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1. 发明授权

US08067652B2 Processes for controlling the viscosity of polyalphaolefins 有权
标题翻译：控制聚α-烯烃粘度的方法
公开(公告)号：US08067652B2
公开(公告)日：2011-11-29
申请号：US12540974
申请日：2009-08-13
申请人： Willie C. Bburton , E. Brian Fox
发明人： Willie C. Bburton , E. Brian Fox
IPC分类号： C07C2/08 , C08F4/6592
CPC分类号： C08F110/14 , C08F4/65908 , C08F4/65912 , C08F10/14 , C10M107/10 , C10M2205/0285 , C10N2220/022 , C10N2270/00 , Y10S526/943 , C08F4/65927 , C08F2500/17
摘要： The invention relates to a process for forming a polyalphaolefin, the process comprising the step of polymerizing at least one C8-C12 monomer, preferably a decene such as 1-decene, in the presence of an aluminoxane, an activator and a metallocene to form the polyalphaolefin, wherein the molar ratio of the aluminoxane to the metallocene is less than 250:1. The invention also relates to a process for forming a polyalphaolefin having a desired kinematic viscosity from at least one monomer in the presence of an aluminoxane, an organoboron compound and a metallocene. The process comprises the steps of, inter alia, providing a correlation between (i) the molar ratio of the aluminoxane to at least one of the organoboron compound and the metallocene, and (ii) the kinematic viscosity of the polyalphaolefin to form polyalphaolefins having predictable viscosities.
摘要翻译：本发明涉及形成聚α-烯烃的方法，该方法包括在铝氧烷，活化剂和金属茂存在下聚合至少一种C 8 -C 12单体，优选癸烯如1-癸烯的步骤，以形成聚α-烯烃，其中铝氧烷与茂金属的摩尔比小于250:1。本发明还涉及在铝氧烷，有机硼化合物和茂金属存在下形成具有来自至少一种单体的所需运动粘度的聚α-烯烃的方法。该方法特别包括以下步骤：（i）铝氧烷与至少一种有机硼化合物与茂金属的摩尔比之间的相关性，和（ii）聚α-烯烃的运动粘度以形成具有可预测性的聚α-烯烃粘度。

2. 发明申请

US20110092752A1 Polyalphaolefins and processes for forming polyalphaolefins 有权
公开(公告)号：US20110092752A1
公开(公告)日：2011-04-21
申请号：US12928752
申请日：2010-12-17
申请人： Daniel C. Knowles , Jesus R. Fabian , Vilan Kosover , Susan Ferrarotti , E. Brian Fox , Frank DeBlase
发明人： Daniel C. Knowles , Jesus R. Fabian , Vilan Kosover , Susan Ferrarotti , E. Brian Fox , Frank DeBlase
IPC分类号： C07C9/22
CPC分类号： C08F6/003 , B01J8/20 , B01J2208/00283 , C08F4/65912 , C08F6/02 , C08F10/14 , C08F110/14 , C08L23/18 , C08F2/02 , C08F2/06 , C08F4/65927 , C08F2500/02 , C08F2500/17 , C08F2500/03 , C08F2500/15
摘要： The invention is directed to polyalphaolefins (PAOs) and processes for forming PAOs. In one embodiment, the invention is to a process for forming a PAO comprising polymerizing C8-C12 α-olefin monomers in the presence of hydrogen, a C8-C12 saturated hydrocarbon, e.g., a C8-C12 saturated straight-chain hydrocarbon, and a catalyst system in a reaction vessel, wherein the C8-C12 saturated straight-chain hydrocarbon has about the same number of carbon atoms as the C8-C12 α-olefin monomers. The C8-C12 saturated straight-chain hydrocarbon optionally is derived from a crude PAO product formed by the process of the invention. The invention is also directed to reaction systems for performing the processes of the invention, to processes for controlling PAO viscosity based on residence time, and to the removal of spent catalyst using a solid adsorbent particles.

3. 发明授权

US08389780B2 Polyalphaolefins and processes for forming polyalphaolefins 有权
标题翻译：聚α-烯烃和形成聚α-烯烃的方法
公开(公告)号：US08389780B2
公开(公告)日：2013-03-05
申请号：US12928752
申请日：2010-12-17
申请人： Daniel C. Knowles , Jesus R. Fabian , Vilan Kosover , Susan Ferrarotti , E. Brian Fox , Frank DeBlase
发明人： Daniel C. Knowles , Jesus R. Fabian , Vilan Kosover , Susan Ferrarotti , E. Brian Fox , Frank DeBlase
IPC分类号： C07C9/22 , C10M107/02
CPC分类号： C08F6/003 , B01J8/20 , B01J2208/00283 , C08F4/65912 , C08F6/02 , C08F10/14 , C08F110/14 , C08L23/18 , C08F2/02 , C08F2/06 , C08F4/65927 , C08F2500/02 , C08F2500/17 , C08F2500/03 , C08F2500/15
摘要： The invention is directed to polyalphaolefins (PAOs) and processes for forming PAOs. In one embodiment, the invention is to a process for forming a PAO comprising polymerizing C8-C12 α-olefin monomers in the presence of hydrogen, a C8-C12 saturated hydrocarbon, e.g., a C8-C12 saturated straight-chain hydrocarbon, and a catalyst system in a reaction vessel, wherein the C8-C12 saturated straight-chain hydrocarbon has about the same number of carbon atoms as the C8-C12 α-olefin monomers. The C8-C12 saturated straight-chain hydrocarbon optionally is derived from a crude PAO product formed by the process of the invention. The invention is also directed to reaction systems for performing the processes of the invention, to processes for controlling PAO viscosity based on residence time, and to the removal of spent catalyst using a solid adsorbent particles.
摘要翻译：本发明涉及聚α-烯烃（PAO）和形成PAO的方法。在一个实施方案中，本发明涉及形成PAO的方法，该方法包括在氢气，C8-C12饱和烃如C8-C12饱和直链烃存在下聚合C8-C12α-烯烃单体，和催化剂体系，其中C8-C12饱和直链烃具有与C 8 -C 12α-烯烃单体大致相同数量的碳原子。 C8-C12饱和直链烃任选地衍生自通过本发明的方法形成的粗制PAO产物。本发明还涉及用于执行本发明方法的反应系统，基于停留时间控制PAO粘度的方法，以及使用固体吸附剂颗粒除去废催化剂。

4. 发明授权

US07880047B2 Polyalphaolefins and processes for forming polyalphaolefins 有权
标题翻译：聚α-烯烃和形成聚α-烯烃的方法
公开(公告)号：US07880047B2
公开(公告)日：2011-02-01
申请号：US12116147
申请日：2008-05-06
申请人： Daniel C. Knowles , Jesus R. Fabian , Vilen Vilan Kosover , Susan Ferrarotti , E. Brian Fox , Frank DeBlase
发明人： Daniel C. Knowles , Jesus R. Fabian , Vilen Vilan Kosover , Susan Ferrarotti , E. Brian Fox , Frank DeBlase
IPC分类号： C07C2/02
CPC分类号： C08F6/003 , B01J8/20 , B01J2208/00283 , C08F4/65912 , C08F6/02 , C08F10/14 , C08F110/14 , C08L23/18 , C08F2/02 , C08F2/06 , C08F4/65927 , C08F2500/02 , C08F2500/17 , C08F2500/03 , C08F2500/15
摘要： The invention is directed to polyalphaolefins (PAOs) and processes for forming PAOs. In one embodiment, the invention is to a process for forming a PAO comprising polymerizing C8-C12 α-olefin monomers in the presence of hydrogen, a C8-C12 saturated hydrocarbon, e.g., a C8-C12 saturated straight-chain hydrocarbon, and a catalyst system in a reaction vessel, wherein the C8-C12 saturated straight-chain hydrocarbon has about the same number of carbon atoms as the C8-C12 α-olefin monomers. The C8-C12 saturated straight-chain hydrocarbon optionally is derived from a crude PAO product formed by the process of the invention. The invention is also directed to reaction systems for performing the processes of the invention, to processes for controlling PAO viscosity based on residence time, and to the removal of spent catalyst using a solid adsorbent particles.
摘要翻译：本发明涉及聚α-烯烃（PAO）和形成PAO的方法。在一个实施方案中，本发明涉及形成PAO的方法，该方法包括在氢气，C8-C12饱和烃如C8-C12饱和直链烃存在下聚合C8-C12α-烯烃单体，和催化剂体系，其中C8-C12饱和直链烃具有与C 8 -C 12α-烯烃单体大致相同数量的碳原子。 C8-C12饱和直链烃任选地衍生自通过本发明的方法形成的粗制PAO产物。本发明还涉及用于执行本发明方法的反应系统，基于停留时间控制PAO粘度的方法，以及使用固体吸附剂颗粒除去废催化剂。

5. 发明授权

US07312346B2 Method of purifying hydroxyalkyl amide 失效
标题翻译：羟烷基酰胺的纯化方法
公开(公告)号：US07312346B2
公开(公告)日：2007-12-25
申请号：US10712830
申请日：2003-11-12
申请人： Timothy L. Lambert , E. Brian Fox
发明人： Timothy L. Lambert , E. Brian Fox
IPC分类号： C11C3/00
CPC分类号： C10L10/08 , C07C231/24 , C10L1/224 , C07C233/18 , C07C233/20
摘要： A method for purifying hydroxyalkyl amide of residual alkanolamine by using nonpolar solvent, an acidic pH, salt solutions and an elevated temperature.
摘要翻译：通过使用非极性溶剂，酸性pH，盐溶液和升高的温度来纯化残余链烷醇胺的羟烷基酰胺的方法。

6. 发明授权

US07244857B2 Method of making hydroxyalkyl amide containing reduced level of unreacted alkanolamine 有权
标题翻译：制备含有降低水平的未反应的链烷醇胺的羟烷基酰胺的方法
公开(公告)号：US07244857B2
公开(公告)日：2007-07-17
申请号：US10713805
申请日：2003-11-14
申请人： E. Brian Fox , Timothy L. Lambert
发明人： E. Brian Fox , Timothy L. Lambert
IPC分类号： C07C231/00
CPC分类号： C07B43/06 , C07C231/02 , C10L1/221 , C10L1/224 , C10L10/08 , C07C233/18
摘要： A method for reacting alkanolamine with ester in the presence of a metal silicate compound and, optionally, a catalyst, to produce a hydroxyalkyl amide composition with a decreased level of alkanolamine and residual catalyst.
摘要翻译：在金属硅酸盐化合物和任选的催化剂的存在下使链烷醇胺与酯反应的方法，以产生具有降低的链烷醇胺和残余催化剂水平的羟烷基酰胺组合物。

7. 发明授权

US07943807B2 Controlling branch level and viscosity of polyalphaolefins with propene addition 有权
标题翻译：用丙烯添加控制聚α-烯烃的分支水平和粘度
公开(公告)号：US07943807B2
公开(公告)日：2011-05-17
申请号：US12026981
申请日：2008-02-06
申请人： Willie Charles Burton , E. Brian Fox
发明人： Willie Charles Burton , E. Brian Fox
IPC分类号： C07C9/22 , C07C2/30 , C07C2/34 , C08F4/6592 , C08F210/06 , C08F210/14
CPC分类号： C10M143/08 , C08F4/65908 , C08F4/65912 , C08F10/14 , C08F110/14 , C08F210/14 , C10M2205/02 , C10M2205/024 , C10N2220/028 , C10N2230/02 , Y10S526/943 , C08F2/38 , C08F4/65927 , C08F2500/17 , C08F2500/03 , C08F210/06 , C10M2205/028
摘要： The invention relates to a polyalphaolefin formed from a decene and propene and having a branch level greater than 19% and to a process for forming such polyalphaolefins. The invention also relates to a process for forming a polyalphaolefin from at least two monomers, the two monomers comprising a decene and propene, the process comprising the steps of, inter alia, providing a correlation between the total amount of propene used to form the polyalphaolefin and at least one of branch level or viscosity of the polyalphaolefin to make polyalphaolefins comprising decene and propene with predictable branch levels and viscosities.
摘要翻译：本发明涉及由癸烯和丙烯形成并具有大于19％的分支水平的聚α-烯烃以及形成这种聚α-烯烃的方法。本发明还涉及从至少两种单体形成聚α-烯烃的方法，所述两种单体包含癸烯和丙烯，所述方法包括以下步骤：提供用于形成聚α-烯烃的丙烯的总量之间的相关性以及聚α-烯烃的分枝水平或粘度中的至少一种，以制备包含癸烯和丙烯的聚α-烯烃，具有可预测的分支水平和粘度。

8. 发明申请

US20090281360A1 POLYALPHAOLEFINS AND PROCESSES FOR FORMING POLYALPHAOLEFINS 有权
标题翻译：聚对苯二甲酸丁二醇酯的制备及其制备方法
公开(公告)号：US20090281360A1
公开(公告)日：2009-11-12
申请号：US12116147
申请日：2008-05-06
申请人： Daniel C. Knowles , Jesus R. Fabian , Vilen Kosover , Susan Ferrarotti , E. Brian Fox
发明人： Daniel C. Knowles , Jesus R. Fabian , Vilen Kosover , Susan Ferrarotti , E. Brian Fox
IPC分类号： C07C2/02 , B01J19/00
CPC分类号： C08F6/003 , B01J8/20 , B01J2208/00283 , C08F4/65912 , C08F6/02 , C08F10/14 , C08F110/14 , C08L23/18 , C08F2/02 , C08F2/06 , C08F4/65927 , C08F2500/02 , C08F2500/17 , C08F2500/03 , C08F2500/15
摘要： The invention is directed to polyalphaolefins (PAOs) and processes for forming PAOs. In one embodiment, the invention is to a process for forming a PAO comprising polymerizing C8-C12 α-olefin monomers in the presence of hydrogen, a C8-C12 saturated hydrocarbon, e.g., a C8-C12 saturated straight-chain hydrocarbon, and a catalyst system in a reaction vessel, wherein the C8-C12 saturated straight-chain hydrocarbon has about the same number of carbon atoms as the C8-C12 α-olefin monomers. The C8-C12 saturated straight-chain hydrocarbon optionally is derived from a crude PAO product formed by the process of the invention. The invention is also directed to reaction systems for performing the processes of the invention, to processes for controlling PAO viscosity based on residence time, and to the removal of spent catalyst using a solid adsorbent particles.
摘要翻译：本发明涉及聚α-烯烃（PAO）和形成PAO的方法。在一个实施方案中，本发明涉及一种形成PAO的方法，包括在氢存在下使C8-C12α-烯烃单体聚合，C8-C12饱和烃，例如C8-C12饱和直链烃和催化剂体系，其中C8-C12饱和直链烃具有与C 8 -C 12α-烯烃单体大约相同数量的碳原子。 C8-C12饱和直链烃任选地衍生自通过本发明的方法形成的粗制PAO产物。本发明还涉及用于执行本发明方法的反应系统，基于停留时间控制PAO粘度的方法，以及使用固体吸附剂颗粒除去废催化剂。

9. 发明申请

US20090198089A1 CONTROLLING BRANCH LEVEL AND VISCOSITY OF POLYALPHAOLEFINS WITH PROPENE ADDITION 有权
标题翻译：用丙酮添加剂控制分散体水平和粘度
公开(公告)号：US20090198089A1
公开(公告)日：2009-08-06
申请号：US12026981
申请日：2008-02-06
申请人： Willie C. Burton , E. Brian Fox
发明人： Willie C. Burton , E. Brian Fox
IPC分类号： C07C9/16 , C07C2/02
CPC分类号： C10M143/08 , C08F4/65908 , C08F4/65912 , C08F10/14 , C08F110/14 , C08F210/14 , C10M2205/02 , C10M2205/024 , C10N2220/028 , C10N2230/02 , Y10S526/943 , C08F2/38 , C08F4/65927 , C08F2500/17 , C08F2500/03 , C08F210/06 , C10M2205/028
摘要： The invention relates to a polyalphaolefin formed from a decene and propene and having a branch level greater than 19% and to a process for forming such polyalphaolefins. The invention also relates to a process for forming a polyalphaolefin from at least two monomers, the two monomers comprising a decene and propene, the process comprising the steps of, inter alia, providing a correlation between the total amount of propene used to form the polyalphaolefin and at least one of branch level or viscosity of the polyalphaolefin to make polyalphaolefins comprising decene and propene with predictable branch levels and viscosities.
摘要翻译：本发明涉及由癸烯和丙烯形成并具有大于19％的分支水平的聚α-烯烃以及形成这种聚α-烯烃的方法。本发明还涉及从至少两种单体形成聚α-烯烃的方法，所述两种单体包含癸烯和丙烯，所述方法包括以下步骤：提供用于形成聚α-烯烃的丙烯的总量之间的相关性以及聚α-烯烃的分枝水平或粘度中的至少一种，以制备包含癸烯和丙烯的聚α-烯烃，具有可预测的分支水平和粘度。

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