团的环状，可以含有羟基，羧基，氨基，酰胺基，酰亚胺基，缩水甘油基，氰基，氟代甲醇基，磺基或磺酰胺基及其配合物，可以含有氟原子，氧原子，氮原子，硅原子或硫原子，并且相同类型或不同类型的R 2可以通过酯键，酰胺键，醚键，硫醚键，硫酯键或氨基甲酸酯键连接）。该化合物可以衍生自二醇化合物和二环[2.2.2]辛烷-2,3：5,6-四羧酸酐。

6. 发明申请

US20080050674A1 Polyester compound and resist material using the same 有权
标题翻译：聚酯化合物和使用其的抗蚀剂材料
公开(公告)号：US20080050674A1
公开(公告)日：2008-02-28
申请号：US11509638
申请日：2006-08-25
申请人： Satoru Miyazawa , Satoru Kobayashi , Kazuhiko Maeda
发明人： Satoru Miyazawa , Satoru Kobayashi , Kazuhiko Maeda
IPC分类号： G03C1/00 , C08G63/16
CPC分类号： G03F7/0395 , C08G63/199 , G03F7/0046 , G03F7/11 , G03F7/2041 , Y10S430/109
摘要： There is provided a novel polyester compound having in its main polymer chain an aliphatic cyclic structure with carboxylic acids or carboxylic acid ester groups as represented by the chemical formula (1), a resist material containing the polyester compound and a patterning method using the resist material.
摘要翻译：提供了一种新颖的聚酯化合物，其主要聚合物链具有由化学式（1）表示的具有羧酸或羧酸酯基的脂族环状结构，含有聚酯化合物的抗蚀剂材料和使用抗蚀剂材料的图案化方法。

7. 发明申请

US20050171375A1 Process for producing acrylic ester compound 有权
标题翻译：制备丙烯酸酯化合物的方法
公开(公告)号：US20050171375A1
公开(公告)日：2005-08-04
申请号：US10995334
申请日：2004-11-24
申请人： Satoru Miyazawa , Yusuke Kuramoto , Satoru Kobayashi , Kazuhiko Maeda
发明人： Satoru Miyazawa , Yusuke Kuramoto , Satoru Kobayashi , Kazuhiko Maeda
IPC分类号： C07C67/14 , C07C69/653 , C07C69/62
CPC分类号： C07C67/14 , C07C69/653
摘要： A process for producing an acrylic ester compound includes reacting in the presence of alkene an alcohol represented by the formula (1), wherein R1 represents a hydrogen atom, a fluorine atom, a straight-chain or branched hydrocarbon group, a fluorine-containing alkyl group, or an aromatic or aliphatic ring and optionally contains oxygen, sulfur or a carbonyl bond, with an acid halide represented by the formula (2), wherein R2 represents a hydrogen atom, a halogen atom, a hydrocarbon group, or a fluorine-containing alkyl group, and X represents a halogen atom.
摘要翻译：丙烯酸酯化合物的制造方法包括在烯烃存在下使式（1）表示的醇反应，其中R 1表示氢原子，氟原子，直链或支链烃基，含氟烷基或芳族或脂族环，并且任选地含有氧，硫或羰基键，与式（2）表示的酰基卤，其中R 2表示氢原子，卤素原子，烃基或含氟烷基，X表示卤素原子。

8. 发明授权

US07919224B2 Coating materials consisting of low- or medium-molecular organic compounds 有权
标题翻译：涂料由低分子或中等分子量的有机化合物组成
公开(公告)号：US07919224B2
公开(公告)日：2011-04-05
申请号：US12088455
申请日：2006-09-05
申请人： Satoru Miyazawa , Satoru Kobayashi , Kazuhiko Maeda
发明人： Satoru Miyazawa , Satoru Kobayashi , Kazuhiko Maeda
IPC分类号： G03F7/00 , G03F7/032 , C08G63/02
CPC分类号： C09D4/00 , G03F7/0046 , G03F7/0397 , G03F7/091 , Y10S430/106 , Y10S430/109
摘要： A coating material including a low-molecular or medium-molecular organic compound represented by general formula (1). (In the formula, R1 is a single bond, methylene, ethylene or oxygen; and R2 is a hydrogen atom, or a hydrocarbon group, a fluorine-containing alkyl group, a cyclic form containing an aromatic group or aliphatic group, which may contain hydroxy group, carboxyl group, amino group, amide group, imide group, glycidyl group, cyano group, fluorocarbinol group, sulfonic group or sulfonylamide group, and a complex thereof, and may contain a fluorine atom, oxygen atom, nitrogen atom, silicon atom or sulfur atom, and R2's of the same type or different type may be connected by an ester bond, amide bond, ether bond, thioether bond, thioester bond or urethane bond.). This compound can be derived from a diol compound and bicyclo[2.2.2]octane-2,3:5,6-tetracarboxylic anhydride.
摘要翻译：一种包含由通式（1）表示的低分子或中分子有机化合物的涂料。（式中，R 1为单键，亚甲基，亚乙基或氧，R 2为氢原子或烃基，含氟烷基，含有芳香族基团或脂肪族基团的环状，可以含有羟基，羧基，氨基，酰胺基，酰亚胺基，缩水甘油基，氰基，氟代甲醇基，磺基或磺酰胺基及其配合物，可以含有氟原子，氧原子，氮原子，硅原子或硫原子，并且相同类型或不同类型的R 2可以通过酯键，酰胺键，醚键，硫醚键，硫酯键或氨基甲酸酯键连接）。该化合物可以衍生自二醇化合物和二环[2.2.2]辛烷-2,3：5,6-四羧酸酐。

9. 发明授权

US07517635B2 Polyester compound and resist material using the same 有权
标题翻译：聚酯化合物和使用其的抗蚀剂材料
公开(公告)号：US07517635B2
公开(公告)日：2009-04-14
申请号：US11509638
申请日：2006-08-25
申请人： Satoru Miyazawa , Satoru Kobayashi , Kazuhiko Maeda
发明人： Satoru Miyazawa , Satoru Kobayashi , Kazuhiko Maeda
IPC分类号： G03C1/73 , G03F7/039 , G03F7/038 , G03F7/09 , C08G63/137
CPC分类号： G03F7/0395 , C08G63/199 , G03F7/0046 , G03F7/11 , G03F7/2041 , Y10S430/109
摘要： There is provided a novel polyester compound having in its main polymer chain an aliphatic cyclic structure with carboxylic acids or carboxylic acid ester groups as represented by the chemical formula (1), a resist material containing the polyester compound and a patterning method using the resist material.
摘要翻译：提供了一种新颖的聚酯化合物，其主要聚合物链具有由化学式（1）表示的具有羧酸或羧酸酯基的脂族环状结构，含有聚酯化合物的抗蚀剂材料和使用抗蚀剂材料的图案化方法。

10. 发明授权

US07399815B2 Fluorine-containing allyl ether compounds, their copolymers, and resist compositions and anti-reflection film materials using such copolymers 有权
标题翻译：含氟烯丙基醚化合物，它们的共聚物和抗蚀剂组合物以及使用这种共聚物的抗反射膜材料
公开(公告)号：US07399815B2
公开(公告)日：2008-07-15
申请号：US11492056
申请日：2006-07-25
申请人： Satoru Kobayashi , Katsunori Kawamura , Kazuhiro Yamanaka , Haruhiko Komoriya , Kazuhiko Maeda
发明人： Satoru Kobayashi , Katsunori Kawamura , Kazuhiro Yamanaka , Haruhiko Komoriya , Kazuhiko Maeda
IPC分类号： C08F18/20
CPC分类号： G03F7/0397 , C07C43/1781 , C07C43/192 , C07C2601/14 , C07C2603/68 , C08F16/24 , G03F7/0046 , G03F7/091 , Y10S430/108
摘要： The invention relates to a fluorine-containing allyl ether compound represented by the formula 1, wherein R represents an organic group containing at least one fluorine atom and an alicyclic structure. The invention further relates to a fluorine-containing copolymer containing a first unit derived from the fluorine-containing allyl ether represented by the formula 1; and a second unit derived from a vinyl monomer.
摘要翻译：本发明涉及由式1表示的含氟烯丙基醚化合物，其中R表示含有至少一个氟原子和脂环结构的有机基团。本发明还涉及含有由式1表示的含氟烯丙基醚衍生的第一单元的含氟共聚物; 和衍生自乙烯基单体的第二单元。

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