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1. 发明授权

US5026720A 1-hydroxyazole compounds and fungicides containing these 失效
标题翻译：含有这些的1-羟基唑化合物和杀真菌剂
公开(公告)号：US5026720A
公开(公告)日：1991-06-25
申请号：US502237
申请日：1990-03-30
申请人： Ulf Baus , Wolfgang Reuther , Gisela Lorenz , Eberhard Ammermann
发明人： Ulf Baus , Wolfgang Reuther , Gisela Lorenz , Eberhard Ammermann
IPC分类号： C07D405/12 , A01N43/56 , A01N43/653 , C07D249/08 , C07D521/00
CPC分类号： C07D231/12 , A01N43/653 , C07D233/56 , C07D249/08
摘要： Compounds of the general formula I ##STR1## where X is alkyl, aryl, aryloxy or alkoxy, Y is hydrogen, alkyl, alkoxy, halogen, aryl or aryloxy, n is 0 to 5, and Z is CH or N, and fungicides containing these compounds.
摘要翻译：其中X为烷基，芳基，芳氧基或烷氧基，Y为氢，烷基，烷氧基，卤素，芳基或芳氧基的通式I（I）化合物，n为0至5，Z为CH或N，和含有这些化合物的杀真菌剂。

2. 发明授权

US5216010A Biocidal N-thiocyanatomethoxyazaheterocycles 失效
标题翻译：生物N-甲基亚氨基四氢叶酸盐
公开(公告)号：US5216010A
公开(公告)日：1993-06-01
申请号：US692728
申请日：1991-04-29
申请人： Wolfgang Reuther , Ulf Baus , Gisela Lorenz
发明人： Wolfgang Reuther , Ulf Baus , Gisela Lorenz
IPC分类号： A01N43/50 , A01N43/52 , A01N43/56 , A01N43/647 , A01N43/653 , A01N47/48 , C07D231/10 , C07D231/12 , C07D231/56 , C07D233/54 , C07D233/56 , C07D235/22 , C07D249/04 , C07D249/08 , C07D249/18 , C07D521/00
CPC分类号： C07D231/12 , A01N43/50 , A01N43/52 , A01N43/56 , A01N43/647 , A01N43/653 , C07D233/56 , C07D235/22 , C07D249/04 , C07D249/08
摘要： N-Thiocyanatomethoxyazaheterocycles of the general formula INCS--CH.sub.2 --O--Het(where Het is pyrazolyl, imidazolyl or triazolyl, each of which may be substituted, or is indazolyl, benzoimidazolyl or benzotriazolyl, where each of the fused benzene rings may furthermore be substituted, and the salts and metal complexes thereof, with the exception of 1-[(thiocyanato)methoxy]-pyrazole, and biocides containing them.
摘要翻译：通式I NCS-CH2-O-Het（其中Het是吡唑基，咪唑基或三唑基，其各自可以被取代）或是吲唑基，苯并咪唑基或苯并三唑基的N-硫代氰基甲氧基加成杂环，其中每个稠合苯环可以进一步为取代的，及其盐和金属络合物，除了1 - [（氰硫基）甲氧基] - 吡唑和含有它们的杀生物剂。

3. 发明授权

US5081142A Derivatives of 1-hydroxy-1,2,4-triazole and fungicides and growth regulators containing them 失效
标题翻译： 1-羟基-1,2,4-三唑和杀真菌剂及其含有生长调节剂的衍生物
公开(公告)号：US5081142A
公开(公告)日：1992-01-14
申请号：US589216
申请日：1990-09-28
申请人： Hubert Sauter , Thomas Zierke , Wolfgang Reuther , Ulf Baus , Gisela Lorenz , Eberhard Ammermann
发明人： Hubert Sauter , Thomas Zierke , Wolfgang Reuther , Ulf Baus , Gisela Lorenz , Eberhard Ammermann
IPC分类号： A01N43/653 , C07D249/08 , C07D401/12 , C07D403/12 , C07D409/12 , C07D413/12 , C07D417/12 , C07D521/00
CPC分类号： C07D231/12 , A01N43/653 , C07D233/56 , C07D249/08
摘要： Compounds of the formula I ##STR1## where Ar is unsubstituted or substituted phenyl, pyridyl, thienyl or napthyl,R.sup.1 is hydrogen or CN,R.sup.2 is unsubstituted or substituted aryl, hetaryl, alkyl or cycloalkyl, or is unsubstituted or substituted alkenyl or alkynyl,x is CH.sub.2, O or S andn is 0 or 1,their plant-tolerated acid addition salts and metal complexes, and fungicides and growth regulators containing these compounds.
摘要翻译：式I的化合物其中Ar是未取代或取代的苯基，吡啶基，噻吩基或萘基，R1是氢或CN，R2是未取代或取代的芳基，杂芳基，烷基或环烷基，或未取代或取代的烯基或炔基，x是CH 2，O或S，n是0或1，它们的植物耐受的酸加成盐和金属络合物，以及含有这些化合物的杀真菌剂和生长调节剂。

4. 发明授权

US4988721A 0-(1,2,4-triazol-1-yl) o-phenyl acetals useful as fungicides 失效
标题翻译： O-（1,2,4-三唑-1-基）邻苯基缩醛可用作杀真菌剂
公开(公告)号：US4988721A
公开(公告)日：1991-01-29
申请号：US477730
申请日：1990-02-09
申请人： Ulf Baus , Wolfgang Reuther , Gisela Lorenz , Eberhard Ammermann
发明人： Ulf Baus , Wolfgang Reuther , Gisela Lorenz , Eberhard Ammermann
IPC分类号： A01N43/653 , C07D249/08 , C07D521/00
CPC分类号： C07D231/12 , A01N43/653 , C07D233/56 , C07D249/08
摘要： Compounds of the general formula ##STR1## where 5 R is alkyl or substituted or unsubstituted aryl,X is C.dbd.O or CHOH and derivatives thereof,Y is hydrogen, alkyl, alkoxy, halogen, aryl or aryloxy, andn is 1 to 5,and fungicides containing these compounds.
摘要翻译：通式为其中5 R为烷基或取代或未取代的芳基的化合物，X为C = O或CHOH及其衍生物，Y为氢，烷基，烷氧基，卤素，芳基或芳氧基，n为1至 5，含有这些化合物的杀真菌剂。

5. 发明授权

US4987143A 1-hydroxy-1,2,4-triazole compounds useful as fungicides 失效
标题翻译：可用作杀真菌剂的1-羟基-1,2,4-三唑化合物
公开(公告)号：US4987143A
公开(公告)日：1991-01-22
申请号：US480143
申请日：1990-02-14
申请人： Ulf Baus , Wolfgang Reuther , Gisela Lorenz , Eberhard Ammermann
发明人： Ulf Baus , Wolfgang Reuther , Gisela Lorenz , Eberhard Ammermann
IPC分类号： A01N43/653 , C07D249/08 , C07D521/00
CPC分类号： C07D231/12 , A01N43/653 , C07D233/56 , C07D249/08
摘要： Compounds of the general formula ##STR1## where X is CH.sub.2 or O, Y is hydrogen, alkyl, alkoxy, halogen, aryl or aryloxy and n is from 1 to 5, and their salts and complexes, and fungicides containing these compounds.
摘要翻译：通式为其中X为CH 2或O，Y为氢，烷基，烷氧基，卤素，芳基或芳氧基且n为1至5的通式为其的化合物及其盐和络合物以及含有这些化合物的杀真菌剂。

6. 发明授权

US4957937A Substituted N-hydroxypyrazoles and fungicides which contain these compounds 失效
标题翻译：含有这些化合物的取代的N-羟基吡唑和杀真菌剂
公开(公告)号：US4957937A
公开(公告)日：1990-09-18
申请号：US478963
申请日：1990-02-12
申请人： Franz Schuetz , Hubert Sauter , Siegbert Brand , Bernd Wenderoth , Ulf Baus , Wolfgang Reuther , Gisela Lorenz , Eberhard Ammermann
发明人： Franz Schuetz , Hubert Sauter , Siegbert Brand , Bernd Wenderoth , Ulf Baus , Wolfgang Reuther , Gisela Lorenz , Eberhard Ammermann
IPC分类号： A01N43/56 , A01N43/58 , C07D231/12 , C07D231/14 , C07D231/16 , C07D231/56 , C07D521/00
CPC分类号： C07D249/08 , A01N43/56 , C07D231/12 , C07D231/14 , C07D231/16 , C07D231/56 , C07D233/56
摘要： Substituted N-hydroxypyrazoles of the general formula ##STR1## where R.sup.1, R.sup.2 and R.sup.3 are identical or different and are hydrogen, alkyl, haloalkyl, cycloalkyl, alkoxycarbonyl, halogen, aryl or arylalkyl, the aromatic ring being unsubstituted or substituted,or R.sup.2 and R.sup.3 form, with the pyrazole ring, a substituted or unsubstituted aromatic or aliphatic ring,X is CH or N, and their plant-tolerated acid addition salts and metal complexes,and fungicides containing these compounds.
摘要翻译：取代的通式为其中R 1，R 2和R 3相同或不同且为氢，烷基，卤代烷基，环烷基，烷氧基羰基，卤素，芳基或芳基烷基的N-取代的N-羟基吡唑，芳环为未取代或取代的，或R 2 和R 3与吡唑环形成取代或未取代的芳族或脂族环，X是CH或N，以及它们的植物耐受的酸加成盐和金属络合物，以及含有这些化合物的杀真菌剂。

7. 发明授权

US5120756A Substituted n-hydroxypyrazoles and n-hydroxy-triazoles for controlling pests 失效
标题翻译：取代的N-羟基吡唑和用于控制PES的N-羟基三唑
公开(公告)号：US5120756A
公开(公告)日：1992-06-09
申请号：US638011
申请日：1991-01-07
申请人： Hans-Juergen Neubauer , Uwe Kardoff , Joachim Leyendecker , Ulf Baus , Christoph Kuenast , Peter Hofmeister , Wolfgang Krieg , Reinhard Kirstgen , Wolfgang Reuther
发明人： Hans-Juergen Neubauer , Uwe Kardoff , Joachim Leyendecker , Ulf Baus , Christoph Kuenast , Peter Hofmeister , Wolfgang Krieg , Reinhard Kirstgen , Wolfgang Reuther
IPC分类号： A01N43/56 , A01N43/653 , C07D231/12 , C07D231/16 , C07D231/18 , C07D249/08 , C07D521/00
CPC分类号： C07D231/12 , A01N43/56 , A01N43/653 , C07D231/16 , C07D233/56 , C07D249/08
摘要： Novel substituted N-hydroxypyrazoles or N-hydroxytriazoles of the general formula I ##STR1## where X and Y are O, S, SO, SO.sub.2 or CH.sub.2, B is N-pyrazolyl or N-1,2,4-triazolyl of the formulae Ba and Bb respectively ##STR2## R.sup.1 and R.sup.2 are hydrogen or C.sub.1 -C.sub.3 -alkyl, R.sup.3 is hydrogen, halogen or C.sub.1 -C.sub.3 -alkyl, z is 1, 2 or 3, R.sup.4, R.sup.5 and R.sup.6 are hydrogen, halogen, C.sub.1 -C.sub.4 -alkyl, C.sub.1 -C.sub.4 -alkoxy, C.sub.1 -C.sub.4 -haloalkyl or C.sub.1 -C.sub.4 -haloalkoxy, and n is 0, 1 or 2, and methods of combating pests.
摘要翻译： B是N-吡唑基或N-1,2,4-三唑基，其中X和Y是O，S，SO，SO 2或CH 2，通式I的新型取代的N-羟基吡唑或N-羟基三唑，式中Ba和Bb分别表示Bb R1和R2是氢或C1-C3-烷基，R3是氢，卤素或C1-C3-烷基，z是1,2或3，R4，R5 R 6为氢，卤素，C 1 -C 4 - 烷基，C 1 -C 4 - 烷氧基，C 1 -C 4卤代烷基或C 1 -C 4卤代烷氧基，n为0,1或2，以及防治害虫的方法。

8. 发明授权

US4945167A Preparation of N-hydroxypyrazoles 失效
标题翻译： N-羟基吡唑的制备
公开(公告)号：US4945167A
公开(公告)日：1990-07-31
申请号：US367047
申请日：1989-06-16
申请人： Ulf Baus , Wolfgang Reuther , Erwin Hahn
发明人： Ulf Baus , Wolfgang Reuther , Erwin Hahn
IPC分类号： C07D231/12 , C07D231/16 , C07D521/00
CPC分类号： C07D231/12 , C07D231/16 , C07D233/56 , C07D249/08
摘要： N-hydroxypyrazoles of the general formula I ##STR1## where R.sup.1, R.sup.2 and R.sup.3 may be identical or different and are each hydrogen or halogen, are prepared by a process in which a pyrazole of the general formula II ##STR2## where R.sup.1, R.sup.2 and R.sup.3 have the meanings stated for formula I, is reacted with an aliphatic or aromatic peroxocarboxylic acid, preferably in the presence of from 0 to 15 moles of an alkali metal hydroxide, alkaline earth metal hydroxide, alkali meteal carbonate or alkaline earth metal carbonate in such a way that the reaction temperature is from -5.degree. C. to 60.degree.C.The reaction can be carried out in water as a solvent or in a 2-phase system consisting of water and an inert organic solvent which is poorly miscible with water, in the presence or absence of a suitable phase transfer catalyst. The peroxocarboxylic acid can be prepared in the reaction mixture before the reaction from H.sub.2 O.sub.2 and an acyl halide or a carboxylic anhydride or can be used in the form of an alkali metal salt or alkaline earth metal salt.
摘要翻译：其中R 1，R 2和R 3可以相同或不同并且各自为氢或卤素的通式I（I）的N-羟基吡唑通过其中通式II的吡唑（IMAGE）（ II）其中R 1，R 2和R 3具有式I所述的含义，与脂族或芳族过氧羧酸反应，优选在0至15摩尔碱金属氢氧化物，碱土金属氢氧化物，碱金属碳酸盐或碱土金属碳酸盐，使得反应温度为-5℃至60℃。该反应可以在作为溶剂的水中或在由水和惰性有机物组成的2相体系中进行在有或没有合适的相转移催化剂的情况下与水很难混溶的溶剂。过氧化羧酸可以在与H 2 O 2和酰卤或羧酸酐反应之前在反应混合物中制备，或者可以以碱金属盐或碱土金属盐的形式使用。

9. 发明授权

US4945166A Preparation of N-hydroxypyrazoles 失效
标题翻译： N-羟基吡唑的制备
公开(公告)号：US4945166A
公开(公告)日：1990-07-31
申请号：US367053
申请日：1989-06-16
申请人： Ulf Baus , Wolfgang Reuther , Rolf Fikentscher
发明人： Ulf Baus , Wolfgang Reuther , Rolf Fikentscher
IPC分类号： C07D231/12 , C07D231/16 , C07D231/54 , C07D231/56 , C07D521/00
CPC分类号： C07D249/08 , C07D231/12 , C07D231/16 , C07D231/56 , C07D233/56
摘要： N-hydroxypyrazoles of the general formula I ##STR1## where R.sup.1, R.sup.2 and R.sup.3 may be identical or different and are each hydrogen, alkyl, halogen or aryl, or R.sup.1 and R.sup.2 or R.sup.2 and R.sup.3 together with the carbon atoms carrying these radicals form an aromatic or nonaromatic ring of 5 or 6 carbon atoms are prepared by a process in which(A) a pyrazole of the general formula II ##STR2## is converted in a conventional manner with an alkali metal hydroxide, alkali metal hydride or alkali metal carbonate into one of its metal salts of the general formula III ##STR3## where ME.sym. is a cation of an alkali metal, and (B) the resulting metal salt of the general formula III is reacted with dibenzoyl peroxide in an inert organic solvent or in a 2-phase system, in the presence or absence of a phase transfer catalyst.
摘要翻译：通式I的N-羟基吡唑（I）其中R 1，R 2和R 3可以相同或不同，各自为氢，烷基，卤素或芳基，或R 1和R 2或R 2和R 3与携带的碳原子一起这些基团形成5或6个碳原子的芳族或非芳族环是通过以下方法制备的：其中（A）通式II的吡唑（II）以常规方式用碱金属氢氧化物，碱金属氢化物或碱金属碳酸盐转化成其通式III（III）的金属盐之一，其中ME（+）是碱金属的阳离子，和（B）所得到的通式III的金属盐是在相转移催化剂存在或不存在下，在惰性有机溶剂或2-相体系中与二苯甲酰基过氧化物反应。

10. 发明授权

US5484938A 1-hydroxyimidazole compounds 失效
标题翻译： 1-羟基咪唑化合物
公开(公告)号：US5484938A
公开(公告)日：1996-01-16
申请号：US800065
申请日：1991-11-27
申请人： Ulf Baus , Wolfgang Reuther
发明人： Ulf Baus , Wolfgang Reuther
IPC分类号： C07D233/54 , C07D233/56 , C07D233/68 , C07D521/00
CPC分类号： C07D233/54 , C07D231/12 , C07D233/56 , C07D233/68 , C07D249/08
摘要： The preparation of 1-hydroxyimidazoles of the formula I ##STR1## where the R radicals can be identical or different and are each halogen or an organic radical, it also being possible for vicinal radicals to be connected to form an aromatic or nonaromatic ring of from 3 to 12 carbon atoms, and n is from 0 to 3, entails reacting an imidazole of the formula II ##STR2## where Q is preferably hydrogen or, especially where R is not halogen, an alkali metal or alkaline earth metal cation, with an organic peroxide.The 1-hydroxyimidazole and its halogen substituted derivatives of the formula I and the acid addition salts thereof are valuable intermediates for organic syntheses.
摘要翻译：制备式I（I）的1-羟基咪唑，其中R基团可以相同或不同，各自为卤素或有机基团，连接基团可连接形成芳族或非芳族化合物 3至12个碳原子的环，n为0至3，使式II（II）的咪唑与Q优选为氢或特别是其中R不是卤素的碱金属或碱土壤金属阳离子，有机过氧化物。式I的1-羟基咪唑及其卤素取代的衍生物及其酸加成盐是有机合成的有价值的中间体。

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