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1. 发明申请

US20130059391A1 TEST PIECE FOR HEAVY METAL ION, PROCESS FOR DETECTING HEAVY METAL ION, KIT AND SENSOR 审中-公开
标题翻译：用于重金属离子的测试方法，用于检测重金属离子，工具包和传感器的过程
公开(公告)号：US20130059391A1
公开(公告)日：2013-03-07
申请号：US13594799
申请日：2012-08-25
申请人： Xiaoke Zhang , Yongming Li , Hisashi Kajiura
发明人： Xiaoke Zhang , Yongming Li , Hisashi Kajiura
IPC分类号： G01N31/22 , G01N21/75 , G01N33/20 , G01N30/96
CPC分类号： G01N33/1813 , G01N2021/7759
摘要： The invention provides a test piece for detecting heavy metal ions in an aqueous system to be detected, comprising a substrate, a polymer coating layer and a layer of heavy metal ion-detecting agent, wherein the polymer coating layer is provided such that the surface of the test piece is hydrophobic. The invention further provides a process for detecting heavy metal ions in an aqueous system, a kit comprising the heavy metal ion test piece and a sensor. A portable test piece and/or a device can be provided by the test piece according to the invention, so as to detect the heavy metal ions in a convenient, efficient and rapid manner.
摘要翻译：本发明提供一种用于检测待检测的水性体系中的重金属离子的试片，包括基底，聚合物涂层和重金属离子检测剂层，其中聚合物涂层被设置成使得试件是疏水的。本发明还提供了一种用于检测水性体系中的重金属离子的方法，包括重金属离子试验片和传感器的试剂盒。可以通过根据本发明的试件提供便携式测试件和/或设备，以便以方便，有效和快速的方式检测重金属离子。

2. 发明申请

US20120184040A1 METHOD AND DEVICE FOR DETECTION OF HEAVY METAL IONS IN WATER 失效
标题翻译：用于检测水中重金属离子的方法和装置
公开(公告)号：US20120184040A1
公开(公告)日：2012-07-19
申请号：US13348206
申请日：2012-01-11
申请人： Xiaoke Zhang , Hisashi Kajiura , Yongming Li
发明人： Xiaoke Zhang , Hisashi Kajiura , Yongming Li
IPC分类号： G01N33/20
CPC分类号： G01N33/1813
摘要： This disclosure discloses a method and a device for the detection of heavy metal ions in water. The method includes: providing a detection material, wherein the detection material includes a hydrophilic layer which is at least partially covered by a hydrophobic layer formed from a long-chain compound selected from the group consisting of a long-chain thiol, a long-chain fatty acid and combinations thereof, and wherein a detection area is an area covered by the hydrophobic layer, and the detection area has a surface having an initial contact angle with water of more than or equal to about 120°; contacting the detection area with an aqueous solution sample; determining whether the surface of the detection area has a hydrophobicity-hydrophilicity change after contact with the aqueous solution sample; and deciding whether heavy metal ions exist in the aqueous solution sample according to the determination.
摘要翻译：本公开公开了一种用于检测水中重金属离子的方法和装置。该方法包括：提供检测材料，其中所述检测材料包括至少部分被由长链化合物形成的疏水层覆盖的亲水层，所述长链化合物选自长链硫醇，长链脂肪酸及其组合，并且其中检测区域是由疏水层覆盖的区域，并且检测区域具有与水的初始接触角大于或等于约120°的表面; 使检测区域与水溶液样品接触; 确定检测区域的表面在与水溶液样品接触之后是否具有疏水性 - 亲水性变化; 并根据测定判定水溶液样品中是否存在重金属离子。

3. 发明授权

US08679849B2 Method and device for detection of heavy metal ions in water 失效
标题翻译：用于检测水中重金属离子的方法和装置
公开(公告)号：US08679849B2
公开(公告)日：2014-03-25
申请号：US13348206
申请日：2012-01-11
申请人： Xiaoke Zhang , Hisashi Kajiura , Yongming Li
发明人： Xiaoke Zhang , Hisashi Kajiura , Yongming Li
IPC分类号： G01N33/20
CPC分类号： G01N33/1813
摘要： This disclosure discloses a method and a device for the detection of heavy metal ions in water. The method includes: providing a detection material, wherein the detection material includes a hydrophilic layer which is at least partially covered by a hydrophobic layer formed from a long-chain compound selected from the group consisting of a long-chain thiol, a long-chain fatty acid and combinations thereof, and wherein a detection area is an area covered by the hydrophobic layer, and the detection area has a surface having an initial contact angle with water of more than or equal to about 120°; contacting the detection area with an aqueous solution sample; determining whether the surface of the detection area has a hydrophobicity-hydrophilicity change after contact with the aqueous solution sample; and deciding whether heavy metal ions exist in the aqueous solution sample according to the determination.
摘要翻译：本公开公开了一种用于检测水中重金属离子的方法和装置。该方法包括：提供检测材料，其中所述检测材料包括至少部分被由长链化合物形成的疏水层覆盖的亲水层，所述长链化合物选自长链硫醇，长链脂肪酸及其组合，并且其中检测区域是由疏水层覆盖的区域，并且检测区域具有与水的初始接触角大于或等于约120°的表面; 使检测区域与水溶液样品接触; 确定检测区域的表面在与水溶液样品接触之后是否具有疏水性 - 亲水性变化; 并根据测定判定水溶液样品中是否存在重金属离子。

4. 发明授权

US08231854B2 Method for treating carbon nanotubes, carbon nanotubes and carbon nanotubes device comprising thereof 失效
标题翻译：用于处理碳纳米管的方法，碳纳米管和包含它们的碳纳米管装置
公开(公告)号：US08231854B2
公开(公告)日：2012-07-31
申请号：US12270026
申请日：2008-11-13
申请人： Hisashi Kajiura , Yongming Li , Xianglong Li , Yunqi Liu , Lingchao Cao , Lei Fu , Dacheng Wei , Yu Wang , Daoben Zhu
发明人： Hisashi Kajiura , Yongming Li , Xianglong Li , Yunqi Liu , Lingchao Cao , Lei Fu , Dacheng Wei , Yu Wang , Daoben Zhu
IPC分类号： D01F9/12 , C01B31/00
CPC分类号： B82Y30/00 , B82Y40/00 , C01B32/174 , C01B2202/02 , C01B2202/06 , C01B2202/28 , H01M4/9083 , Y10S977/845
摘要： An efficient and cost-effective method for treating carbon nanotubes (CNTs) is provided. The method includes comprising: dispersing said carbon nanotubes in a dispersing medium to prepare a dispersion system; mixing said dispersion system with adsorbent so that type-specific carbon nanotubes contained in said dispersion system are absorbed onto the adsorbent, wherein the adsorbent is modified by a chemical/biological modifier so as to have different adsorption selectivity to carbon nanotubes of different types; and separating the adsorbent from the dispersion system, whereby the type-specific carbon nanotubes adsorbed onto the adsorbent is separated from the carbon nanotubes of another type enriched in the dispersion system; carbon nanotubes produced by the treatment method, and CNTs devices comprising thereof.
摘要翻译：提供了一种用于处理碳纳米管（CNT）的有效且经济有效的方法。该方法包括：将所述碳纳米管分散在分散介质中以制备分散系统; 将所述分散系统与吸附剂混合，使包含在所述分散系统中的型号碳纳米管被吸附到吸附剂上，其中吸附剂被化学/生物改性剂改性，以对不同类型的碳纳米管具有不同的吸附选择性; 从分散体系分离吸附剂，由此吸附在吸附剂上的特定类型的碳纳米管与分散系统中富集的另一种类型的碳纳米管分离; 通过处理方法制造的碳纳米管，以及包含它们的CNTs器件。

5. 发明申请

US20100143234A1 METHODS OF PREPARING AND PURIFYING CARBON NANOTUBES, CARBON NANOTUBES, AND AN ELEMENT USING THE SAME 审中-公开
标题翻译：制备和纯化碳纳米管，碳纳米管和使用其的元素的方法
公开(公告)号：US20100143234A1
公开(公告)日：2010-06-10
申请号：US12628718
申请日：2009-12-01
申请人： Hisashi Kajiura , Yongming Li , Hongliang Zhang , Yu Wang , Yunqi Liu , Dacheng Wei , Liping Huang
发明人： Hisashi Kajiura , Yongming Li , Hongliang Zhang , Yu Wang , Yunqi Liu , Dacheng Wei , Liping Huang
IPC分类号： D01F9/12
CPC分类号： B82Y40/00 , B82Y30/00 , C01B32/162 , C01B32/17 , C01B32/174 , C01B2202/02 , C01B2202/28
摘要： A method of preparing carbon nanotubes (CNT), a method of purifying carbon nanotubes, carbon nanotubes, and an element using said carbon nanotubes are provided. The method includes preparing carbon nanotubes by arc-discharge and employs a coordination chemistry process to remove a catalyst and/or optional promoter used in arc-discharge.
摘要翻译：提供了制备碳纳米管（CNT）的方法，碳纳米管的净化方法，碳纳米管和使用所述碳纳米管的元件。该方法包括通过电弧放电制备碳纳米管，并采用配位化学方法去除用于电弧放电的催化剂和/或任选的助催化剂。

6. 发明申请

US20090285746A1 METHOD FOR TREATING CARBON NANOTUBES, CARBON NANOTUBES AND CARBON NANOTUBES DEVICE COMPRISING THEREOF 失效
标题翻译：用于处理碳纳米管，碳纳米管和包含其的碳纳米管装置的方法
公开(公告)号：US20090285746A1
公开(公告)日：2009-11-19
申请号：US12270026
申请日：2008-11-13
申请人： Hisashi Kajiura , Yongming Li , Xianglong Li , Yunqi Liu , Lingchao Cao , Lei Fu , Dacheng Wei , Yu Wang , Daoben Zhu
发明人： Hisashi Kajiura , Yongming Li , Xianglong Li , Yunqi Liu , Lingchao Cao , Lei Fu , Dacheng Wei , Yu Wang , Daoben Zhu
IPC分类号： D01F9/12 , C01B31/00
CPC分类号： B82Y30/00 , B82Y40/00 , C01B32/174 , C01B2202/02 , C01B2202/06 , C01B2202/28 , H01M4/9083 , Y10S977/845
摘要： An efficient and cost-effective method for treating carbon nanotubes (CNTs) is provided. The method includes comprising: dispersing said carbon nanotubes in a dispersing medium to prepare a dispersion system; mixing said dispersion system with adsorbent so that type-specific carbon nanotubes contained in said dispersion system are absorbed onto the adsorbent, wherein the adsorbent is modified by a chemical/biological modifier so as to have different adsorption selectivity to carbon nanotubes of different types; and separating the adsorbent from the dispersion system, whereby the type-specific carbon nanotubes adsorbed onto the adsorbent is separated from the carbon nanotubes of another type enriched in the dispersion system; carbon nanotubes produced by the treatment method, and CNTs devices comprising thereof.
摘要翻译：提供了一种用于处理碳纳米管（CNT）的有效且经济有效的方法。该方法包括：将所述碳纳米管分散在分散介质中以制备分散系统; 将所述分散系统与吸附剂混合，使包含在所述分散系统中的型号碳纳米管被吸附到吸附剂上，其中吸附剂被化学/生物改性剂改性，以对不同类型的碳纳米管具有不同的吸附选择性; 从分散体系分离吸附剂，由此吸附在吸附剂上的特定类型的碳纳米管与分散系统中富集的另一种类型的碳纳米管分离; 通过处理方法制造的碳纳米管，以及包含它们的CNTs器件。

7. 发明申请

US20090211901A1 METHODS FOR PREPARING CNT FILM, CNT FILM WITH A SANDWICH STRUCTURE, AN ANODE INCLUDING THE CNT FILM AND AN ORGANIC LIGHT-EMITTING DIODES INCLUDING THE ANODE AND CNT DEVICE 审中-公开
标题翻译：用于制备CNT膜的方法，具有三明治结构的CNT膜，包括CNT膜的AN阳极和包括阳极和CNT装置的有机发光二极管
公开(公告)号：US20090211901A1
公开(公告)日：2009-08-27
申请号：US12370176
申请日：2009-02-12
申请人： Hisashi Kajiura , Yongming Li , Yu Wang , Yunqi Liu , Lingchao Cao , Dacheng Wei , Dachuan Shi , Hongliang Zhang , Gui Yu
发明人： Hisashi Kajiura , Yongming Li , Yu Wang , Yunqi Liu , Lingchao Cao , Dacheng Wei , Dachuan Shi , Hongliang Zhang , Gui Yu
IPC分类号： C25B11/04 , B05D3/02 , B32B37/00 , B32B23/20 , B32B9/04 , B28B1/14 , B82B1/00
CPC分类号： H01L51/0003 , B82Y10/00 , B82Y30/00 , B82Y40/00 , C01B32/174 , C01B2202/02 , C01B2202/28 , H01L51/002 , H01L51/0048 , H01L51/5215 , Y02E10/549 , Y10T428/30 , Y10T428/31786
摘要： Methods for preparing flexible transparent conducting carbon nanotube (CNT) films, the CNT film prepared from said methods, a method of treating CNT film by using thionyl bromide (SOBr2) as a dopant are provided. A novel CNT film laminate with a sandwich structure are also provided, a transparent, flexible anode including the CNT film and an organic light-emitting diodes (LEDs) including the anode are also provided. The method of the present application can very quickly and completely remove the filter membrane, compared with a general immersion method. CNTs are not destroyed by the “soft method”, which will allow for expanded applications in electroluminescent or photovoltaic devices.
摘要翻译：制备柔性透明导电碳纳米管（CNT）膜的方法，由所述方法制备的CNT膜，通过使用亚硫酰溴（SOBr 2）作为掺杂剂处理CNT膜的方法。还提供了具有夹层结构的新型CNT膜层压体，还提供了包括CNT膜的透明柔性阳极和包括阳极的有机发光二极管（LED）。与一般的浸渍方法相比，本申请的方法可以非常快速且完全地除去过滤膜。 CNT不会被“软方法”破坏，这将允许在电致发光或光伏器件中的扩展应用。

8. 发明申请

US20090202422A1 METHOD FOR TREATING CARBON NANOTUBES, CARBON NANOTUBES AND CARBON NANOTUBE DEVICE 审中-公开
标题翻译：碳纳米管，碳纳米管和碳纳米管装置的处理方法
公开(公告)号：US20090202422A1
公开(公告)日：2009-08-13
申请号：US12269999
申请日：2008-11-13
申请人： Hisashi Kajiura , Yongming Li , Lei Fu , Yunqi Liu , Xianglong Li , Lingchao Cao , Dacheng Wei , Yu Wang , Gui Yu
发明人： Hisashi Kajiura , Yongming Li , Lei Fu , Yunqi Liu , Xianglong Li , Lingchao Cao , Dacheng Wei , Yu Wang , Gui Yu
IPC分类号： C01B31/00 , D01F9/12 , C01B31/02
CPC分类号： B82Y30/00 , B82Y40/00 , C01B32/174 , C01B2202/28 , H01J1/304 , H01J9/025 , H01J2201/30469 , H01J2329/0455
摘要： A method for treating carbon nanotubes is proved, which comprises treating the carbon nanotubes with an aqueous solution containing hydroxyl radicals (HO.).
摘要翻译：证明了用于处理碳纳米管的方法，其包括用含羟基（HO）的水溶液处理碳纳米管。

9. 发明申请

US20110052479A1 METHOD FOR PREPARING CARBON NANOTUBES, CARBON NANOTUBE FILMS, AND ELECTRONIC DEVICES 审中-公开
标题翻译：制备碳纳米管，碳纳米管膜和电子器件的方法
公开(公告)号：US20110052479A1
公开(公告)日：2011-03-03
申请号：US12868285
申请日：2010-08-25
申请人： Hisashi Kajiura , Yongming Li , Jiaping Wang , Jing Sun , Lian Gao , Yan Wang , Jing Zhang
发明人： Hisashi Kajiura , Yongming Li , Jiaping Wang , Jing Sun , Lian Gao , Yan Wang , Jing Zhang
IPC分类号： D01F9/12
CPC分类号： B82Y40/00 , B82Y30/00 , C01B32/15
摘要： A method for preparing carbon nanotubes for synthesizing carbon nanotubes, fabricating carbon nanotube films and electronic devices is provided. The method for preparing carbon nanotubes can repair the defects in side walls of carbon nanotubes under stable condition easily and prepare carbon nanotubes of excellent properties. The method utilizes uric acid solution or ammonia water to treat carbon nanotubes after acidifying the carbon nanotubes by refluxing with nitric acid. The treatment temperature is, for example, 25° C.˜90° C., and treatment time is at least two 2 days. Preferably, the carbon nanotubes are treated with thionyl chloride solution before being treated with uric acid solution or ammonia water.
摘要翻译：提供了制备碳纳米管的碳纳米管的制备方法，制造碳纳米管膜和电子器件。制备碳纳米管的方法可以容易地在稳定条件下修复碳纳米管侧壁的缺陷，并制备性能优良的碳纳米管。该方法利用尿酸溶液或氨水在用硝酸回流酸化碳纳米管后处理碳纳米管。处理温度例如为25℃〜90℃，处理时间为2天以上。优选地，在用尿酸溶液或氨水处理之前，用亚硫酰氯溶液处理碳纳米管。

10. 发明申请

US20100193747A1 PROCESS OF PREPARING CARBON NANOTUBE FILM, THE CARBON NANOTUBE FILM PREPARED THEREBY AND CARBON NANOTUBE ELEMENTS COMPRISING THE SAME 审中-公开
标题翻译：制备碳纳米管膜的方法，制备的碳纳米管膜和包含其的碳纳米管元素
公开(公告)号：US20100193747A1
公开(公告)日：2010-08-05
申请号：US12638452
申请日：2009-12-15
申请人： Hisashi Kajiura , Yongming Li , Hongliang Zhang , Yunqi Liu , Lingchao Cao , Dacheng Wei , Yu Wang , Liping Huang
发明人： Hisashi Kajiura , Yongming Li , Hongliang Zhang , Yunqi Liu , Lingchao Cao , Dacheng Wei , Yu Wang , Liping Huang
IPC分类号： H01B1/04 , C23C16/44
CPC分类号： H01M4/926 , B82Y30/00 , B82Y40/00 , C01B32/162 , C01B2202/02 , C01B2202/36
摘要： A process of a preparing transparent conductive carbon nanotube (CNT) film, the carbon nanotube film prepared by the process, and carbon nanotube elements including the carbon nanotube film are provided. The carbon nanotube film has a higher transparency and much lower sheet resistance compared with the carbon nanotube film obtained by a conventional filtration process.
摘要翻译：提供制备透明导电碳纳米管（CNT）膜，通过该方法制备的碳纳米管膜和包括碳纳米管膜的碳纳米管元件的方法。与通过常规过滤方法获得的碳纳米管膜相比，碳纳米管膜具有更高的透明度和更低的片电阻。

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