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1. 发明授权

US5948152A Homogeneous liquid complexes of anionic organic dyes and quaternary ammonium compounds and methods of coloring utilizing such complexes 失效
标题翻译：阴离子有机染料和季铵化合物的均相液体络合物和利用这种络合物着色的方法
公开(公告)号：US5948152A
公开(公告)日：1999-09-07
申请号：US065597
申请日：1998-04-24
申请人： Xiaodong Edward Zhao , Kaye Cannon Suddeth , Patrick D. Moore , Raj Batlaw
发明人： Xiaodong Edward Zhao , Kaye Cannon Suddeth , Patrick D. Moore , Raj Batlaw
IPC分类号： C09B69/04 , C08K5/17 , C08L101/00 , C09B62/465 , C09B67/26 , C09B67/54 , C09D11/00 , C09D11/02
CPC分类号： C09D11/328 , C09B67/0073 , C09B67/0096 , C09D11/037
摘要： This invention relates to liquid complexes of anionic organic dyes with quaternary ammonium compounds which are homogeneous and thus substantially free of unwanted inorganic salts. Of particular interest as quaternary ammonium compounds are those which comprise alkoxylated moieties. Such complexes are formed through ionic bonds formed between the two compounds. The complexes are then removed of substantially all resultant unwanted salt formed from the cations of the dye and the counter ions of the quat so as to obtain an homogeneous liquid colorant which easily disperses within different media and which possess favorable migration and coloring characteristics. This invention also concerns methods of making the aforementioned salt-free anionic dye/quat complexes as well as methods of utilizing such complexes for dyeing thermoplastic and thermoset compositions and the incorporation of such complexes within aqueous and non-aqueous formulations and ink compositions.
摘要翻译：本发明涉及阴离子有机染料与季铵化合物的液体络合物，其是均匀的，因此基本上不含不需要的无机盐。特别令人感兴趣的季铵化合物是包含烷氧基化部分的化合物。通过在两种化合物之间形成的离子键形成这种络合物。然后将复合物从染料的阳离子和季铵盐的反离子中除去基本上由所得到的所有不希望的盐，以获得容易分散在不同介质中并具有良好迁移和着色特性的均匀液体着色剂。本发明还涉及制备上述无盐阴离子染料/季铵络合物的方法以及利用这种络合物染色热塑性和热固性组合物的方法以及将这些络合物引入含水和非水性配方和油墨组合物中的方法。

2. 发明授权

US5938828A Solid complexes of anionic organic dyes and quaternary ammonium compounds and methods of coloring utilizing such complexes 失效
标题翻译：阴离子有机染料和季铵化合物的固体络合物和利用这种络合物着色的方法
公开(公告)号：US5938828A
公开(公告)日：1999-08-17
申请号：US65620
申请日：1998-04-24
申请人： Xiaodong Edward Zhao , Kaye Cannon Suddeth , Robert L. Mahaffey, Jr.
发明人： Xiaodong Edward Zhao , Kaye Cannon Suddeth , Robert L. Mahaffey, Jr.
IPC分类号： C08K5/17 , C08L101/00 , C09B62/465 , C09B67/54 , C09B69/04 , C09D11/00
CPC分类号： C09D11/328 , C09B67/0096 , C09B69/04
摘要： This invention relates to solid complexes of anionic organic dyes with quaternary ammonium compounds which have average molecular weights of below about 900 which are substantially free from unwanted salts. Of particular interest as quaternary ammonium compounds are those which comprise alkoxylated moieties. Such complexes are formed through ionic bonds formed between the two compounds. The complexes are then removed of substantially all resultant unwanted salt formed from the cations of the dye and the counter-ions of the quat so as to obtain a solid dyeing agent which easily disperses within different media and which possess extremely good non-migration and coloring characteristics. This invention also concerns methods of making the aforementioned salt-free solid anionic dye/quat complexes as well as methods of utilizing such complexes for dyeing thermoplastic, thermoset, and wax compositions.
摘要翻译：本发明涉及阴离子有机染料与平均分子量低于约900的季铵化合物的固体络合物，其基本上不含不需要的盐。特别令人感兴趣的季铵化合物是包含烷氧基化部分的化合物。通过在两种化合物之间形成的离子键形成这种络合物。然后将复合物从染料阳离子和季铵盐的反离子中除去基本上所有由此形成的不需要的盐，以获得容易分散在不同介质中并且具有非常好的非迁移和着色的固体染色剂特点本发明还涉及制备上述无盐固体阴离子染料/季铵络合物的方法以及利用这种络合物染色热塑性，热固性和蜡组合物的方法。

3. 发明授权

US07501462B2 Polyolefin composition 有权
标题翻译：聚烯烃组合物
公开(公告)号：US07501462B2
公开(公告)日：2009-03-10
申请号：US12072898
申请日：2008-02-28
申请人： Jiannong Xu , Xiaodong Edward Zhao , Jiang Li , Kemper David Lake, Jr.
发明人： Jiannong Xu , Xiaodong Edward Zhao , Jiang Li , Kemper David Lake, Jr.
IPC分类号： C08K5/15 , C07D323/04
CPC分类号： C08K5/1575 , C08K2201/014 , Y10S525/938 , C08L23/02
摘要： Clarified polyolefins such as polypropylene are used widely to make polymer articles, containers, and the like. Such articles may be manufactured by the injection of molten polymer into a mold or forming device in manufacturing processes at high rates. A clarified composition is provided to achieve optimized clarity and organoleptic performance at lower processing temperatures and/or within a polypropylene resin having a higher melt flow rate.
摘要翻译：澄清的聚烯烃如聚丙烯广泛用于制备聚合物制品，容器等。这样的制品可以通过在高速率的制造工艺中将熔融聚合物注入模具或成型装置中来制造。提供澄清的组合物以在较低加工温度下和/或具有较高熔体流动速率的聚丙烯树脂内获得最佳的透明度和感官性能。

4. 发明授权

US06599968B2 Thermoplastic nucleating compounds 有权
标题翻译：热塑性成核化合物
公开(公告)号：US06599968B2
公开(公告)日：2003-07-29
申请号：US10008322
申请日：2001-11-03
申请人： Xiaodong Edward Zhao , Darin L. Dotson , Brian M. Burkhart , Jeffrey R. Jones
发明人： Xiaodong Edward Zhao , Darin L. Dotson , Brian M. Burkhart , Jeffrey R. Jones
IPC分类号： C08K509
CPC分类号： C08K5/12 , C07C61/13 , C07C2602/42 , C08K5/0083 , C08K5/098 , C08L23/10
摘要： Compounds and compositions comprising specific metal salts of bicyclo[2.2.1]heptane dicarboxylate salts in order to provide highly desirable properties within polyolefin articles are provided. The inventive salts and derivatives thereof are useful as nucleating and/or clarifying agents for such polyolefin, provide excellent crystallization temperatures, stiffness, and calcium stearate compatibility within target polyolefin. Also, such compounds exhibit very low hygroscopicity and therefore excellent shelf stability as powdered or granular formulations. Polyolefin additive compositions and methods of producing polyolefin with such compounds are also contemplated within this invention.
摘要翻译：提供了包含双环[2.2.1]庚烷二羧酸盐的特定金属盐以提供聚烯烃制品中非常理想的性能的化合物和组合物。本发明的盐及其衍生物可用作这种聚烯烃的成核剂和/或澄清剂，在目标聚烯烃内提供优异的结晶温度，刚度和硬脂酸钙相容性。此外，这些化合物显示出非常低的吸湿性，因此表现出作为粉末或颗粒制剂的优异的贮存稳定性。聚烯烃添加剂组合物和用这些化合物生产聚烯烃的方法也在本发明中。

5. 发明授权

US5948153A Water-soluble complexes of optical brighteners and quaternary ammonium compounds which are substantially free from unwanted salts 失效
标题翻译：基本上不含不需要的盐的荧光增白剂和季铵化合物的水溶性络合物
公开(公告)号：US5948153A
公开(公告)日：1999-09-07
申请号：US65619
申请日：1998-04-24
申请人： Qinghong Jessica Ann , Xiaodong Edward Zhao , James Michael Spry
发明人： Qinghong Jessica Ann , Xiaodong Edward Zhao , James Michael Spry
IPC分类号： C09K11/06 , C08K5/17 , C08L101/00 , C09B69/04 , C09D7/12 , C09D11/00 , C09D201/00 , C11D3/42 , D06L3/12 , C09B67/54
CPC分类号： C09D11/00 , C09D7/1233 , C11D3/42 , D06L3/1207 , D06L3/1264 , C08K5/19 , Y02P20/582
摘要： This invention relates to water-soluble complexes of optical brighteners with quaternary ammonium compounds which are substantially free from unwanted salts. Such complexes are formed through ionic bonds formed between the two compounds. The inventive complexes are then removed of substantially all excess unwanted salt so as to obtain an optical brightener compound which easily solubilizes within, dispenses from, and exhibits excellent compatibility with standard detergent and softener compositions, which exhibits the desired degree of affinity for various substrate surfaces, including textile, paper, wood, and plastics, as well as within leak detector formulations, and which provides a desired accumulation effect on substrate surfaces upon repeated treatments. Such inventive complexes can also be utilized to whiten thermoplastics and thermosets. Furthermore, this invention also concerns methods of making and utilizing such inventive optical brightening complexes.
摘要翻译：本发明涉及荧光增白剂与基本上不含不需要的盐的季铵化合物的水溶性络合物。通过在两种化合物之间形成的离子键形成这种络合物。然后将本发明的复合物除去基本上所有过量的不需要的盐，以便获得在标准洗涤剂和软化剂组合物中容易溶解，分配和显示出优异的相容性的荧光增白剂化合物，其对各种底物表面具有所需程度的亲和力，包括纺织品，纸张，木材和塑料以及泄漏检测器配方中，并且在反复处理时对基材表面提供期望的积累效果。这种本发明的复合物也可用于增塑热塑性塑料和热固性材料。此外，本发明还涉及制备和利用这种本发明的光学增亮配合物的方法。

6. 发明授权

US06521685B1 Clarifying agent formulations for thermoplastics exhibiting very high nucleation efficacy 有权
标题翻译：表现出非常高的成核效力的热塑性塑料的澄清剂配方
公开(公告)号：US06521685B1
公开(公告)日：2003-02-18
申请号：US09898359
申请日：2001-07-03
申请人： Xiaodong Edward Zhao
发明人： Xiaodong Edward Zhao
IPC分类号： C08K5098
CPC分类号： C08K5/098 , C08K5/1575
摘要： Certain thermoplastic additives that induce simultaneous low clarity and high nucleation efficacy are provided. Such additives include combinations of certain bicyclic salts (which by themselves induce very high nucleation efficacy) and certain benzylidene sorbitol acetals and derivatives (hereinafter collectively referred to as “DBSs”)(which alone provide very low haze measurements and thus highly desirable clarity characteristics). In comparison, other types of standard thermoplastic nucleators, such as sodium benzoate and sodium 2,2′-methylene-bis-(4,6-di-tert-butylphenyl)phosphate provide relatively high peak crystallization temperatures, but do not combine synergistically with DBSs to provide the same results as for the inventive combination of bicyclic salts and DBSs.
摘要翻译：提供了诱导同时低澄清度和高成核效力的某些热塑性添加剂。这些添加剂包括某些双环盐（其自身诱导非常高的成核效力）和某些亚苄基山梨糖醇缩醛和衍生物（以下统称为“DBS”）的组合（其单独提供非常低的雾度测量，因此提供非常理想的澄清特性）。相比之下，其他类型的标准热塑性成核剂，如苯甲酸钠和2,2'-亚甲基 - 双 - （4,6-二叔丁基苯基）磷酸钠可提供较高的峰值结晶温度，但不能与 DBS以提供与双环盐和DBS的本发明组合相同的结果。

7. 发明授权

US06465551B1 Bicyclo[2.2.1]heptane dicarboxylate salts as polyolefin nucleators 有权
标题翻译：双环[2.2.1]庚烷二羧酸盐作为聚烯烃成核剂
公开(公告)号：US06465551B1
公开(公告)日：2002-10-15
申请号：US09815832
申请日：2001-03-24
申请人： Xiaodong Edward Zhao , Darin L. Dotson
发明人： Xiaodong Edward Zhao , Darin L. Dotson
IPC分类号： C08K509
CPC分类号： C08K5/098 , C07C61/13 , C07C2602/42 , C08K5/12 , C08L23/10
摘要： Compounds and compositions comprising specific metal salts of bicyclo[2.2.1 ]heptane dicarboxylate salts in order to provide highly desirable properties within polyolefin articles are provided. The inventive salts and derivatives thereof are useful as nucleating and/or clarifying agents for such polyolefin, provide excellent crystallization temperatures, stiffness, and calcium stearate compatibility within target polyolefin. Also, such compounds exhibit very low hygroscopicity and therefore excellent shelf stability as powdered or granular formulations. Polyolefin additive compositions and methods of producing polyolefin with such compounds are also contemplated within this invention.
摘要翻译：提供了包含双环[2.2.1]庚烷二羧酸盐的特定金属盐以提供聚烯烃制品中非常理想的性能的化合物和组合物。本发明的盐及其衍生物可用作这种聚烯烃的成核剂和/或澄清剂，在目标聚烯烃内提供优异的结晶温度，刚度和硬脂酸钙相容性。此外，这些化合物显示出非常低的吸湿性，因此表现出作为粉末或颗粒制剂的优异的贮存稳定性。聚烯烃添加剂组合物和用这些化合物生产聚烯烃的方法也在本发明中。

8. 发明授权

US07351758B2 Addictive composition and articles containing the same 有权
标题翻译：上瘾的成分和含有相同的物品
公开(公告)号：US07351758B2
公开(公告)日：2008-04-01
申请号：US11135786
申请日：2005-05-24
申请人： Jiannong Xu , Xiaodong Edward Zhao , Jiang Li , Kemper David Lake, Jr.
发明人： Jiannong Xu , Xiaodong Edward Zhao , Jiang Li , Kemper David Lake, Jr.
IPC分类号： C08K5/15 , C07D323/04
CPC分类号： C08K5/1575 , C08K2201/014 , Y10S525/938 , C08L23/02
摘要： Clarified polyolefins such as polypropylene are used widely to make polymer articles, containers, and the like. Such articles may be manufactured by the injection of molten polymer into a mold or forming device in manufacturing processes at high rates. A clarified composition is provided to achieve optimized clarity and organoleptic performance at lower processing temperatures and/or within a polypropylene resin having a higher melt flow rate.
摘要翻译：澄清的聚烯烃如聚丙烯广泛用于制备聚合物制品，容器等。这样的制品可以通过在高速率的制造工艺中将熔融聚合物注入模具或成型装置中来制造。提供澄清的组合物以在较低加工温度下和/或具有较高熔体流动速率的聚丙烯树脂内获得最佳的透明度和感官性能。

9. 发明授权

US06583206B2 Saturated [2.2.2] dicarboxylate salt thermoplastic nucleators and thermoplastic compositions thereof 有权
标题翻译：饱和[2.2.2]二羧酸盐热塑性成核剂及其热塑性组合物
公开(公告)号：US06583206B2
公开(公告)日：2003-06-24
申请号：US09874858
申请日：2001-06-05
申请人： Xiaodong Edward Zhao
发明人： Xiaodong Edward Zhao
IPC分类号： C08J300
CPC分类号： C08K5/098 , C07C61/13 , C07C2602/44 , C08K5/0083 , C08L23/02
摘要： Compounds of and compositions comprising specific salts of saturated [2.2.2] dicarboxylate in order to provide highly desirable properties within thermoplastic (e.g., polyolefin) articles are provided. The inventive salts and derivatives thereof are useful as nucleating and/or clarifying agents for such thermoplastics, are easy to produce and handle, and relatively inexpensive to manufacture. Such compounds induce high peak crystallization and improved stiffness within thermoplastics. Also, thermoplastic compositions comprising such novel nucleating agents exhibit improved heat distortion properties and clarity levels in comparison with the closest unsaturated salt nucleating agents. Thermoplastic additive compositions and methods of producing thermoplastics with such compounds are also contemplated within this invention.
摘要翻译：提供了包含饱和[2.2.2]二羧酸盐的特定盐的化合物和组合物，以便在热塑性（例如聚烯烃）制品中提供高度期望的性能。本发明的盐及其衍生物可用作这种热塑性塑料的成核剂和/或澄清剂，易于生产和处理，制造成本相对便宜。这种化合物在热塑性塑料中引起高峰结晶和改善刚度。此外，包含这种新型成核剂的热塑性组合物与最接近的不饱和盐成核剂相比表现出改进的热变形性能和澄清度。本发明也考虑了热塑性添加剂组合物和用这种化合物生产热塑性塑料的方法。

10. 发明授权

US06534574B1 Highly nucleated thermoplastic articles 有权
标题翻译：高度成核的热塑性制品
公开(公告)号：US06534574B1
公开(公告)日：2003-03-18
申请号：US09995315
申请日：2001-11-27
申请人： Xiaodong Edward Zhao , Darin L. Dotson , Brian G. Morin , Brian M. Burkhart , Martin E. Cowan , Jeffrey R. Jones
发明人： Xiaodong Edward Zhao , Darin L. Dotson , Brian G. Morin , Brian M. Burkhart , Martin E. Cowan , Jeffrey R. Jones
IPC分类号： C08K509
CPC分类号： C08K5/0083 , C07C61/13 , C07C2602/42 , C08K5/098 , C08K5/12 , C08L23/10 , C08L23/12
摘要： Compounds and compositions comprising specific metal salts of bicyclo[2.2.1 ]heptane dicarboxylate salts in order to provide highly desirable properties within polyolefin articles are provided. The inventive salts and derivatives thereof are useful as nucleating and/or clarifying agents for such polyolefin, provide excellent crystallization temperatures, stiffness, and calcium stearate compatibility within target polyolefin. Also, such compounds exhibit very low hygroscopicity and therefore excellent shelf stability as powdered or granular formulations. Polyolefin additive compositions and methods of producing polyolefin with such compounds are also contemplated within this invention.
摘要翻译：提供了包含双环[2.2.1]庚烷二羧酸盐的特定金属盐以提供聚烯烃制品中非常理想的性能的化合物和组合物。本发明的盐及其衍生物可用作这种聚烯烃的成核剂和/或澄清剂，在目标聚烯烃内提供优异的结晶温度，刚度和硬脂酸钙相容性。此外，这些化合物显示出非常低的吸湿性，因此表现出作为粉末或颗粒制剂的优异的贮存稳定性。聚烯烃添加剂组合物和用这些化合物生产聚烯烃的方法也在本发明中。

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