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1. 发明授权

US5753716A Use of aluminum phosphate as the dehydration catalyst in single step dimethyl ether process 失效
标题翻译：在单步二甲醚工艺中使用磷酸铝作为脱水催化剂
公开(公告)号：US5753716A
公开(公告)日：1998-05-19
申请号：US803608
申请日：1997-02-21
申请人： Xiang-Dong Peng , Gene E. Parris , Bernard A. Toseland , Paula J. Battavio
发明人： Xiang-Dong Peng , Gene E. Parris , Bernard A. Toseland , Paula J. Battavio
IPC分类号： C07C29/153 , C07C29/154 , C07C29/156 , C07C41/01 , C07C27/00
CPC分类号： C07C29/156 , C07C29/153 , C07C29/154 , C07C41/01
摘要： The present invention pertains to a process for the coproduction of methanol and dimethyl ether (DME) directly from a synthesis gas in a single step (hereafter, the "single step DME process"). In this process, the synthesis gas comprising hydrogen and carbon oxides is contacted with a dual catalyst system comprising a physical mixture of a methanol synthesis catalyst and a methanol dehydration catalyst. The present invention is an improvement to this process for providing an active and stable catalyst system. The improvement comprises the use of an aluminum phosphate based catalyst as the methanol dehydration catalyst. Due to its moderate acidity, such a catalyst avoids the coke formation and catalyst interaction problems associated with the conventional dual catalyst systems taught for the single step DME process.
摘要翻译：本发明涉及在单一步骤（以下称为“单步DME方法”）中从合成气中直接共同生产甲醇和二甲醚（DME）的方法。在该方法中，包含氢和碳氧化物的合成气与包含甲醇合成催化剂和甲醇脱水催化剂的物理混合物的双重催化剂体系接触。本发明是提供活性和稳定的催化剂体系的该方法的改进。改进之处在于使用磷酸铝基催化剂作为甲醇脱水催化剂。由于其中等酸度，这种催化剂避免了与用于单步DME方法教导的常规双催化剂体系相关的焦炭形成和催化剂相互作用问题。

2. 发明申请

US20100224834A1 Method For Determining Carbon Content Of A Hydrocarbon-Containing Mixture 审中-公开
标题翻译：测定含烃混合物中碳含量的方法
公开(公告)号：US20100224834A1
公开(公告)日：2010-09-09
申请号：US12784852
申请日：2010-05-21
申请人： Xiang-Dong Peng , Blaine Edward Herb , Matthew H. MacConnell , Winfried Stephen Hoglen
发明人： Xiang-Dong Peng , Blaine Edward Herb , Matthew H. MacConnell , Winfried Stephen Hoglen
IPC分类号： C09K3/00 , G01N31/00
CPC分类号： G01N9/36 , G01N33/225 , Y10T436/21
摘要： A method for determining a carbon content value of a hydrocarbon-containing mixture. At least one composition-dependent bulk property of the hydrocarbon-containing mixture is measured and optionally at least one non-hydrocarbon component concentration is measured with the resulting measurements used in a carbon content correlation for calculating the carbon content of the hydrocarbon-containing mixture. The carbon content may be used in a hydrogen and/or synthesis gas production process for calculating a target flow rate of steam to be combined with the hydrocarbon-containing mixture to form a mixed feed having a target steam-to-carbon ratio.
摘要翻译：一种用于测定含烃混合物的碳含量值的方法。测量含烃混合物的至少一种组成依赖的整体性质，并且任选地测量至少一种非烃组分浓度，用碳含量相关性得到的测量值用于计算含烃混合物的碳含量。碳含量可以用于氢和/或合成气生产过程中，用于计算与含烃混合物组合的蒸汽的目标流速，以形成具有目标蒸汽 - 碳比的混合进料。

3. 发明申请

US20080241059A1 Catalytic Steam Reforming With Recycle 有权
标题翻译：催化蒸汽重整与回收
公开(公告)号：US20080241059A1
公开(公告)日：2008-10-02
申请号：US11691039
申请日：2007-03-26
申请人： Xiang-Dong Peng , James Richard O'Leary , Blaine Edward Herb , Krishnakumar Jambunathan
发明人： Xiang-Dong Peng , James Richard O'Leary , Blaine Edward Herb , Krishnakumar Jambunathan
IPC分类号： C01B3/32
CPC分类号： C01B3/382 , C01B3/384 , C01B3/48 , C01B2203/0233 , C01B2203/0283 , C01B2203/04 , C01B2203/0811 , C01B2203/0827 , C01B2203/0883 , C01B2203/0894 , C01B2203/127 , C01B2203/1294 , C01B2203/142 , C01B2203/148
摘要： A method for generating hydrogen in a production facility having a catalytic steam reformer, a boiler downstream of the catalytic steam reformer, optionally having a prereformer, and optionally having a shift reactor, wherein the reformer feed gas mixture is formed using a steam-containing recycle gas mixture which was formed from boiler effluent. The boiler generates steam which may be used to form the reformer feed gas mixture, used elsewhere in the production facility, and/or used for export steam.
摘要翻译：一种在具有催化蒸汽重整器，催化蒸汽重整器下游的锅炉，任选地具有预重整器和任选地具有变换反应器的生产设备中产生氢的方法，其中重整器进料气体混合物是使用含蒸汽的再循环由锅炉废水形成的气体混合物。锅炉产生可用于形成重整器进料气体混合物的蒸汽，其用于生产设备中的其他地方和/或用于出口蒸汽。

4. 发明申请

US20050132884A1 Generation of elevated pressure gas mixtures by absorption and stripping 有权
标题翻译：通过吸收和汽提生成高压气体混合物
公开(公告)号：US20050132884A1
公开(公告)日：2005-06-23
申请号：US10739970
申请日：2003-12-18
申请人： Jianguo Xu , Xiang-Dong Peng , Harold Gunardson
发明人： Jianguo Xu , Xiang-Dong Peng , Harold Gunardson
IPC分类号： B01D53/14 , C01B3/52 , C01B32/50
CPC分类号： B01D53/1493 , B01D53/14 , B01D53/1425 , B01D53/1475 , C01B3/52 , C01B2203/0233 , C01B2203/0283 , C01B2203/0415 , C01B2203/0475 , Y02C10/06 , Y02P20/152
摘要： Method of making a product gas mixture comprising providing a first gas mixture, contacting the first gas mixture with a lean absorber liquid at a first pressure and absorbing a portion of the first gas mixture in the lean absorber liquid to provide a rich absorber liquid and a non-absorbed residual gas, pressurizing the rich absorber liquid provide a pressurized rich absorber liquid, stripping the pressurized rich absorber liquid with a stripping gas at a second pressure greater than the first pressure to provide a pressurized lean absorber liquid and the product gas mixture, and reducing the pressure of the pressurized lean absorber liquid to provide the lean absorber liquid at the first pressure.
摘要翻译：制备产物气体混合物的方法包括提供第一气体混合物，在第一压力下使第一气体混合物与贫吸收剂液体接触并吸收贫吸收液体中的第一气体混合物的一部分，以提供富吸收液体和非吸收的残余气体，对富吸收剂液体加压提供加压的富吸收剂液体，在大于第一压力的第二压力下用汽提气体汽提加压的富吸收剂液体，以提供加压的贫吸收液体和产物气体混合物，以及降低加压贫吸收液体的压力，以在第一压力下提供贫吸收液体。

5. 发明申请

US20050102901A1 In-situ gasification of soot contained in exothermically generated syngas stream 有权
标题翻译：含放热产生的合成气流中烟灰的原位气化
公开(公告)号：US20050102901A1
公开(公告)日：2005-05-19
申请号：US10715757
申请日：2003-11-18
申请人： William Licht , Shankar Nataraj , Xiang-Dong Peng , John Repasky
发明人： William Licht , Shankar Nataraj , Xiang-Dong Peng , John Repasky
IPC分类号： C01B3/36 , C10J3/84 , C01B31/20 , C01B3/24
CPC分类号： C10K1/02 , C01B3/36 , C01B2203/0233 , C01B2203/0255 , C01B2203/04 , C01B2203/049 , C01B2203/0838 , C01B2203/141 , C10J3/466 , C10J3/721 , C10J3/84 , C10J2200/06 , C10J2300/094 , C10J2300/0983 , C10J2300/1846 , C10K3/003
摘要： A system is set forth for the exothermic generation of soot depleted syngas comprising (i) reacting a hydrocarbon-containing fuel with an oxygen containing gas in a first reactor to produce the syngas and byproducts comprising CO2, H2O and soot; and (ii) introducing the syngas and byproducts into a second reactor containing a non-carbonaceous material that traps the soot for a sufficient time such that the majority of the byproduct soot is gasified via reaction with the byproduct CO2 and/or H2O to produce a syngas stream that is depleted in the soot. The system is particularly suitable for the practice of heat exchange reforming wherein a portion of the heat is recovered from the soot depleted syngas stream and used as at least a portion of the heat to facilitate the additional production of syngas via the (endothermic) catalytic reforming of natural gas and steam.
摘要翻译：阐述了用于放出产生不含烟灰的合成气的系统，其包括（i）在第一反应器中使含烃燃料与含氧气体反应以产生合成气，以及包含CO 2 H， O和烟灰; 和（ii）将合成气和副产物引入到含有非碳质材料的第二反应器中，所述非碳质材料捕集烟灰足够的时间，使得大部分副产物烟灰通过与副产物CO 2反应而气化和/或H 2 O以产生在烟炱中耗尽的合成气流。该系统特别适用于热交换重整的实践，其中一部分热量从不含烟灰的合成气流中回收并用作至少一部分热量，以促进通过（吸热）催化重整而额外生产合成气的天然气和蒸汽。

6. 发明授权

US6069180A Single step synthesis gas-to-dimethyl ether process with methanol introduction 有权
标题翻译：用甲醇引入单步合成气 - 二甲醚工艺
公开(公告)号：US6069180A
公开(公告)日：2000-05-30
申请号：US213480
申请日：1998-12-17
申请人： Xiang-Dong Peng , Andrew Wilson Wang , Bernard Allen Toseland
发明人： Xiang-Dong Peng , Andrew Wilson Wang , Bernard Allen Toseland
IPC分类号： C07C41/01 , C07C27/00
CPC分类号： C07C41/01 , Y02P20/142
摘要： A process is set forth for converting synthesis gas into dimethyl ether (DME) in a single step comprising contacting the synthesis gas with a bifunctional catalyst system having a methanol synthesis functionality and a methanol dehydration functionality. In particular, the present invention is an improvement to said process for increasing the stability of the bifunctional catalyst system, particularly when the process is conducted in the liquid phase. The improvement comprises introducing a methanol containing stream into the DME reactor such that the methanol concentration throughout the DME reactor is maintained at a concentration greater than 1.0%, generally between 4.0% and 8.0%. In one embodiment of the present invention, the methanol containing stream comprises at least a portion of the byproduct methanol from the DME reactor such that said portion of byproduct methanol is introduced into the DME reactor as a recycle stream.
摘要翻译：阐述了在单步骤中将合成气转化为二甲醚（DME）的方法，包括使合成气与具有甲醇合成官能度和甲醇脱水官能团的双功能催化剂体系接触。特别地，本发明是提高双官能催化剂体系的稳定性的所述方法的改进，特别是当该方法在液相中进行时。改进之处在于将含甲醇的料流引入DME反应器，使得整个DME反应器中的甲醇浓度保持在大于1.0％，通常在4.0％和8.0％之间的浓度。在本发明的一个实施方案中，含甲醇的物流包含来自DME反应器的副产物甲醇的至少一部分，使得所述部分副产物甲醇作为循环物流引入DME反应器。

7. 发明授权

US08303929B2 Process for producing a hydrogen-containing product gas 有权
标题翻译：含氢产物气体的制造方法
公开(公告)号：US08303929B2
公开(公告)日：2012-11-06
申请号：US12760583
申请日：2010-04-15
申请人： Xiang-Dong Peng , Diwakar Garg , William Robert Licht , Shankar Nataraj , Peter de Geest , Eric S. Wagner
发明人： Xiang-Dong Peng , Diwakar Garg , William Robert Licht , Shankar Nataraj , Peter de Geest , Eric S. Wagner
IPC分类号： C01B3/24 , C01B3/38
CPC分类号： C01B3/382 , C01B3/384 , C01B2203/0233 , C01B2203/1017 , C01B2203/1052 , C01B2203/1058 , C01B2203/1082 , C01B2203/1094 , C01B2203/1241 , C01B2203/1247 , C01B2203/1258 , C01B2203/143
摘要： A process for producing a hydrogen-containing product gas by catalytic steam-hydrocarbon reforming with an overall steam-to-carbon molar ratio between 1.5 and 2.4 for the process. The process stream is reacted in at least two prereformers prior to reaction in catalyst-containing tubes in a top-fired reformer furnace. The process stream is reacted adiabatically in the first prereformer, while the process stream is heated prior to being introduced into the second prereformer and/or the second prereformer is heated. The process avoids carbon formation on the catalyst in the catalyst-containing tubes in the primary reformer.
摘要翻译：通过催化蒸汽 - 烃重整制备含氢产物气的方法，该方法的总蒸汽 - 碳摩尔比为1.5-2.4。在顶燃式重整炉中含催化剂的管中反应之前，工艺流在至少两个预重整器中反应。工艺物流在第一预重整器中进行绝热反应，同时在加入第二预重整器和/或第二预重整器之前加热工艺物流。该方法避免了初级重整器中含催化剂的管中催化剂上的碳形成。

8. 发明申请

US20100140553A1 PROCESS AND APPARATUS FOR THE PRODUCTION OF SYNTHESIS GAS 有权
标题翻译：生产合成气的工艺和装置
公开(公告)号：US20100140553A1
公开(公告)日：2010-06-10
申请号：US12704311
申请日：2010-02-11
申请人： Shoou-I Wang , John Repasky , Shankar Nataraj , Xiang-Dong Peng
发明人： Shoou-I Wang , John Repasky , Shankar Nataraj , Xiang-Dong Peng
IPC分类号： C01B3/38 , B01J8/00 , B01J8/06
CPC分类号： C01B3/382 , B01J8/0285 , B01J8/0488 , B01J8/067 , B01J2208/00256 , B01J2208/00504 , B01J2208/0053 , B01J2219/00006 , C01B3/26 , C01B3/36 , C01B3/384 , C01B3/386 , C01B2203/0233 , C01B2203/0244 , C01B2203/0255 , C01B2203/0261 , C01B2203/0283 , C01B2203/06 , C01B2203/061 , C01B2203/062 , C01B2203/0838 , C01B2203/0844 , C01B2203/0877 , C01B2203/1241 , C01B2203/127 , C01B2203/141 , C01B2203/143 , C10J3/02 , C10J3/20 , C10J2300/094 , C10J2300/0976 , C10J2300/0986 , C10K3/026 , Y02E60/324 , Y02P20/52
摘要： Reactive diluent fluid (22) is introduced into a stream of synthesis gas (or “syngas”) produced in a heat-generating unit such as a partial oxidation (“POX”) reactor (12) to cool the syngas and form a mixture of cooled syngas and reactive diluent fluid. Carbon dioxide and/or carbon components and/or hydrogen in the mixture of cooled syngas and reactive diluent fluid is reacted (26) with at least a portion of the reactive diluent fluid in the mixture to produce carbon monoxide-enriched and/or solid carbon depleted syngas which is fed into a secondary reformer unit (30) such as an enhanced heat transfer reformer in a heat exchange reformer process. An advantage of the invention is that problems with the mechanical integrity of the secondary unit arising from the high temperature of the syngas from the heat-generating unit are avoided.
摘要翻译：将反应性稀释剂流体（22）引入在诸如部分氧化（“POX”）反应器（12）的发热单元中产生的合成气（或“合成气”）流中，以冷却合成气，并形成冷却合成气和反应性稀释液。将冷却的合成气和反应性稀释剂流体的混合物中的二氧化碳和/或碳组分和/或氢气与混合物中的至少一部分反应性稀释液反应（26）以产生富含一氧化碳和/或固体碳在热交换重整器方法中将其供入二级重整器单元（30），例如增强的热转移重整器。本发明的一个优点是避免了由来自发热单元的合成气的高温引起的次级单元的机械完整性的问题。

9. 发明授权

US07695708B2 Catalytic steam reforming with recycle 有权
标题翻译：催化蒸汽重整与回收
公开(公告)号：US07695708B2
公开(公告)日：2010-04-13
申请号：US11691039
申请日：2007-03-26
申请人： Xiang-Dong Peng , James Richard O'Leary , Blaine Edward Herb , Krishnakumar Jambunathan
发明人： Xiang-Dong Peng , James Richard O'Leary , Blaine Edward Herb , Krishnakumar Jambunathan
IPC分类号： C01B3/26
CPC分类号： C01B3/382 , C01B3/384 , C01B3/48 , C01B2203/0233 , C01B2203/0283 , C01B2203/04 , C01B2203/0811 , C01B2203/0827 , C01B2203/0883 , C01B2203/0894 , C01B2203/127 , C01B2203/1294 , C01B2203/142 , C01B2203/148
摘要： A method for generating hydrogen in a production facility having a catalytic steam reformer, a boiler downstream of the catalytic steam reformer, optionally having a prereformer, and optionally having a shift reactor, wherein the reformer feed gas mixture is formed using a steam-containing recycle gas mixture which was formed from boiler effluent. The boiler generates steam which may be used to form the reformer feed gas mixture, used elsewhere in the production facility, and/or used for export steam.
摘要翻译：一种在具有催化蒸汽重整器，催化蒸汽重整器下游的锅炉，任选地具有预重整器和任选地具有变换反应器的生产设备中产生氢的方法，其中重整器进料气体混合物是使用含蒸汽的再循环由锅炉废水形成的气体混合物。锅炉产生可用于形成重整器进料气体混合物的蒸汽，其用于生产设备中的其他地方和/或用于出口蒸汽。

10. 发明授权

US07591992B2 Hydrogen production process with regenerant recycle 失效
标题翻译：氢生产过程与再生剂回收
公开(公告)号：US07591992B2
公开(公告)日：2009-09-22
申请号：US11339806
申请日：2006-01-25
申请人： Xiang-Dong Peng , Shankar Nataraj
发明人： Xiang-Dong Peng , Shankar Nataraj
IPC分类号： C07C15/00
CPC分类号： C01B3/38 , B01D53/047 , B01D2253/1124 , B01D2256/16 , B01D2257/30 , B01D2257/302 , B01D2257/502 , B01D2257/504 , B01D2259/40007 , B01D2259/40052 , B01D2259/40056 , B01D2259/404 , C01B3/46 , C01B2203/0233 , C01B2203/0425 , C01B2203/043 , C01B2203/0475 , C01B2203/0485 , C01B2203/0827 , C01B2203/0833 , C01B2203/10 , C01B2203/148 , Y02C10/08 , Y02P20/152
摘要： The present invention relates to a process for producing a hydrogen-containing gas. The process comprises introducing a regeneration gas into a hydrogen reaction vessel containing solid packing material thereby at least partially regenerating the solid packing material and forming an effluent gas from the regeneration gas. At least a portion of the effluent gas is introduced into another hydrogen reaction vessel containing solid packing material. The effluent gas may be used, for example, to purge the other hydrogen reaction vessel and/or regenerate the solid packing material in the other hydrogen reaction vessel. Solid packing materials may include at least one of a complex metal oxide, a steam hydrocarbon reforming catalyst, an oxygen ion conducting ceramic, a hydrocarbon partial oxidation catalyst, and a hydrocarbon cracking catalyst.
摘要翻译：本发明涉及含氢气体的制造方法。该方法包括将再生气体引入含有固体包装材料的氢反应容器中，从而至少部分地再生固体包装材料并形成来自再生气体的流出气体。将至少一部分废气引入含有固体包装材料的另一氢反应容器中。可以使用流出气体，例如清洗另一个氢反应容器和/或再生另一个氢反应容器中的固体填充材料。固体包装材料可以包括复合金属氧化物，蒸汽烃重整催化剂，氧离子导电陶瓷，烃部分氧化催化剂和烃裂化催化剂中的至少一种。

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