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1. 发明申请

US20180127280A1 WATER SOLVATED GLASS/AMORPHOUS SOLID IONIC CONDUCTORS 审中-公开
公开(公告)号：US20180127280A1
公开(公告)日：2018-05-10
申请号：US15868751
申请日：2018-01-11
申请人： Board of Regents, The University of Texas System , Universidade Do Porto , LNEG-LABORATORIO NACIONAL DE ENEGIA E GEOLOGIA
发明人： John B. Goodenough , Maria Helena Sousa Soares De Oliveira Braga , Jose Jorge Do Amaral Ferreira , Preetam Singh
IPC分类号： C01B33/32 , C01D5/02 , H01M10/0562 , H01M8/124 , H01G11/56 , C03C4/18 , C03C1/00 , H01M10/36 , H01G11/62 , H01G11/84 , H01M8/1016 , C01B11/00 , C01B25/30 , C01B25/32 , C01B33/24 , C01F11/46
CPC分类号： C01B33/32 , C01B11/00 , C01B25/306 , C01B25/322 , C01B33/24 , C01D5/02 , C01F11/462 , C03C1/006 , C03C4/18 , H01G11/56 , H01G11/62 , H01G11/84 , H01M8/1016 , H01M8/124 , H01M10/0562 , H01M10/36 , H01M2300/0071 , H01M2300/008 , Y02E60/13 , Y02P70/56 , Y02T10/7022
摘要： The disclosure provides a water-solvated glass/amorphous solid that is an ionic conductor-an electronic insulator, and a dielectric as well as electrochemical devices and processes that use this material, such as batteries, including rechargeable batteries, fuel cells, capacitors, electrolysis cells, and electronic devices. The electrochemical devices and products use a combination of ionic and electronic conduction as well as internal electric dipoles.

2. 发明申请

US20160368777A1 WATER SOLVATED GLASS/AMORPHOUS SOLID IONIC CONDUCTORS 有权
标题翻译：水溶性玻璃/非晶固体离子导体
公开(公告)号：US20160368777A1
公开(公告)日：2016-12-22
申请号：US15178228
申请日：2016-06-09
申请人： Board of Regents, The University of Texas System , Universidade Do Porto , LNEG-LABORATORIO NACIONAL DE ENEGIA E GEOLOGIA
发明人： John B. Goodenough , Maria Helena Sousa Soares De Oliveira Braga , Jose Jorge Do Amaral Ferreira , Preetam Singh
IPC分类号： C01B33/32 , H01M10/36 , H01G11/62 , H01G11/84 , C01B33/24 , C01D5/02 , C01F11/46 , C01B25/30 , C01B25/32 , H01M8/1016 , C01B11/00
CPC分类号： C01B33/32 , C01B11/00 , C01B25/306 , C01B25/322 , C01B33/24 , C01D5/02 , C01F11/462 , C03C1/006 , C03C4/18 , H01G11/56 , H01G11/62 , H01G11/84 , H01M8/1016 , H01M8/124 , H01M10/0562 , H01M10/36 , H01M2300/0071 , H01M2300/008 , Y02E60/13 , Y02P70/56 , Y02T10/7022
摘要： The disclosure provides a water-solvated glass/amorphous solid that is an ionic conductor-an electronic insulator, and a dielectric as well as electrochemical devices and processes that use this material, such as batteries, including rechargeable batteries, fuel cells, capacitors, electrolysis cells, and electronic devices. The electrochemical devices and products use a combination of ionic and electronic conduction as well as internal electric dipoles.
摘要翻译：本公开提供了一种水溶性玻璃/无定形固体，其是离子导体 - 电子绝缘体，以及电介质以及使用该材料的电化学装置和工艺，例如电池，包括可再充电电池，燃料电池，电容器，电解电池和电子设备。电化学装置和产品使用离子和电子传导以及内部电偶极子的组合。

3. 发明申请

US20160368776A1 SPHERICAL SILICON OXYCARBIDE PARTICLE MATERIAL AND MANUFACTURING METHOD THEREOF 审中-公开
标题翻译：球形硅氧烷颗粒材料及其制造方法
公开(公告)号：US20160368776A1
公开(公告)日：2016-12-22
申请号：US15185011
申请日：2016-06-16
申请人： JNC CORPORATION
发明人： Tetsuro KIZAKI , Keizo IWATANI
IPC分类号： C01B31/30 , C10M103/02 , C09K3/14 , C04B35/56 , C04B35/65
CPC分类号： C10M103/02 , C01B32/907 , C01P2004/32 , C01P2004/60 , C01P2004/61 , C01P2004/62 , C03C1/006 , C03C3/045 , C03C12/00 , C04B35/5603 , C04B35/65 , C04B2235/3895 , C04B2235/483 , C08G77/06 , C09K3/1418 , C10M2201/10 , C10N2230/06 , C10N2250/08
摘要： Provided are spherical silicon oxycarbide particle material and manufacturing method thereof, wherein the average particle size is in the range of 0.1-100 μm and having a sphericity of 0.95-1.0.Spherical silicon oxycarbide particle material and manufacturing method thereof are provided as follows. Organotrialkoxysilane is hydrolyzed in a pH 3-6 acetic acid aqueous solution, thereafter an alkaline aqueous solution such as a pH 7-12 ammonia water was added to the obtained hydrolysate. The condensation reaction is performed in an alkaline range to form spherical polysilsesquioxane particles that are spherical silicon oxycarbide precursors that has no melting point or softening point. Sintering was then performed at a sintering temperature of 600-1400° C. under inert atmosphere to obtain spherical silicon oxycarbide particle material.
摘要翻译：球状碳氧化硅颗粒材料及其制造方法如下。有机三烷氧基硅烷在pH 3-6乙酸水溶液中水解，然后向得到的水解产物中加入pH7-12氨水等碱性水溶液。缩合反应在碱性范围内进行以形成球形聚倍半硅氧烷颗粒，其是不具有熔点或软化点的球形碳氧化碳前体。然后在惰性气氛下，在600-1400℃的烧结温度下进行烧结，得到球形碳氧化硅颗粒材料。

4. 发明授权

US09517965B2 Method for preparing a soda-lime-silica glass basic formulation and a method for extracting aluminum from coal ash for co-production of glass 有权
标题翻译：制备钠钙硅玻璃碱性配方的方法以及从煤灰中提取铝用于共同生产玻璃的方法
公开(公告)号：US09517965B2
公开(公告)日：2016-12-13
申请号：US14647739
申请日：2012-11-27
申请人： Shenhua Group Corporation Limited , National Institute of Clean-and-Low-Carbon Energy
发明人： Qi Sun , Lijun Zhao , Baodong Wang , Xiaoting Liu
IPC分类号： C03B5/00 , C03C1/00 , C03C3/087 , C03C3/062 , C03C3/097
CPC分类号： C03C1/002 , C03C1/006 , C03C3/062 , C03C3/087 , C03C3/097
摘要： The present invention discloses a method for preparing a soda-lime-silica glass basic formulation and a method for producing soda-lime-silica glass, comprising the steps of: pre-desiliconizing silicon-containing powdery industrial waste with a sodium hydroxide solution; introducing carbon dioxide for carbonation decomposition, and filtering to obtain a silicic acid precipitate and a sodium carbonate solution; drying the silicic acid precipitate to obtain silicon dioxide; adding lime milk into the filtered sodium carbonate for causticization, and filtering to obtain a sodium hydroxide solution and a calcium carbonate precipitate; drying the calcium carbonate precipitate; using said silicon dioxide and part of the calcium carbonate and adding sodium oxide. The present invention further discloses a method for extracting aluminum from coal ash for co-production of soda lime glass, which uses silicon dioxide obtained from alkali dissolution and desiliconization of coal ash and calcium carbonate generated from causticization as main raw materials. The method for extracting aluminum from coal ash for co-production of soda lime glass according to the present invention integrates and optimizes a process of extracting aluminum from the coal ash, has a high material and energy utilization rate, good quality of co-product glass, and high added value, and can greatly improve economical efficiency of aluminum extraction of coal ash.
摘要翻译：本发明公开了一种制备钠钙石英玻璃碱性配方的方法及其制备方法，其特征在于包括以下步骤：用氢氧化钠溶液预硅化含硅粉末工业废料; 引入二氧化碳进行碳酸化分解，过滤得到硅酸沉淀物和碳酸钠溶液; 干燥硅酸沉淀物，得到二氧化硅; 将白砂糖加入过滤的碳酸钠中进行苛化处理，过滤得到氢氧化钠溶液和碳酸钙沉淀物; 干燥碳酸钙沉淀物; 使用所述二氧化硅和一部分碳酸钙并加入氧化钠。本发明还公开了一种从用于共同生产钠钙玻璃的煤灰中提取铝的方法，该方法使用从碱溶解和硅酸脱硅得到的二氧化硅和由苛性碱生成的碳酸钙作为主要原料。根据本发明的用于共同生产钠钙玻璃的煤灰提取铝的方法整合并优化从煤灰中提取铝的方法，具有高的材料和能量利用率，良品质的共同产品玻璃，附加值高，可大大提高煤灰铝提取的经济效益。

5. 发明授权

US08763430B2 Method for manufacturing grin lens 有权
标题翻译：制造咧嘴透镜的方法
公开(公告)号：US08763430B2
公开(公告)日：2014-07-01
申请号：US13001920
申请日：2008-06-30
申请人： Tomomi Ichinose , Toru Achiwa
发明人： Tomomi Ichinose , Toru Achiwa
IPC分类号： C03B37/016 , C03B37/027 , C03B19/12 , C03C1/00
CPC分类号： C03B37/016 , C03B19/12 , C03B37/027 , C03B2203/26 , C03C1/006 , C03C2201/40 , C03C2201/42 , C03C2203/26
摘要： [Object] In manufacturing a GRIN lens by a sol-gel method, an operation for preparing a wet gel is facilitated and cracking in a base material during sintering and foaming during drawing are prevented.[Solution] The object is achieved by obtaining a GRIN lens by producing a wet gel from an alcohol solution containing a silicon alkoxide, a dopant alkoxide, and a boron alkoxide as the main ingredients, leaching the same, drying the same to form a dry gel, and sintering and drawing the same.
摘要翻译：在通过溶胶 - 凝胶法制造GRIN透镜时，促进制备湿凝胶的操作，并且防止了在烧结期间的基材中的裂纹和拉伸期间的发泡。 [解决方案]通过从含有硅醇盐，掺杂剂醇盐和硼醇盐的醇溶液中生产湿凝胶作为主要成分，通过获得GRIN透镜获得GRIN透镜，浸出，干燥，形成干燥凝胶，烧结和拉丝。

6. 发明授权

US08563620B2 High purity silica monoliths and process for the synthesis thereof 有权
标题翻译：高纯二氧化硅整料及其合成方法
公开(公告)号：US08563620B2
公开(公告)日：2013-10-22
申请号：US13123350
申请日：2009-10-01
申请人： Mohamed Bouazaoui , Bruno Capoen , Hicham El-Hamzaoui , Laurent Bigot , Géraud Bouwmans
发明人： Mohamed Bouazaoui , Bruno Capoen , Hicham El-Hamzaoui , Laurent Bigot , Géraud Bouwmans
IPC分类号： C03B19/12 , C03C3/06
CPC分类号： C03B19/12 , C03B37/016 , C03B2201/04 , C03B2203/42 , C03C1/006 , C03C3/06
摘要： The process for the synthesis of a silica monolith comprises the following steps: hydrolysis of a silicon alkoxide in order to form a hydrolysis precursor followed by a condensation of said hydrolysis precursor in the presence of an organic solvent, in the presence of water and of a basic catalyst in order to form oligomeric clusters containing several silicon atoms; dispersion of said oligomeric clusters in a solution in order to form a sol; polymerization of the sol in order to obtain a gel via a first heat treatment, at a temperature below the boiling point of the constituents of the sol; drying of the gel via a second heat treatment; conversion of the gel to a xerogel via a third heat treatment; dehydration and densification of the xerogel until the silica monolith is obtained via a fourth heat treatment.
摘要翻译：用于合成二氧化硅整料的方法包括以下步骤：水解硅烷醇以形成水解前体，随后在有机溶剂存在下，在水和有机溶剂存在下使所述水解前体缩合碱性催化剂，以形成含有几个硅原子的低聚簇; 将所述低聚簇分散在溶液中以形成溶胶; 在低于溶胶成分的沸点的温度下通过第一热处理获得凝胶的溶胶的聚合; 通过第二次热处理干燥凝胶; 通过第三次热处理将凝胶转化为干凝胶; 干凝胶的脱水和致密化直到通过第四次热处理获得二氧化硅整料。

7. 发明授权

US08552426B2 Composite dielectric material doped with rare earth metal oxide and manufacturing method thereof 失效
标题翻译：掺杂稀土金属氧化物的复合介电材料及其制造方法
公开(公告)号：US08552426B2
公开(公告)日：2013-10-08
申请号：US13848038
申请日：2013-03-20
申请人： National Sun Yat-Sen University
发明人： Hung-Duen Yang , Sudip Mukherjee , Ching-Hsuan Chen
IPC分类号： H01L29/12
CPC分类号： H01L29/12 , B82Y10/00 , B82Y30/00 , B82Y40/00 , C03C1/006 , C03C14/004 , C03C14/006 , C03C2214/16 , H01B3/10 , H01L21/02164 , H01L21/02172 , H01L21/02192 , H01L21/02282
摘要： A composite dielectric material doped with rare earth metal oxide and a manufacturing method thereof are provided. The composite dielectric material is doped with nano-crystalline rare metal oxide which is embedded in silicon dioxide glass matrix, and the composite dielectric material of the nano-crystalline rare metal oxide and the silicon dioxide glass matrix is synthesized by the manufacturing method using sol-gel route. The dielectric value of the glass composite dielectric material is greater than that of pure rare metal oxide or that of silicon dioxide. In presence of magnetic field, the dielectric value of the composite dielectric material is substantially enhanced compared with that of the composite dielectric material at zero field.
摘要翻译：提供掺杂有稀土金属氧化物的复合电介质材料及其制造方法。复合电介质材料掺入纳米二氧化硅玻璃基体中的纳米晶稀土金属氧化物，纳米晶稀土金属氧化物和二氧化硅玻璃基体的复合介电材料采用溶胶 - 凝胶法制备方法合成，凝胶路线。玻璃复合电介质材料的电介质值大于纯稀土金属氧化物或二氧化硅的电介质值。在存在磁场的情况下，复合电介质材料的介电值与零场下的复合电介质的电介质值相比显着提高。

8. 发明申请

US20130224966A1 COMPOSITE DIELECTRIC MATERIAL DOPED WITH RARE EARTH METAL OXIDE AND MANUFACTURING METHOD THEREOF 失效
标题翻译：具有稀土金属氧化物的复合电介质材料及其制造方法
公开(公告)号：US20130224966A1
公开(公告)日：2013-08-29
申请号：US13848026
申请日：2013-03-20
申请人： National Sun Yat-Sen University
发明人： Hung-Duen YANG , Sudip MUKHERJEE , Ching-Hsuan CHEN
IPC分类号： H01L21/02
CPC分类号： H01L29/12 , B82Y10/00 , B82Y30/00 , B82Y40/00 , C03C1/006 , C03C14/004 , C03C14/006 , C03C2214/16 , H01B3/10 , H01L21/02164 , H01L21/02172 , H01L21/02192 , H01L21/02282
摘要： A composite dielectric material doped with rare earth metal oxide and a manufacturing method thereof are provided. The composite dielectric material is doped with nano-crystalline rare metal oxide which is embedded in silicon dioxide glass matrix, and the composite dielectric material of the nano-crystalline rare metal oxide and the silicon dioxide glass matrix is synthesized by the manufacturing method using sol-gel route. The dielectric value of the glass composite dielectric material is greater than that of pure rare metal oxide or that of silicon dioxide. In presence of magnetic field, the dielectric value of the composite dielectric material is substantially enhanced compared with that of the composite dielectric material at zero field.
摘要翻译：提供掺杂有稀土金属氧化物的复合电介质材料及其制造方法。复合电介质材料掺入纳米二氧化硅玻璃基体中的纳米晶稀土金属氧化物，纳米晶稀土金属氧化物和二氧化硅玻璃基体的复合介电材料采用溶胶 - 凝胶法制备方法合成，凝胶路线。玻璃复合电介质材料的电介质值大于纯稀土金属氧化物或二氧化硅的电介质值。在存在磁场的情况下，复合电介质材料的介电值与零场下的复合电介质的电介质值相比显着提高。

9. 发明授权

US08408027B2 Method for the production of a composite body from a basic body of opaque quartz glass and a tight sealing layer 有权
标题翻译：从不透明石英玻璃的基体和密封层制造复合体的方法
公开(公告)号：US08408027B2
公开(公告)日：2013-04-02
申请号：US12452413
申请日：2008-06-18
申请人： Waltraud Werdecker , Johann Leist
发明人： Waltraud Werdecker , Johann Leist
IPC分类号： C03C17/02
CPC分类号： C03C1/006 , C03B19/06 , C03B19/066 , C03B20/00 , C03C1/008 , C03C3/06 , C03C17/02 , C03C2203/22 , C03C2218/11
摘要： To optimize a known method for producing a composite body from a basic body of opaque quartz glass and a dense sealing layer, in such a way that the basic body can be provided with the dense sealing layer without any significant changes and deformations in the opaque material being noticed, the invention suggests a method comprising the following steps: (a) producing the basic body by using a first slip which contains larger amorphous SiO2 particles; (b) providing a second slip which contains smaller amorphous SiO2 particles and the composition of which differs from that of the first slip at least in that it contains SiO2 nanoparticles in the range between 0.2% by wt. to 15% by wt. and which is distinguished by a relatively low vitrification temperature; (d) producing a slip layer from the second slip on a surface of the basic body, drying the slip layer, and (e) subsequently vitrifying the slip layer with formation of the dense sealing layer.
摘要翻译：为了优化用于从不透明石英玻璃和致密密封层的基体制造复合体的已知方法，使得基体可以设置有致密的密封层，而在不透明材料中没有任何显着变化和变形本发明提出了一种方法，包括以下步骤：（a）通过使用包含较大的非晶SiO 2颗粒的第一滑移来生产基体; （b）提供包含较小的非晶SiO 2颗粒的第二滑移，其组成与第一滑移的组成不同，至少其中含有0.2重量％范围内的SiO 2纳米颗粒。至15重量％并且由相对低的玻璃化温度区分; （d）从基体表面上的第二滑移层产生滑动层，干燥滑动层，（e）随后形成致密密封层玻璃化滑动层。

10. 发明授权

US08367769B2 Silicon-based nanosilicon composites and fabrication methods 失效
标题翻译：硅基纳米硅复合材料及其制备方法
公开(公告)号：US08367769B2
公开(公告)日：2013-02-05
申请号：US12707247
申请日：2010-02-17
申请人： Abdullah Saleh Aldwayyan , Mohamad Saleh AlSalhi , Abdurahman Mohammed Aldukhail , Mansour S. Alhoshan , Muhammad Naziruddin Khan , Ghassan K. Al-Chaar , Munir Nayfeh
发明人： Abdullah Saleh Aldwayyan , Mohamad Saleh AlSalhi , Abdurahman Mohammed Aldukhail , Mansour S. Alhoshan , Muhammad Naziruddin Khan , Ghassan K. Al-Chaar , Munir Nayfeh
IPC分类号： C03C14/00 , C09K11/00
CPC分类号： C03B19/12 , C03C1/006 , C03C14/006 , C03C2203/20
摘要： Embodiments of the invention provide silicon-based nanoparticle composites, where the silicon nanoparticles are highly luminescent. Preferred embodiments of the invention are Si—O solid composite networks, e.g., glass, having a homogenous distribution of luminescent hydrogen terminated silicon nanoparticles in a homogenous distribution throughout the solid. Embodiments of the invention also provide fabrication processes for silicon-based silicon nanoparticle composites. A preferred method for forming a silicon-based nanoparticle composite disperses hydrogen terminated silicon nanoparticles and an inorganic precursor of an organosilicon gel in an aprotic solvent to form a sol. A catalyst is mixed into the sol. The sol is then permitted to dry into a gel of the silicon-based nanoparticle composite.
摘要翻译：本发明的实施方案提供硅基纳米颗粒复合物，其中硅纳米颗粒是高度发光的。本发明的优选实施方案是Si-O固体复合网络，例如玻璃，其具有在整个固体中均匀分布的发光氢封端的硅纳米颗粒的均匀分布。本发明的实施方案还提供了硅基硅纳米颗粒复合材料的制造方法。用于形成硅基纳米颗粒复合物的优选方法将氢封端的硅纳米颗粒和有机硅凝胶的无机前体在非质子溶剂中分散以形成溶胶。将催化剂混入溶胶中。然后允许溶胶干燥成硅基纳米颗粒复合物的凝胶。

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