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1. 发明授权

US4945167A Preparation of N-hydroxypyrazoles 失效
标题翻译： N-羟基吡唑的制备
公开(公告)号：US4945167A
公开(公告)日：1990-07-31
申请号：US367047
申请日：1989-06-16
申请人： Ulf Baus , Wolfgang Reuther , Erwin Hahn
发明人： Ulf Baus , Wolfgang Reuther , Erwin Hahn
IPC分类号： C07D231/12 , C07D231/16 , C07D521/00
CPC分类号： C07D231/12 , C07D231/16 , C07D233/56 , C07D249/08
摘要： N-hydroxypyrazoles of the general formula I ##STR1## where R.sup.1, R.sup.2 and R.sup.3 may be identical or different and are each hydrogen or halogen, are prepared by a process in which a pyrazole of the general formula II ##STR2## where R.sup.1, R.sup.2 and R.sup.3 have the meanings stated for formula I, is reacted with an aliphatic or aromatic peroxocarboxylic acid, preferably in the presence of from 0 to 15 moles of an alkali metal hydroxide, alkaline earth metal hydroxide, alkali meteal carbonate or alkaline earth metal carbonate in such a way that the reaction temperature is from -5.degree. C. to 60.degree.C.The reaction can be carried out in water as a solvent or in a 2-phase system consisting of water and an inert organic solvent which is poorly miscible with water, in the presence or absence of a suitable phase transfer catalyst. The peroxocarboxylic acid can be prepared in the reaction mixture before the reaction from H.sub.2 O.sub.2 and an acyl halide or a carboxylic anhydride or can be used in the form of an alkali metal salt or alkaline earth metal salt.
摘要翻译：其中R 1，R 2和R 3可以相同或不同并且各自为氢或卤素的通式I（I）的N-羟基吡唑通过其中通式II的吡唑（IMAGE）（ II）其中R 1，R 2和R 3具有式I所述的含义，与脂族或芳族过氧羧酸反应，优选在0至15摩尔碱金属氢氧化物，碱土金属氢氧化物，碱金属碳酸盐或碱土金属碳酸盐，使得反应温度为-5℃至60℃。该反应可以在作为溶剂的水中或在由水和惰性有机物组成的2相体系中进行在有或没有合适的相转移催化剂的情况下与水很难混溶的溶剂。过氧化羧酸可以在与H 2 O 2和酰卤或羧酸酐反应之前在反应混合物中制备，或者可以以碱金属盐或碱土金属盐的形式使用。

2. 发明授权

US5332830A Preparation of N-hydroxyazoles 失效
标题翻译： N-羟基唑的制备
公开(公告)号：US5332830A
公开(公告)日：1994-07-26
申请号：US37910
申请日：1993-03-26
申请人： Klaus H. von Locquenghien , Wolfgang Hoelderich , Ulf Baus , Wolfgang Reuther , Erwin Hahn
发明人： Klaus H. von Locquenghien , Wolfgang Hoelderich , Ulf Baus , Wolfgang Reuther , Erwin Hahn
IPC分类号： C07D231/12 , C07D233/54 , C07D249/08 , C07D521/00 , C07D233/56
CPC分类号： C07D231/12 , C07D233/56 , C07D249/08
摘要： N-Hydroxyazoles of the general formula I ##STR1## where A is ##STR2## and R.sup.1, R.sup.2 and R.sup.3 are each hydrogen, C.sub.1 -C.sub.4 -alkyl or halogen, are prepared by a process in which an azole of the general formula II ##STR3## where A, R.sup.1, R.sup.2 and R.sup.3 have the abovementioned meanings, is reacted with hydrogen peroxide or an alkyl peroxide in the presence of a zeolite catalyst at from -20.degree. to 150.degree. C. and from 0.1 to 150 bar.
摘要翻译：通式Ⅰ的N-羟基唑（I）其中A是，并且R 1，R 2和R 3各自是氢，C 1 -C 4 - 烷基或卤素，其通过以下方法制备：其中唑其中A，R 1，R 2和R 3具有上述含义的通式II的化合物在沸石催化剂存在下，在-20℃至150℃下与过氧化氢或烷基过氧化物反应。和0.1至150巴。

3. 发明授权

US5382476A Recycling of cured aminoplast resins 失效
标题翻译：固化的氨基塑料树脂的回收
公开(公告)号：US5382476A
公开(公告)日：1995-01-17
申请号：US247184
申请日：1994-05-20
申请人： Juergen Weiser , Wolfgang Reuther , Erwin Hahn
发明人： Juergen Weiser , Wolfgang Reuther , Erwin Hahn
IPC分类号： C08G14/10 , C08J11/16 , C09D161/34 , C14C3/20 , B32B9/04 , C14C9/00
CPC分类号： C08J11/16 , C08G14/10 , C09D161/34 , C14C3/20 , C08J2361/20 , Y02W30/705 , Y10T428/31504 , Y10T428/4935
摘要： Cured aminoplast resins are recycled by a process in which said resins, which may contain fillers, are treated with an aqueous sulfite, hydrogen sulfite or disulfite solution and the resulting low molecular weight degradation products are used in chemical processes. The resulting low molecular weight degradation products of cured aminoplast resins are used for coating moldings, for tanning leather and skins and for the production of moldings which contain cured aminoplast resins or consist thereof.
摘要翻译：固化的氨基塑料树脂通过其中可以含有填料的所述树脂用亚硫酸氢盐，亚硫酸氢盐或二亚硫酸盐溶液处理的方法再循环，并且所得到的低分子量降解产物用于化学方法。所得到的固化的氨基塑料树脂的低分子量降解产物用于涂布模制品，用于鞣制皮革和皮肤，以及用于生产包含固化的氨基塑料树脂或由其组成的模制品。

4. 发明授权

US5393828A Chemical degradation of cured amino resins 失效
标题翻译：固化的氨基树脂的化学降解
公开(公告)号：US5393828A
公开(公告)日：1995-02-28
申请号：US163715
申请日：1993-12-09
申请人： Juergen Weiser , Wolfgang Reuther , Erwin Hahn
发明人： Juergen Weiser , Wolfgang Reuther , Erwin Hahn
IPC分类号： C08J11/28 , C08G63/91
CPC分类号： C08J11/28 , C08J2361/20 , Y02W30/706
摘要： A process for chemically degrading cured amino resins comprises reacting cured amino resins, which may contain fillers, with a primary and/or secondary amine at from 40.degree. to 250.degree. C.
摘要翻译：化学降解固化的氨基树脂的方法包括将可含有填料的固化的氨基树脂与40℃至250℃的伯胺和/或仲胺反应。

5. 发明授权

US5356938A Recycling of cured aminoplast resins 失效
标题翻译：固化的氨基塑料树脂的回收
公开(公告)号：US5356938A
公开(公告)日：1994-10-18
申请号：US196493
申请日：1994-02-15
申请人： Juergen Weiser , Wolfgang Reuther , Erwin Hahn
发明人： Juergen Weiser , Wolfgang Reuther , Erwin Hahn
IPC分类号： C08G14/10 , C08J11/16 , C09D161/34 , C14C3/20 , C08J11/04
CPC分类号： C08J11/16 , C08G14/10 , C09D161/34 , C14C3/20 , C08J2361/20 , Y02W30/705 , Y10T428/31504 , Y10T428/4935
摘要： Cured aminoplast resins are recycled by a process in which said resins, which may contain fillers, are treated with an aqueous sulfite, hydrogen sulfite or disulfite solution and the resulting low molecular weight degradation products are used in chemical processes. The resulting low molecular weight degradation products of cured aminoplast resins are used for coating moldings, for tanning leather and skins and for the production of moldings which contain cured aminoplast resins or consist thereof.
摘要翻译：固化的氨基塑料树脂通过其中可以含有填料的所述树脂用亚硫酸氢盐，亚硫酸氢盐或二亚硫酸盐溶液处理的方法再循环，并且所得到的低分子量降解产物用于化学方法。所得到的固化的氨基塑料树脂的低分子量降解产物用于涂布模制品，用于鞣制皮革和皮肤，以及用于生产包含固化的氨基塑料树脂或由其组成的模制品。

6. 发明授权

US5076808A Dyeing of polyamide substrates with an organic N-nitroso-hydroxylamine as light stabilizer 失效
标题翻译：聚氨酯基质与有机N-硝基羟基胺作为光稳定剂的染色
公开(公告)号：US5076808A
公开(公告)日：1991-12-31
申请号：US623568
申请日：1990-12-07
申请人： Erwin Hahn , Alexander Aumueller , Wolfgang Reuther , Reinhold Krallmann , Dieter Wegerle
发明人： Erwin Hahn , Alexander Aumueller , Wolfgang Reuther , Reinhold Krallmann , Dieter Wegerle
IPC分类号： D06P1/642 , D06P3/24
CPC分类号： D06P1/6422 , D06P3/241 , Y10S8/917 , Y10S8/924
摘要： Polyamide substrates are dyed from aqueous baths with suitable dyes and with copper complexes of organic N-nitrosohydroxylamines as light stabilizers for the dyed polyamide.
摘要翻译：聚酰胺底物用合适的染料和有机N-亚硝基羟胺的铜络合物作为染色聚酰胺的光稳定剂从水浴染色。

7. 发明授权

US5144064A Preparation of J-acid urea 失效
标题翻译：制备J-酸尿素
公开(公告)号：US5144064A
公开(公告)日：1992-09-01
申请号：US764359
申请日：1991-09-23
申请人： Erwin Hahn , Udo Mayer , Friedrich-Wilhelm Raulfs , Ulrike Schloesser
发明人： Erwin Hahn , Udo Mayer , Friedrich-Wilhelm Raulfs , Ulrike Schloesser
IPC分类号： C07C303/22 , C07C309/51
CPC分类号： C07C303/22
摘要： J-Acid urea of the formula ##STR1## is prepared by reacting 7-amino-4-hydroxynaphthalene-2-sulfonic acid (J-acid) with urea at from 100.degree. to 140.degree. C. under a pressure ranging from atmospheric pressure to 10 bar in an inert solvent to a partial extent, precipitating unconverted J-acid in an acidic medium and separating it off, and, if desired, isolating J-acid urea from the resulting neutralized solution by salting out.
摘要翻译：通过使7-氨基-4-羟基萘-2-磺酸（J-酸）与尿素在100-140℃下在大气压至大约压力的压力下反应制备式“IMAGE”的γ-酸尿素 10巴在惰性溶剂中的一部分程度，在酸性介质中沉淀未转化的J-酸，并将其分离出来，如果需要，通过盐析从得到的中和溶液中分离出J-酸尿素。

8. 发明授权

US4846892A Tetrachloroperylene-3,4,9,10-tetracarboxylic acid diimide pigment and its use 失效
标题翻译：四氯化苯-3,4,9,10-四羧酸二酰亚胺颜料及其用途
公开(公告)号：US4846892A
公开(公告)日：1989-07-11
申请号：US92600
申请日：1987-09-03
申请人： Georg Henning , Erwin Hahn , Peter Hauser , Manfred Patsch
发明人： Georg Henning , Erwin Hahn , Peter Hauser , Manfred Patsch
IPC分类号： C08K5/3412 , C08K5/3437 , C09B5/62 , C09B67/48 , C09D7/12 , C09D11/02
CPC分类号： C09B5/62 , C09B67/0025
摘要： A tetrachloroperylene-3,4,9,10-tetracarboxylic acid diimide pigment which contains not less than 85% by weight of the tetrachloro compound of the formula ##STR1## which is present to the extent of not less than 95% by weight in the .beta.-modification and which, in an X-ray spectrum, exhibits 2.sup..crclbar. CuK.sub..alpha. main lines at 9.0.degree., 13.3.degree., 15.0.degree., 16.8.degree., 19.1.degree., 21.5.degree., 24.2.degree., 25.4.degree., 26.5.degree., 27.0.degree. and 27.5.degree..In finishes, the pigment gives very brilliant colorations which are very highly lightfast and fast to weathering and which, upon weathering, neither bleach nor darken up.
摘要翻译：含有不少于85重量％的式“IMAGE”的四氯化合物的四氯化亚丙基-3,4,9,10-四羧酸二酰亚胺颜料，其量为不少于95重量％在9.0°，13.3°，15.0°，16.8°，19.1°，21.5°，24.2度，25.4度，26.5度，X射线谱中显示2（ - ）CuKα主线， 27.0°和27.5°。在表面处理中，颜料产生非常明亮的着色，其具有非常高的耐光性和耐候性，并且在风化时，既不漂白也不变暗。

9. 发明授权

US4694075A Bisazo compounds containing anthranilic acid and thiazole moieties 失效
标题翻译：含有邻氨基苯甲酸和噻唑部分的双偶氮化合物
公开(公告)号：US4694075A
公开(公告)日：1987-09-15
申请号：US820018
申请日：1986-01-21
申请人： Horst Colberg , Erwin Hahn
发明人： Horst Colberg , Erwin Hahn
IPC分类号： C09B44/02 , C09B31/14 , C09B44/08 , D06P1/04 , D06P1/41
CPC分类号： C09B44/02
摘要： The compounds of the formula ##STR1## where Y is hydrogen, chlorine, bromine or nitro, Z is hydrogen, chlorine, bromine, a sulfonic ester group or unsubstituted or substituted sulfamyl, X is --O-- or ##STR2## R is alkylene which may or may not be interrupted by oxygen or ##STR3## m is 0 or 1, p is 1 or 2, R.sup.1 and R.sup.2 independently of one another are each hydrogen, unsubstituted or substituted alkyl, alkenyl, cycloalkyl, aralkyl, or aryl, or R.sup.1 and R.sup.2 together with the nitrogen form a heterocyclic structure, R.sup.3 is hydrogen or unsubstituted or substituted alkyl, R.sup.6 and R.sup.7 independently of one another are each hydrogen, unsubstituted or substituted alkyl, alkoxy or acylamino, K is a radical of a coupling component, A.crclbar. is an anion, R.sup.4 is unsubtituted or substituted alkyl and R.sup.5 is hydrogen or C.sub.1 -C.sub.4 -alkyl, and the radical ##STR4## may furthermore be an unsubstituted or substituted piperazine radical, are useful for dyeing acid-modified fibers, leather and in particular paper.
摘要翻译：其中Y是氢，氯，溴或硝基，Z是氢，氯，溴，磺酸酯基或未取代或取代的亚磺酰基的式“IMAGE”的化合物，X是-O-或R是氧可以或不会被氧中断，或者m为0或1，p为1或2，R 1和R 2彼此独立地为氢，未取代或取代的烷基，烯基，环烷基，芳烷基或芳基，或 R 1和R 2与氮一起形成杂环结构，R 3为氢或未取代或取代的烷基，R 6和R 7彼此独立地为氢，未取代或取代的烷基，烷氧基或酰氨基，K为偶联组分的基团， A（ - ）是阴离子，R4是未取代的或取代的烷基，R5是氢或C1-C4-烷基，基团还可以是未取代或取代的哌嗪基，可用于染色酸改性纤维，皮革，特别是纸张。

10. 发明授权

US4670591A Preparation of N-.alpha.-alkoxyethylformamides 失效
标题翻译：制备N-烷氧基乙酰甲酰胺
公开(公告)号：US4670591A
公开(公告)日：1987-06-02
申请号：US863167
申请日：1986-05-14
申请人： Alfred Oftring , Erwin Hahn , Rolf Fikentscher
发明人： Alfred Oftring , Erwin Hahn , Rolf Fikentscher
IPC分类号： C07C231/00 , C07C233/00 , C07C233/16 , C07C233/18 , C07C103/44 , C07C103/38
CPC分类号： C07C233/00 , C07C233/16
摘要： N-.alpha.-alkoxyethylformamides of the formula ##STR1## where R is C.sub.1 -C.sub.18 -alkyl, are prepared by reacting a vinyl ether of the formulaCH.sub.2 .dbd.CH--OR (II),where R has the meaning stated in the formula I, with formamide in the presence of an acidic or basic catalyst at from -10.degree. to 150.degree. C.
摘要翻译：通过使式CH 2 = CH-OR（II）的乙烯基醚反应制备其中R为C 1 -C 18 - 烷基的通式为其中R为具有如下定义的含义的式（I）的N- 式I化合物与甲酰胺在-10至150℃的酸性或碱性催化剂存在下反应。

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