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    • 7. 发明授权
    • Process for the production of metal oxide and metalloid oxide dispersions
    • 用于生产金属氧化物和类金属氧化物分散体的方法
    • US08529651B2
    • 2013-09-10
    • US12894539
    • 2010-09-30
    • Wolfgang LortzChristoph Batz-SohnGabriele PerletWerner WillGerrit Schneider
    • Wolfgang LortzChristoph Batz-SohnGabriele PerletWerner WillGerrit Schneider
    • B24D3/02C09C1/68C09K3/14C01B33/12
    • C09G1/02C01B13/145C01B33/1417C01F7/026C01P2002/50C01P2006/12C01P2006/22C03C1/006C09K3/1463
    • Process for the production of an aqueous dispersion of pyrogenically produced metal oxide and metalloid oxide powders with a BET surface area of between 5 and 600 m2/g, with a metal oxide or metalloid oxide content in the dispersion of between 5 and 25 wt. %, comprising the following steps: water, which is optionally adjusted to pH values of between 2 and 4 by adding acids, is circulated from a receiving vessel via a rotor/stator machine, and metal oxide or metalloid oxide powder is introduced, using a feed device, into the shear zone between the slots in the rotor teeth and the stator slots, continuously or discontinuously and with the rotor/stator machine running, in a quantity such that a predispersion with a solids content of between 20 and 40 wt. % results, and, after all the metal oxide powder or metalloid oxide powder has been added, the feed device closes and shearing continues in such a way that the shear rate is in the range of between 10000 and 40000 s−1, and then, by dilution, the predispersion is adjusted to the desired solids content of the dispersion while maintaining the dispersing conditions.
    • 制备热解法生产的金属氧化物和类金属氧化物粉末的水性分散体的方法,其BET表面积为5至600m 2 / g,分散体中的金属氧化物或准金属氧化物含量为5至25重量%。 %,包括以下步骤:通过添加酸任选地将pH调节至2至4的水通过转子/定子机从接收容器循环,并引入金属氧化物或准金属氧化物粉末,使用 进料装置连续或不连续地进入转子齿中的狭槽和定子槽之间的剪切区域中,并且转子/定子机器运行,其量使得固体含量为20至40重量%的预分散体。 %的结果,并且在添加了所有的金属氧化物粉末或准金属氧化物粉末之后,进料装置关闭并且剪切继续进行,使得剪切速率在10000和40000s -1之间,然后, 通过稀释,将预分散体调节至分散体的所需固体含量,同时保持分散条件。