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1. 发明授权

US4812490A Epoxy resin molding compounds 失效
标题翻译：环氧树脂模塑料
公开(公告)号：US4812490A
公开(公告)日：1989-03-14
申请号：US132405
申请日：1987-12-14
申请人： Wolfgang Kleeberg , Heinz Hacker , Jurgen Huber , Dieter Wilhelm , Heinz K. Laupenmuhlen
发明人： Wolfgang Kleeberg , Heinz Hacker , Jurgen Huber , Dieter Wilhelm , Heinz K. Laupenmuhlen
IPC分类号： C07D251/34 , C08G59/00 , C08G59/18 , C08G59/40 , C08G59/50 , C08K3/36 , C08K7/02 , C08L63/00 , H01B3/40 , H01L23/29 , H01L23/31 , C08K7/04
CPC分类号： H01L23/295 , C07D251/34 , C08G59/5086 , C08K3/36 , H01B3/40 , H01L2924/0002
摘要： Molding compounds for encapsulating semiconductor components comprise filler-containing polyepoxy resins and a 1,3,5-tris(3-amino-4-alkylphenyl)-2,4,6-trioxohexahydrotriazine with a C.sub.1 to C.sub.4 alkyl radical as a hardener. The molding compounds are storage-stable and moldings manufactured therefrom meet the requirements for these materials.
摘要翻译：用于封装半导体组分的成型化合物包括含有填料的聚环氧树脂和具有C1至C4烷基作为硬化剂的1,3,5-三（3-氨基-4-烷基苯基）-2,4,6-三氧代六氢三嗪。成型化合物是储存稳定的，由其制造的模制品满足这些材料的要求。

2. 发明授权

US4783345A Method for the manufacture of prepregs and their use 失效
标题翻译：制备预浸料及其用途的方法
公开(公告)号：US4783345A
公开(公告)日：1988-11-08
申请号：US132404
申请日：1987-12-14
申请人： Wolfgang Kleeberg , Heinz Hacker , Jurgen Huber , Dieter Wilhelm
发明人： Wolfgang Kleeberg , Heinz Hacker , Jurgen Huber , Dieter Wilhelm
IPC分类号： C08J5/24 , C08G59/40 , C08G59/50 , H05K1/03 , B05D5/12
CPC分类号： C08G59/5086 , H05K1/0326
摘要： Prepregs can be prepared by impregnating reinforcement materials such as glass, carbon or plastic (in the form of fibers or nonwoven or woven materials) with a solution of a polyepoxy resin and a polyamine as a hardener and subsequent drying. For the manufacture of storage-stable prepregs based on polyepoxy resins, 1,3,5-tris(3-amino-4-alkylphenyl-2,4,6-trioxo-hexahydrotriazine with a C.sub.1 - to C.sub.4 alkyl radical is used as the hardener. The new method leads to storage-stable prepregs and assures that composite materials, especially circuit boards, manufactured therefrom meet the requirements for these materials.
摘要翻译：通过用聚环氧树脂和多胺作为硬化剂的溶液浸渍增强材料如玻璃，碳或塑料（以纤维或非织造材料或编织材料的形式）可以制备预浸料，随后干燥。为了制备基于聚环氧树脂的储存稳定的预浸料，使用具有C1-至C4烷基的1,3,5-三（3-氨基-4-烷基苯基-2,4,6-三氧代六氢三嗪）作为这种新方法导致储存稳定的预浸料，并确保由其制造的复合材料，特别是电路板满足这些材料的要求。

3. 发明授权

US4528358A Method for the manufacture of epoxy resin molding materials 失效
标题翻译：环氧树脂成型材料的制造方法
公开(公告)号：US4528358A
公开(公告)日：1985-07-09
申请号：US635423
申请日：1984-07-30
申请人： Wolfgang Kleeberg , Klaus-Robert Hauschildt , Heinz Hacker , Klaus Kretzschmar
发明人： Wolfgang Kleeberg , Klaus-Robert Hauschildt , Heinz Hacker , Klaus Kretzschmar
IPC分类号： B32B27/12 , B32B27/38 , C08G59/00 , C08G59/40 , C08G59/50 , C08G59/68 , C09D163/00 , H01B3/30 , H01B3/40 , H01B3/42
CPC分类号： H01B3/305 , C08G59/686 , H01B3/40 , H01B3/422
摘要： Molding materials, laminates, stratified material and cover or protective layers which are of high electrical and mechanical quality are formed from polymerisable epoxy compounds if the corss-linking of the epoxy resins is accomplished by anionic polymerisation, using mixed catalysts of tertiary amines of the formula: ##STR1## and an imidazoles of the formula: ##STR2## as a polymerisation catalysts.
摘要翻译：如果通过阴离子聚合实现环氧树脂的连接，则可聚合的环氧化合物由具有高的电学和机械质量的成型材料，层压材料，分层材料和覆盖层或保护层形成，使用式和下式的咪唑：作为聚合催化剂的。

4. 发明授权

US4780360A Method for manufacturing electrical insulating composite materials 失效
标题翻译：电绝缘复合材料的制造方法
公开(公告)号：US4780360A
公开(公告)日：1988-10-25
申请号：US898866
申请日：1986-08-20
申请人： Wolfgang Kleeberg , Klaus-Robert Hauschildt , Heinz Hacker
发明人： Wolfgang Kleeberg , Klaus-Robert Hauschildt , Heinz Hacker
IPC分类号： C08G59/00 , C08G59/50 , C08G59/68 , H01B3/30 , H01B3/40 , H01B3/42 , B32B27/04
CPC分类号： C08G59/686 , H01B3/305 , H01B3/40 , H01B3/422 , Y10T428/2967 , Y10T428/2969 , Y10T428/31511 , Y10T442/2475
摘要： Electrically insulating composite materials formed from (1) epoxy resins and (2) polymeric fiber reinforcement which have high strength are formed if the cross-linking of the epoxy resin is accomplished by anionic polymerization using tertiary amines of the formula ##STR1## as catalyst.
摘要翻译：如果通过使用式“IMAGE”的叔胺作为催化剂的阴离子聚合来实现环氧树脂的交联，则形成由（1）环氧树脂和（2）具有高强度的聚合物纤维增强材料形成的电绝缘复合材料。

5. 发明授权

US4578452A Method for manufacturing epoxy resin molded materials 失效
标题翻译：制备环氧树脂成型材料的方法
公开(公告)号：US4578452A
公开(公告)日：1986-03-25
申请号：US633005
申请日：1984-07-20
申请人： Wolfgang Kleeberg , Klaus-Robert Hauschildt , Heinz Hacker , Klaus Kretzschmar
发明人： Wolfgang Kleeberg , Klaus-Robert Hauschildt , Heinz Hacker , Klaus Kretzschmar
IPC分类号： C08G59/00 , C08G59/22 , C08G59/32 , C08G59/38 , C08G59/42 , C08G59/62 , H01B3/40 , C08G59/24
CPC分类号： C08G59/38 , C08G59/226 , C08G59/32 , C08G59/42 , H01B3/40
摘要： This application relates to methods for the manufacture of leakage current-proof epoxy-resin molded materials from epoxy resin mixture based on di- or polycarboxylic-acid glycidyl esters, di- or polyfunctional cycloaliphatic olefinic epoxides and dicarboxylic-acid anhydrides, carried out in such a manner that molded materials with good mechanical properties are obtained also for parts of large volume. For this purpose, the invention provides that, by means of the experimentally determined time necessary to reach the maximum temperature during the cross-linking of the epoxy resin mixture under quasi adiabatic conditions, the rate of cross-linking of the epoxy resin mixture is adjusted, by the addition of a diol or polyol, to at least as long as the time necessary to reach the maximum temperature during cross-linking of the glycidyl ester/dicarboxylic acid anhydride components.
摘要翻译：本申请涉及从基于二羧酸或多羧酸缩水甘油酯，二官能或多功能脂环族烯烃环氧化物和二羧酸酐的环氧树脂混合物制造防漏电环氧树脂模制材料的方法，对于大体积的部件也可获得具有良好机械性能的成型材料的方式。为此，本发明提供了通过在准绝热条件下环氧树脂混合物交联期间达到最高温度所需的实验确定时间，调节环氧树脂混合物的交联速率通过加入二醇或多元醇至少达到在缩水甘油酯/二羧酸酐组分的交联期间达到最高温度所需的时间。

6. 发明授权

US4072804A Cross-linkable epoxy resin casting compounds 失效
标题翻译：可交联环氧树脂浇注料
公开(公告)号：US4072804A
公开(公告)日：1978-02-07
申请号：US617234
申请日：1975-09-26
申请人： Wolfgang Kleeberg , Heinz Hacker , Klaus-Robert Hauschildt
发明人： Wolfgang Kleeberg , Heinz Hacker , Klaus-Robert Hauschildt
IPC分类号： C08F299/00 , C08F290/00 , C08G59/00 , C08G59/40 , C08G59/42 , H01B3/40
CPC分类号： C08G59/42 , H01B3/40
摘要： The invention provides epoxy resin casting compounds based on polyepoxides, polycarboxylic acids and/or polycarboxylic acid anhydrides with directly or latently present carboxyl functions, which can be converted by polyaddition and/or polymerization into insoluble and unmeltable cross-linked polymers. According to the invention, the carboxyl functions are replaced, at least partially, by maleic acid monoallyl ester and a polymerization-initiating radical former, the maleic acid monoallyl ester component being present in the reaction mixture in free form and/or in the form of adducts to the polyepoxide. The epoxy resin casting compounds constitute systems which can be processed in a wide temperature range and are cross-linked rapidly at elevated temperature.
摘要翻译：本发明提供了基于聚环氧化物，多元羧酸和/或具有直接或间接存在的羧基官能团的多元羧酸酐的环氧树脂浇铸化合物，其可以通过加聚和/或聚合转化成不可溶和不可熔的交联聚合物。根据本发明，羧基官能团至少部分地由马来酸单烯丙酯和聚合引发基团原子取代基取代，马来酸单烯丙基酯组分以游离形式存在于反应混合物中，和/或以加成到聚环氧化物。环氧树脂浇铸化合物构成可在宽温度范围内加工并在高温下快速交联的体系。

7. 发明授权

US3957512A Method for the preparation of relief structures 失效
标题翻译：浮雕结构的制备方法
公开(公告)号：US3957512A
公开(公告)日：1976-05-18
申请号：US444552
申请日：1974-02-21
申请人： Wolfgang Kleeberg , Roland Rubner , Wieland Bartel
发明人： Wolfgang Kleeberg , Roland Rubner , Wieland Bartel
IPC分类号： C07C255/34 , C08F290/00 , C08F299/00 , C08G18/67 , C08G73/00 , C08G73/10 , G03F7/004 , G03F7/038 , G03C1/68 , G03C5/00
CPC分类号： C07C255/00 , G03F7/0387
摘要： Novel cyclic monomers leaving two functional groups capable of undergoing condensation reactions to form amide, urea or urethane linkages and at least one photo or radiation-reactive group are condensed with cyclic comonomers to form a soluble, substantially-linear condensation pre-polymer. A solution of the prepolymer is applied to a substrate and the solution is evaporated off to form a film or foil. The photo or radiation-sensitive layer or foil is exposed or irradiated through a pattern, the unexposed or unirradiated part is dissolved or stripped off, and the relief structure which remains is annealed if necessary. The relief structures obtained are distinguished particularly by the sharpness of their edges, good mechanical and chemical properties as well as good insulating properties. They are suited particularly for the preparation of miniaturized insulating layers.
摘要翻译：留下两个能够进行缩合反应以形成酰胺，脲或氨基甲酸酯键和至少一个光或反应性基团的官能团的新型环状单体与环状共聚单体缩合形成可溶的基本上线性的缩合预聚物。将预聚物的溶液施加到基材上，蒸发溶液以形成膜或箔。照片或辐射敏感层或箔通过图案曝光或照射，未曝光或未照射部分被溶解或剥离，并且如果需要，保留的浮雕结构退火。获得的浮雕结构的特征在于其边缘的锐度，良好的机械和化学性质以及良好的绝缘性能。它们特别适用于制备小型化绝缘层。

8. 发明授权

US3936523A Method for the manufacture of elongated material particularly electric cable and wire 失效
标题翻译：用于制造细长材料，特别是电缆和电线的方法
公开(公告)号：US3936523A
公开(公告)日：1976-02-03
申请号：US444100
申请日：1974-02-20
申请人： Wolfgang Kleeberg , Rudolf Wiedenmann , Helmut Ahne
发明人： Wolfgang Kleeberg , Rudolf Wiedenmann , Helmut Ahne
IPC分类号： C08K5/3492 , H01B3/30 , H01B3/44 , B29C25/00
CPC分类号： H01B3/441 , C08K5/34 , C08K5/3492 , H01B3/308
摘要： In a method for the manufacture of formed elongated articles of cross-linked polyethylene in which the polyethylene is shaped in the non-cross-linked condition and is subsequently cross-linked by the application of heat in the presence of organic radical-forming agents, the improvement wherein 0.1 to 20% by weight of polyethylene of a cross-link promoting coagent selected from the group consisting of 2,4-dienoxy-6-amino-alkyl(ene)-s-triazines and N,N'-bis-(2,4-dienoxy-s-triazine-6)-diamines, is admixed with the polyethylene and is thereafter shaped and continuously cross-linked by application of heating at about atmospheric pressure and at a temperature above about 150.degree.C. and below the decomposition temperature of the components of the mixture.
摘要翻译：在制造交联聚乙烯的成形细长制品的方法中，其中聚乙烯成型为非交联状态，随后在有机自由基形成剂存在下通过加热进行交联，改进的是其中0.1-20重量％的交联促进助剂的聚乙烯选自2,4-二烯氧基-6-氨基 - 烷基（烯） - - 三嗪和N，N'-双 - （2,4-二烯氧基-s-三嗪-6） - 二胺与聚乙烯混合，然后通过在约大气压和高于约150℃及以下的温度下加热而成形并连续交联混合物组分的分解温度。

9. 发明授权

US4131600A Hot-hardening reaction resin mixture for impregnating the insulation of electrical equipment and for the manufacture of molded materials with or without inserts 失效
标题翻译：热硬化反应树脂混合物，用于浸渍电气设备的绝缘和用于制造具有或不具有插入件的模制材料
公开(公告)号：US4131600A
公开(公告)日：1978-12-26
申请号：US856490
申请日：1977-12-01
申请人： Walter Ihlein , Wolfgang Kleeberg , Helmuth Markert , Willi Mertens
发明人： Walter Ihlein , Wolfgang Kleeberg , Helmuth Markert , Willi Mertens
IPC分类号： C08G18/00 , C08G18/18 , C08G18/58 , C08G59/40 , C08G59/72 , C09D5/25 , H01B3/30 , H01B3/40 , H02K3/30 , C08G59/18
CPC分类号： H01B3/40 , C08G18/003 , C08G18/18 , C08G59/4028 , C08G59/72 , H01B3/303 , H02K3/30
摘要： Addition complexes of tertiary amines and boron trichloride of the general formula BCl.sub.3.NR.sub. 1 R.sub.2 R.sub. 3 are used as an accelerator system for a heat-curing reaction resin mixture of purified polyisocyanate and polyepoxy resin compounds. Insulation impregnated with this reaction resin mixture exhibits high thermal stability in the hardened condition and can be used at high operating temperatures.
摘要翻译：使用通式BCl3.NR 1R2R3的叔胺和三氯化硼的加成络合物作为纯化的多异氰酸酯和聚环氧树脂化合物的热固化反应树脂混合物的加速剂体系。用该反应树脂混合物浸渍的绝缘体在硬化条件下表现出高的热稳定性，并且可以在高操作温度下使用。

10. 发明授权

US4729906A Method for producing glow polymerisate layers 失效
标题翻译：产生辉光聚合物层的方法
公开(公告)号：US4729906A
公开(公告)日：1988-03-08
申请号：US824937
申请日：1986-01-31
申请人： Wolfgang Kleeberg , Johann Kammermaier , Gerhard Rittmayer , Rolf-Winfried Schulte
发明人： Wolfgang Kleeberg , Johann Kammermaier , Gerhard Rittmayer , Rolf-Winfried Schulte
IPC分类号： C08F2/00 , B05D3/14 , B05D7/24 , C08F2/46 , C08F2/52 , C08F114/26 , C08G85/00 , C08J7/04 , C23C14/12 , B05D3/06
CPC分类号： B05D1/62 , C08F114/26 , C08F2/52 , B05D2506/10
摘要： Glow polymerisate layers can be generated on a substrate, starting from hydrocarbons and/or fluorocarbons, by means of a high-frequency, low-pressure glow discharge. Glow polymerisates completely saturated with hydrogen or fluorine are obtained when the glow discharge is carried out in the microwave range between 0.5 and 1.000 GHz and if the amplitude E.sub.0 of the effective field strength in the vicinity of the substrate no greater than 850 V/cm.
摘要翻译：辉光聚合物层可以通过高频低压辉光放电从烃和/或碳氟化合物开始在基底上产生。当在0.5〜1.000GHz的微波范围内进行辉光放电时，如果衬底附近的有效场强的振幅E0不大于850V / cm，则获得完全饱和的氢或氟的辉光聚合物。

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