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1. 发明授权

US06992144B2 Water-absorbent agent, method for production thereof, and water-absorbent composition 失效
标题翻译：吸水剂，其制造方法和吸水性组合物
公开(公告)号：US06992144B2
公开(公告)日：2006-01-31
申请号：US10229111
申请日：2002-08-28
申请人： Yorimichi Dairoku , Kinya Nagasuna , Yoshihiko Masuda , Nobuyuki Harada , Yoshihiro Motono , Kunihiko Ishizaki
发明人： Yorimichi Dairoku , Kinya Nagasuna , Yoshihiko Masuda , Nobuyuki Harada , Yoshihiro Motono , Kunihiko Ishizaki
IPC分类号： C08F8/32
CPC分类号： C08J3/245 , A61L15/24 , A61L15/60 , C08F220/06 , C08J2300/14 , C08L33/02
摘要： A method for the production of a water-absorbent agent comprises mixing an absorbent resin containing a carboxyl group with an additive soluble in the aqueous solution of at least one member selected from the group consisting of inorganic acids, organic acids, and polyamino acids and a cross-linking agent capable of reacting with the carboxyl group. A water-absorbent agent obtained by adding from 0.005 to 8 parts by weight of an epoxy compound to 100 parts by weight of a water-absorbent resin, exhibiting an absorption capacity without load of at least 45 (g/g), an absorption capacity under load of 20 g/cm2 of not less than 30 (ml/g) and having a residue amount of an epoxy compound of not more than 2 ppm. A water-absorbent composition comprises a polyamino acid (salt) and a water-absorbent resin containing a carboxyl group.
摘要翻译：制造吸水剂的方法包括将含羧基的吸收性树脂与可溶于选自无机酸，有机酸和聚氨基酸中的至少一种的水溶液中的添加剂混合，以及能够与羧基反应的交联剂。通过将0.005〜8重量份的环氧化合物与100重量份的吸水性树脂相加而获得的吸水剂，其表现出无负载的吸收能力为至少45（g / g），吸收能力在20g / cm 2以下的负载不小于30（ml / g），残留量为不大于2ppm的环氧化合物。吸水性组合物包含聚氨基酸（盐）和含有羧基的吸水性树脂。

2. 发明授权

US07250459B2 Absorbent resin composition 有权
标题翻译：吸收性树脂组合物
公开(公告)号：US07250459B2
公开(公告)日：2007-07-31
申请号：US11228332
申请日：2005-09-19
申请人： Yorimichi Dairoku , Kinya Nagasuna , Yoshihiko Masuda , Nobuyuki Harada , Yoshihiro Motono , Kunihiko Ishizaki
发明人： Yorimichi Dairoku , Kinya Nagasuna , Yoshihiko Masuda , Nobuyuki Harada , Yoshihiro Motono , Kunihiko Ishizaki
IPC分类号： C08K5/09
CPC分类号： C08J3/245 , A61L15/24 , A61L15/60 , C08F220/06 , C08J2300/14 , C08L33/02
摘要： A method for the production of a water-absorbent agent comprises mixing an absorbent resin containing a carboxyl group with an additive soluble in the aqueous solution of at least one member selected from the group consisting of inorganic acids, organic acids, and polyamino acids and a cross-linking agent capable of reacting with the carboxyl group. A water-absorbent agent obtained by adding from 0.005 to 8 parts by weight of an epoxy compound to 100 parts by weight of a water-absorbent resin, exhibiting an absorption capacity without load of at least 45 (g/g), an absorption capacity under load of 20 g/cm2 of not less than 30 (ml/g) and having a residue amount of an epoxy compound of not more than 2 ppm. A water-absorbent composition comprises a polyamino acid (salt) and a water-absorbent resin containing a carboxyl group.
摘要翻译：制造吸水剂的方法包括将含羧基的吸收性树脂与可溶于选自无机酸，有机酸和聚氨基酸中的至少一种的水溶液中的添加剂混合，以及能够与羧基反应的交联剂。通过将0.005〜8重量份的环氧化合物与100重量份的吸水性树脂相加而获得的吸水剂，其表现出无负载的吸收能力为至少45（g / g），吸收能力在20g / cm 2以下的负载不小于30（ml / g），残留量为不大于2ppm的环氧化合物。吸水性组合物包含聚氨基酸（盐）和含有羧基的吸水性树脂。

3. 发明申请

US20060025536A1 Absorbent resin composition 有权
标题翻译：吸收性树脂组合物
公开(公告)号：US20060025536A1
公开(公告)日：2006-02-02
申请号：US11228332
申请日：2005-09-19
申请人： Yorimichi Dairoku , Kinya Nagasuna , Yoshihiko Masuda , Nobuyuki Harada , Yoshihiro Motono , Kunihiko Ishizaki
发明人： Yorimichi Dairoku , Kinya Nagasuna , Yoshihiko Masuda , Nobuyuki Harada , Yoshihiro Motono , Kunihiko Ishizaki
IPC分类号： C08F120/02 , C08F120/62
CPC分类号： C08J3/245 , A61L15/24 , A61L15/60 , C08F220/06 , C08J2300/14 , C08L33/02
摘要： A method for the production of a water-absorbent agent comprises mixing an absorbent resin containing a carboxyl group with an additive soluble in the aqueous solution of at least one member selected from the group consisting of inorganic acids, organic acids, and polyamino acids and a cross-linking agent capable of reacting with the carboxyl group. A water-absorbent agent obtained by adding from 0.005 to 8 parts by weight of an epoxy compound to 100 parts by weight of a water-absorbent resin, exhibiting an absorption capacity without load of at least 45 (g/g), an absorption capacity under load of 20 g/cm2 of not less than 30 (ml/g) and having a residue amount of an epoxy compound of not more than 2 ppm. A water-absorbent composition comprises a polyamino acid (salt) and a water-absorbent resin containing a carboxyl group.
摘要翻译：制造吸水剂的方法包括将含羧基的吸收性树脂与可溶于选自无机酸，有机酸和聚氨基酸中的至少一种的水溶液中的添加剂混合，以及能够与羧基反应的交联剂。通过将0.005〜8重量份的环氧化合物与100重量份的吸水性树脂相加而获得的吸水剂，其表现出无负载的吸收能力为至少45（g / g），吸收能力在20g / cm 2以下的负载不小于30（ml / g），残留量为不大于2ppm的环氧化合物。吸水性组合物包含聚氨基酸（盐）和含有羧基的吸水性树脂。

4. 发明授权

US5610208A Water-absorbent agent, method for production thereof, and water-absorbent composition 失效
标题翻译：吸水剂，其制造方法和吸水性组合物
公开(公告)号：US5610208A
公开(公告)日：1997-03-11
申请号：US388838
申请日：1995-02-15
申请人： Yorimichi Dairoku , Kinya Nagasuna , Yoshihiko Masuda , Nobuyuki Harada , Yoshihiro Motono , Kunihiko Ishizaki
发明人： Yorimichi Dairoku , Kinya Nagasuna , Yoshihiko Masuda , Nobuyuki Harada , Yoshihiro Motono , Kunihiko Ishizaki
IPC分类号： A61L15/24 , A61L15/60 , C08J3/24 , C08F8/14
CPC分类号： C08J3/245 , A61L15/24 , A61L15/60 , C08F220/06 , C08J2300/14
摘要： A method for the production of a water-absorbent agent comprises mixing an absorbent resin containing a carboxyl group with an additive soluble in the aqueous solution of at least one member selected from the group consisting of inorganic acids, organic acids, and polyamino acids and a cross-linking agent capable of reacting with the carboxyl group. A water-absorbent agent obtained by adding from 0.005 to 8 parts by weight of an epoxy compound to 100 parts by weight of a water-absorbent resin, exhibiting an absorption capacity without load of at least 45 (g/g), an absorption capacity under load of 20 g/cm.sup.2 of not less than 30 (ml/g) and having a residue amount of an epoxy compound of not more than 2 ppm. A water-absorbent composition comprises a polyamino acid (salt) and a water-absorbent resin containing a carboxyl group.
摘要翻译：制造吸水剂的方法包括将含羧基的吸收性树脂与可溶于选自无机酸，有机酸和聚氨基酸中的至少一种的水溶液中的添加剂混合，以及能够与羧基反应的交联剂。通过将0.005〜8重量份的环氧化合物与100重量份的吸水性树脂相加而获得的吸水剂，其表现出无负载的吸收能力为至少45（g / g），吸收能力负荷为20g / cm 2以下，不低于30（ml / g），残留量不超过2ppm的环氧化合物。吸水性组合物包含聚氨基酸（盐）和含有羧基的吸水性树脂。

5. 发明授权

US06107358A Water-absorbent resin and method for production thereof 失效
标题翻译：吸水性树脂及其制造方法
公开(公告)号：US06107358A
公开(公告)日：2000-08-22
申请号：US915557
申请日：1997-08-21
申请人： Nobuyuki Harada , Koji Miyake , Yoshihiro Motono , Hideyuki Tahara , Takumi Hatsuda , Teruyuki Kanto , Akito Yano , Yorimichi Dairoku , Kazuki Kimura , Yasuhiro Fujita
发明人： Nobuyuki Harada , Koji Miyake , Yoshihiro Motono , Hideyuki Tahara , Takumi Hatsuda , Teruyuki Kanto , Akito Yano , Yorimichi Dairoku , Kazuki Kimura , Yasuhiro Fujita
IPC分类号： C08F2/10 , C08J9/30
CPC分类号： C08F2/10 , C08F120/06 , C08F220/06
摘要： A method for the production of a water-absorbent resin capable of fast water absorption is disclosed which comprises the steps of dispersing bubbles of an inert gas in an aqueous monomer solution of a mixture of a water-soluble unsaturated monomer and a water-soluble cross-linking monomer and subjecting the mixture to copolymerization under the condition that a volume of the monomer solution wherein the inert gas is dispersed is in the range of 1.02 to 5 times of a volume of non-dispersant state.
摘要翻译：公开了一种能够快速吸水的吸水性树脂的制造方法，该方法包括以下步骤：将惰性气体的气泡分散在水溶性不饱和单体和水溶性交联剂的混合物的单体水溶液中在使分散有惰性气体的单体溶液的体积为非分散状态的体积的1.02〜5倍的条件下进行共聚合。

6. 发明授权

US08765857B2 Particulate water retaining material for cultivating plant having water absorbent resin as main component 有权
标题翻译：用于培养具有吸水性树脂作为主要成分的植物的颗粒保水材料
公开(公告)号：US08765857B2
公开(公告)日：2014-07-01
申请号：US10581343
申请日：2004-12-06
申请人： Hirotama Fujimaru , Yorimichi Dairoku , Kunihiko Ishizaki , Yoshifumi Adachi , Nobuyuki Harada
发明人： Hirotama Fujimaru , Yorimichi Dairoku , Kunihiko Ishizaki , Yoshifumi Adachi , Nobuyuki Harada
IPC分类号： C08K3/26 , C08K3/22 , C08F220/06 , A01G7/00
CPC分类号： A01G24/00 , A01G24/35
摘要： A particulate water retaining material for cultivating plant comprising (A) a carboxyl group-containing water-insoluble water absorbent resin and (B) a polyvalent metal compound, by having the compound (B) deposited on the rerin (A), it is made possible to possess an outstanding water absorbing property without impairing the growth of a plant.
摘要翻译：一种含有（A）含羧基的水不溶性吸水性树脂和（B）多价金属化合物的用于培养植物的颗粒状保水材料，通过使化合物（B）沉积在芦丁（A）上，制成可能具有优异的吸水性，而不损害植物的生长。

7. 发明申请

US20070101644A1 Particulate water retaining material for cultivating plant having water absorbent resin as main component 有权
标题翻译：用于培养具有吸水性树脂作为主要成分的植物的颗粒保水材料
公开(公告)号：US20070101644A1
公开(公告)日：2007-05-10
申请号：US10581343
申请日：2004-12-06
申请人： Hirotama Fujimaru , Yorimichi Dairoku , Kunihiko Ishizaki , Yoshifumi Adachi , Nobuyuki Harada
发明人： Hirotama Fujimaru , Yorimichi Dairoku , Kunihiko Ishizaki , Yoshifumi Adachi , Nobuyuki Harada
IPC分类号： A01G7/00
CPC分类号： A01G24/00 , A01G24/35
摘要： A particulate water retaining material for cultivating plant comprising (A) a carboxyl group-containing water-insoluble water absorbent resin and (B) a polyvalent metal compound, by having the compound (B) deposited on the the rerin (A), it is made possible to possess an outstanding water absorbing property without impairing the growth of a plant.
摘要翻译：含有（A）含羧基的水不溶性吸水性树脂和（B）多价金属化合物的栽培植物用颗粒状保水材料，通过使化合物（B）沉积在rerin（A）上，是使得具有优异的吸水性而不损害植物的生长成为可能。

8. 发明授权

US06187872B1 Water-absorbent agent and method for manufacturing the same 失效
标题翻译：吸水剂及其制造方法
公开(公告)号：US06187872B1
公开(公告)日：2001-02-13
申请号：US09051313
申请日：1998-04-06
申请人： Toru Yanase , Kazuki Kimura , Shin-ichi Fujino , Kinya Nagasuna , Kunihiko Ishizaki , Hirotama Fujimaru , Nobuyuki Harada
发明人： Toru Yanase , Kazuki Kimura , Shin-ichi Fujino , Kinya Nagasuna , Kunihiko Ishizaki , Hirotama Fujimaru , Nobuyuki Harada
IPC分类号： C08F812
CPC分类号： A61L15/60 , B01J20/26 , C08F8/00 , C08F8/44 , C08F2800/20 , C08F2810/20 , C08F220/06
摘要： A hydrogel polymer obtained by polymerizing a monomer component including acrylic acid (salt) is post-neutralized so that each of polymer particles derived from a polymer produced by neutralizing the hydrogel polymer has an allowable neutralization ratio. The polymer as obtained by neutralizing the hydrogel polymer is reacted with a crosslinking agent reactive to a functional group of the polymer. The allowable neutralization ratio, for example, is a neutralization ratio which is not lower, by not less than 20 mole percent, or more than, at least 55 mole percent, than an average neutralization ratio of a mass of the polymer particles, and the post-neutralization is carried out so that a number of polymer particles having a non-allowable neutralization ratio outside the allowable neutralization range is not more than 10 in 200 polymer particles, thus obtaining a water-absorbent agent having high absorbency under no applied pressure and high pressure wherein the amount of water soluble component is lower compared with the conventional water-absorbent agent and a change in pH of a swollen gel is small.
摘要翻译：通过使包含丙烯酸（盐）的单体组分聚合而获得的水凝胶聚合物被后中和，使得通过中和水凝胶聚合物产生的聚合物衍生的各聚合物颗粒具有允许的中和比。通过中和水凝胶聚合物获得的聚合物与与聚合物的官能团反应的交联剂反应。例如，容许的中和比例是中和比，其比不到聚合物颗粒的质量的平均中和比不低于20摩尔％，或至多55摩尔％，而且进行中和后，使得在200个聚合物粒子中，许多中和比例不超过允许中和比例的聚合物颗粒数不超过10个，从而获得在无施加压力下具有高吸收性的吸水剂，其中水溶性成分的量与常规吸水剂相比较低，并且溶胀凝胶的pH变化很小。

9. 发明授权

US5981070A Water-absorbent agent powders and manufacturing method of the same 失效
标题翻译：吸水剂粉末及其制造方法相同
公开(公告)号：US5981070A
公开(公告)日：1999-11-09
申请号：US793712
申请日：1997-03-03
申请人： Kunihiko Ishizaki , Kinya Nagasuna , Nobuyuki Harada
发明人： Kunihiko Ishizaki , Kinya Nagasuna , Nobuyuki Harada
IPC分类号： A61L15/60 , C08F8/00 , C08J3/12 , B32B5/16 , C08F2/16
CPC分类号： C08F8/00 , A61L15/60 , C08J3/245 , C08J9/08 , C08J9/102 , C08J9/36 , C08J2207/12 , C08J2300/14 , C08J2333/02 , Y10S521/905 , Y10T428/2991 , Y10T428/2998
摘要： A manufacturing method of water-absorbent agent powders of the present invention is a method of a reducing an amount of a residue of an epoxy crosslinking agent remaining therein by adding a nucleophilic reagent in a form of powder to surface region crosslinked water-absorbent resin powders having a carboxyl group under an applied heat in which the residue of the crosslinking agent remains. Since the method permits an amount of the residue of the crosslinking agent to be reduced by adding a nucleophilic reagent to the heated water-absorbent resin powders, the water-absorbent agent powders exhibiting well-balanced properties which are mutually negatively correlated from one another, i.e., high absorbency under pressure, a reduced amount of a residue of the epoxy crosslinking agent and a high absorbing rate compared with the conventional surface region crosslinked water-absorbent resin powders can be achieved. Such water-absorbent agent powders are suitably used in sanitary materials such as disposable diaper, sanitary napkins, etc.
摘要翻译： PCT No.PCT / JP96 / 01863 Sec。 371日期1997年3月3日 102（e）1997年3月3日PCT PCT 1996年7月5日PCT公布。出版物WO97 / 03114 日本1997年1月30日本发明的吸水剂粉末的制造方法是通过将表面区域交联的粉末状的亲核试剂添加到其中而残留的环氧交联剂的残渣量减少的方法具有羧基的吸水性树脂粉末，其中保留了交联剂的残余物。由于该方法允许通过向加热的吸水性树脂粉末中添加亲核试剂来减少交联剂的残留量，所以表现出彼此相互负相关的良好平衡性能的吸水剂粉末，即，与传统的表面区域交联的吸水性树脂粉末相比，可以实现在压力下的高吸收性，环氧交联剂残留量的减少和吸收率高的优点。这种吸水剂粉末适用于一次性尿布，卫生巾等卫生材料。

10. 发明授权

US5574121A Process for preparing an absorbent resin crosslinked with a mixture of trimethylolpropane diacrylate and triacrylate 失效
标题翻译：制备用三羟甲基丙烷二丙烯酸酯和三丙烯酸酯的混合物交联的吸收性树脂的方法
公开(公告)号：US5574121A
公开(公告)日：1996-11-12
申请号：US262065
申请日：1994-06-17
申请人： Yoshio Irie , Nobuyuki Harada , Kinya Nagasuna , Kohichi Hirota , Yoshihiko Masuda , Hideaki Nagano , Hideyuki Kubo
发明人： Yoshio Irie , Nobuyuki Harada , Kinya Nagasuna , Kohichi Hirota , Yoshihiko Masuda , Hideaki Nagano , Hideyuki Kubo
IPC分类号： A61L15/24 , C08F220/04 , C08F236/22
CPC分类号： C08F220/04 , A61L15/24 , Y10S526/93
摘要： A process for preparing an absorbent resin includes the steps of: preparing a first crosslinking agent (A) including at least two polymerizable unsaturated bonds; preparing a second crosslinking agent (B) including at least two polymerizable unsaturated bonds and hydroxyl groups; preparing a crosslinking agent including (A) and (B) with a ratio of (A) to (B) ranging from 95/5 to 50/50; and polymerizing a hydrophilic unsaturated monomer having at least one carboxyl group using the crosslinking agent. The crosslinking agent includes a crosslinking agent which includes a main component at least 90 percent by weight, the main component being an ester having at least two polymerizable unsaturated bonds, wherein the ester is composed of a polyhydroxy alcohol (C) having not more than six carbon atoms and at least three hydroxy groups, and an unsaturated carboxylic acid (D); and a molecular weight ratio of the main component to a standard compound (E) is in the range of from 0.7/1 to less than 1.3/1, (E) being an ester composed of (C) that composes the main component, and (D) that composes the main component, in which all the hydroxy groups in (C) are ester-linked with (D).
摘要翻译：制备吸收性树脂的方法包括以下步骤：制备包含至少两个可聚合不饱和键的第一交联剂（A）; 制备包含至少两个可聚合不饱和键和羟基的第二交联剂（B）; 制备包含（A）和（B）的交联剂，比例为（A）至（B）为95/5至50/50; 并使用交联剂聚合具有至少一个羧基的亲水性不饱和单体。交联剂包括交联剂，其包含至少90重量％的主要组分，主要组分是具有至少两个可聚合不饱和键的酯，其中该酯由不超过六个的多羟基醇（C）组成碳原子和至少三个羟基，和不饱和羧酸（D）; 并且主成分与标准化合物（E）的分子量比在0.7 / 1〜小于1.3 / 1的范围内，（E）是由构成主成分的（C）构成的酯，和（D）构成其中（C）中的所有羟基与（D）酯连接的主要组分。

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