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1. 发明授权

US07713407B2 Production of low sulfur fuels using improved hydrocracker post-treatment catalyst 有权
标题翻译：使用改进的加氢裂化器后处理催化剂生产低硫燃料
公开(公告)号：US07713407B2
公开(公告)日：2010-05-11
申请号：US11446251
申请日：2006-06-02
申请人： William J. Tracy, III , Chuansheng Bai , Robert A. Bradway , William E. Lewis , Randolph J. Smiley
发明人： William J. Tracy, III , Chuansheng Bai , Robert A. Bradway , William E. Lewis , Randolph J. Smiley
IPC分类号： C10G65/00 , C10G69/00
CPC分类号： C10G65/12 , B01J23/883 , B01J23/8885 , B01J31/10 , C10G45/08
摘要： A hydrocracking process for converting a petroleum feedstock to higher gravity, lower sulfur products, especially ultra low sulfur road diesel fuel. The process may be operated as a single-stage or two-stage hydrocracking. In each case, a hydrocracking step is followed directly by a post-treat hydrodesulfurization zone using a bulk multimetallic catalyst comprised of at least one Group VIII non-noble metal and at least two Group VIB metals with a ratio of Group VIB metal to Group VIII non-noble metal is from about 10:1 to about 1:10. In the two-stage option with interstage ammonia removal, the initial hydrocracking step may be followed by hydrodesulfurization using the bulk multimetallic catalyst prior to the ammonia removal which is followed by the second hydrocracking step. A final hydrodesulfurization over the bulk multimetallic catalyst may follow. The hydrodesulfurization over the bulk multimetallic catalyst is carried out at a pressure of at least 25 barg and preferably at least 40 barg.
摘要翻译：用于将石油原料转化为更高重力，较低硫产物，特别是超低硫道路柴油的加氢裂化方法。该方法可以作为单级或两级加氢裂化来操作。在每种情况下，加氢裂化步骤直接通过后处理加氢脱硫区，使用由至少一种VIII族非贵金属和至少两种VIB族金属与VIII族的VIB族金属组成的本体多金属催化剂非贵金属为约10:1至约1:10。在阶段氨除去的两阶段选择中，初始加氢裂化步骤之后可以在除氨之前使用大量多金属催化剂进行加氢脱硫，其后是第二加氢裂化步骤。可以遵循大量多金属催化剂的最终加氢脱硫。本体多金属催化剂上的加氢脱硫在至少25barg，优选至少40barg的压力下进行。

2. 发明申请

US20070278135A1 Hydrocracker post-treat catalyst for production of low sulfur fuels 有权
标题翻译：用于生产低硫燃料的加氢裂化器后处理催化剂
公开(公告)号：US20070278135A1
公开(公告)日：2007-12-06
申请号：US11446251
申请日：2006-06-02
申请人： William J. Tracy , Chuansheng Bai , Robert A. Bradway , William E. Lewis , Randolph J. Smiley
发明人： William J. Tracy , Chuansheng Bai , Robert A. Bradway , William E. Lewis , Randolph J. Smiley
IPC分类号： C10G65/00 , C10G69/00
CPC分类号： C10G65/12 , B01J23/883 , B01J23/8885 , B01J31/10 , C10G45/08
摘要： A hydrocracking process for converting a petroleum feedstock to higher gravity, lower sulfur products, especially ultra low sulfur road diesel fuel. The process may be operated as a single-stage or two-stage hydrocracking. In each case, a hydrocracking step is followed directly by a post-treat hydrodesulfurization zone using a bulk multimetallic catalyst comprised of at least one Group VIII non-noble metal and at least two Group VIB metals with a ratio of Group VIB metal to Group VIII non-noble metal is from about 10:1 to about 1:10. In the two-stage option with interstage ammonia removal, the initial hydrocracking step may be followed by hydrodesulfurization using the bulk multimetallic catalyst prior to the ammonia removal which is followed by the second hydrocracking step. A final hydrodesulfurization over the bulk multimetallic catalyst may follow. The hydrodesulfurization over the bulk multimetallic catalyst is carried out at a pressure of at least 25 barg and preferably at least 40 barg.
摘要翻译：用于将石油原料转化为更高重力，较低硫产物，特别是超低硫道路柴油的加氢裂化方法。该方法可以作为单级或两级加氢裂化操作。在每种情况下，加氢裂化步骤直接通过后处理加氢脱硫区，使用由至少一种VIII族非贵金属和至少两种VIB族金属与VIII族的VIB族金属组成的本体多金属催化剂非贵金属为约10:1至约1:10。在阶段氨除去的两阶段选择中，初始加氢裂化步骤之后可以在除氨之前使用大量多金属催化剂进行加氢脱硫，其后是第二加氢裂化步骤。可以遵循大量多金属催化剂的最终加氢脱硫。本体多金属催化剂上的加氢脱硫在至少25barg，优选至少40barg的压力下进行。

3. 发明授权

US06893554B2 Naphtha desulfurization with selectively suppressed hydrogenation 有权
公开(公告)号：US06893554B2
公开(公告)日：2005-05-17
申请号：US10375813
申请日：2003-02-27
申请人： Garland B. Brignac , Michele S. Touvelle , Randolph J. Smiley
发明人： Garland B. Brignac , Michele S. Touvelle , Randolph J. Smiley
IPC分类号： B01J23/88 , B01J23/882 , B01J33/00 , B01J35/00 , B01J35/10 , C10G45/02 , C10G45/04 , C10G45/06 , C10G45/08 , C10G45/10 , C10G45/60
CPC分类号： B01J35/10 , B01J23/882 , B01J35/002 , B01J35/1061 , C10G45/02 , C10G45/04 , C10G45/06 , C10G45/08 , C10G45/10
摘要： Naphtha is selectively hydrodesulfurized in the presence of a sulfided, treated catalyst comprising at least a Group VIB metal catalytic component, to produce sulfur-reduced naphtha with reduced olefin loss due to saturation. The catalyst is treated with hydrogen, a selectively deactivating agent which deactivates its hydrogenation activity, and a protective agent which preserves its hydrodesulfurization activity during the treatment.

4. 发明授权

US09597655B2 Boron selectivated molecular sieves and their use in sorptive separations 有权
公开(公告)号：US09597655B2
公开(公告)日：2017-03-21
申请号：US14945516
申请日：2015-11-19
申请人： Jean W. Beeckman , Ivy D. Johnson , Natalie A. Fassbender , Tilman W. Beutel , Nadya A. Hrycenko , Randolph J. Smiley , Peter I. Ravikovitch
发明人： Jean W. Beeckman , Ivy D. Johnson , Natalie A. Fassbender , Tilman W. Beutel , Nadya A. Hrycenko , Randolph J. Smiley , Peter I. Ravikovitch
IPC分类号： B01D53/02 , C01B39/02 , B01J20/18 , C01B39/48
CPC分类号： B01J20/18 , B01D53/02 , B01D2253/116 , B01D2256/245 , B01D2257/102 , B01D2257/304 , B01D2257/40 , B01D2257/504 , C01B39/026 , C01B39/48 , Y02C10/08 , Y02P20/152
摘要： A composition is described comprising a molecular sieve having pores defined by channels formed by one or more 8-membered rings of tetrahedrally coordinated atoms, such as a DDR-type molecular sieve, and an amorphous deposit of a boron compound on the molecular sieve.

5. 发明申请

US20150008157A1 SLURRY HYDROCONVERSION AND COKING OF HEAVY OILS 有权
标题翻译：浆料的重油和重油
公开(公告)号：US20150008157A1
公开(公告)日：2015-01-08
申请号：US14308867
申请日：2014-06-19
申请人： Randolph J. Smiley , Anjaneya Sarma KOVVALI , David G. HAMMOND , Grace Shi Qian YEO
发明人： Randolph J. Smiley , Anjaneya Sarma KOVVALI , David G. HAMMOND , Grace Shi Qian YEO
IPC分类号： C10G69/06 , C10G69/14
CPC分类号： C10G69/14 , C10G9/005 , C10G31/09 , C10G45/16 , C10G47/26 , C10G49/12 , C10G69/06 , C10G2300/301
摘要： Systems and methods are provided for use of coking and slurry hydroconversion for conversion of heavy oil feeds. The combination of coking and slurry hydroconversion allows for improved yield of liquid products while reducing or minimizing the consumption of hydrogen in slurry hydroconversion reaction stages. Coking and slurry hydroconversion can be combined by segregating feeds based on Conradson carbon residue. Alternatively, slurry hydroconversion can be used to process unconverted bottoms from a coking process.
摘要翻译：提供了用于焦化和浆料加氢转化用于重油进料转化的系统和方法。焦化和浆料加氢转化的组合允许提高液体产物的产率，同时减少或最小化浆料加氢转化反应阶段中的氢消耗。焦化和浆料加氢转化可以通过基于康拉逊碳残留物的分离进料进行组合。或者，浆料加氢转化可用于处理焦化工艺中未转化的底部物质。

6. 发明申请

US20110132806A1 REMOVAL OF NITROGEN COMPOUNDS FROM FCC DISTILLATE 有权
标题翻译：从FCC馏分中除去硝酸化合物
公开(公告)号：US20110132806A1
公开(公告)日：2011-06-09
申请号：US12908091
申请日：2010-10-20
申请人： Stacey E. Siporin , David Thomas Ferrughelli , Steven S. Lowenthal , Randolph J. Smiley , Alan Roy Katritzky , Bruce R. Cook
发明人： Stacey E. Siporin , David Thomas Ferrughelli , Steven S. Lowenthal , Randolph J. Smiley , Alan Roy Katritzky , Bruce R. Cook
IPC分类号： C10G67/00 , C10G29/20
CPC分类号： C10G11/18 , C10G21/16 , C10G29/24 , C10G45/02 , C10G67/00 , C10G69/12
摘要： A method for the removal of nitrogen compounds from FCC feed or from catalytically cracked distillates including FCC cycle oils by using formaldehyde to selectively couple organic heterocyclic nitrogen species in the FCC feed or FCC distillate to form higher boiling coupling products out of the boiling range of FCC distillate. Removal of the nitrogenous compounds improves the operation of subsequent hydrodesulfurization steps needed for the distillate fraction to conform to low sulfur standards. The formaldehyde is preferably used in the form of paraformaldehyde. The reaction between the nitrogenous compounds in the cycle oil fraction with the formaldehyde is conveniently carried out in the cycle oil pumparound circuit of the FCC main column.
摘要翻译：一种从FCC原料或催化裂化的馏出物（包括FCC循环油）中除去氮化合物的方法，其中使用甲醛选择性地将有机杂环氮物质在FCC进料或FCC馏出物中偶联，以在沸点范围内形成较高沸点的偶联产物馏出物去除含氮化合物改善了馏出物馏分所需的随后加氢脱硫步骤的操作以符合低硫标准。甲醛优选以多聚甲醛的形式使用。循环油馏分中的含氮化合物与甲醛的反应在FCC主塔的循环油循环回路中方便地进行。

7. 发明授权

US07576023B2 Naphtha desulfurization with selectively suppressed hydrogenation 有权
标题翻译：石脑油脱硫选择性抑制加氢
公开(公告)号：US07576023B2
公开(公告)日：2009-08-18
申请号：US11103002
申请日：2005-04-11
申请人： Garland B. Brignac , Michele S. Touvelle , Randolph J. Smiley
发明人： Garland B. Brignac , Michele S. Touvelle , Randolph J. Smiley
IPC分类号： B01J38/56 , B01J38/08 , B01J23/00
CPC分类号： B01J35/10 , B01J23/882 , B01J35/002 , B01J35/1061 , C10G45/02 , C10G45/04 , C10G45/06 , C10G45/08 , C10G45/10
摘要： Naphtha is selectively hydrodesulfurized in the presence of a sulfided, treated catalyst comprising at least a Group VIB metal catalytic component, to produce sulfur-reduced naphtha with reduced olefin loss due to saturation. The catalyst is treated with hydrogen, a selectively deactivating agent which deactivates its hydrogenation activity, and a protective agent which preserves its hydrodesulfurization activity during the treatment.
摘要翻译：在包含至少一种VIB族金属催化组分的硫化处理过的催化剂的存在下，石脑油被选择性地加氢脱硫，以产生由于饱和而使烯烃损失降低的减硫石脑油。催化剂用氢气去除其氢化活性的选择性钝化剂，以及在处理过程中保持其加氢脱硫活性的保护剂。

8. 发明申请

US20160167013A1 BORON-SELECTIVATED MOLECULAR SIEVES AND THEIR USE IN SORPTIVE SEPARATIONS 有权
标题翻译：硼选择性分子筛及其在分离分离中的应用
公开(公告)号：US20160167013A1
公开(公告)日：2016-06-16
申请号：US14945516
申请日：2015-11-19
申请人： Jean W. Beeckman , Ivy D. Johnson , Natalie A. Fassbender , Tilman W. Beutel , Nadya A. Hrycenko , Randolph J. Smiley , Peter I. Ravikovitch
发明人： Jean W. Beeckman , Ivy D. Johnson , Natalie A. Fassbender , Tilman W. Beutel , Nadya A. Hrycenko , Randolph J. Smiley , Peter I. Ravikovitch
IPC分类号： B01J20/18 , B01D53/02
CPC分类号： B01J20/18 , B01D53/02 , B01D2253/116 , B01D2256/245 , B01D2257/102 , B01D2257/304 , B01D2257/40 , B01D2257/504 , C01B39/026 , C01B39/48 , Y02C10/08 , Y02P20/152
摘要： A composition is described comprising a molecular sieve having pores defined by channels formed by one or more 8-membered rings of tetrahedrally coordinated atoms, such as a DDR-type molecular sieve, and an amorphous deposit of a boron compound on the molecular sieve.
摘要翻译：描述了一种组合物，其包含具有由一个或多个四面体配位原子的8元环（例如DDR型分子筛）和硼化合物在分子筛上的无定形沉积物形成的通道限定的孔的分子筛。

9. 发明申请

US20150014217A1 INTEGRATED HYDROCRACKING AND SLURRY HYDROCONVERSION OF HEAVY OILS 有权
标题翻译：重油加氢和浆液重油的重油
公开(公告)号：US20150014217A1
公开(公告)日：2015-01-15
申请号：US14308893
申请日：2014-06-19
申请人： Randolph J. Smiley , Ajit Bhaskar Dandekar , Ramanathan Sundararaman , Rustom Merwan Billimoria , Thomas Francis Degnan, JR.
发明人： Randolph J. Smiley , Ajit Bhaskar Dandekar , Ramanathan Sundararaman , Rustom Merwan Billimoria , Thomas Francis Degnan, JR.
IPC分类号： C10G65/12
CPC分类号： C10G65/12 , C10G45/16 , C10G47/26 , C10G49/12
摘要： Improved yields of fuels and/or lubricants from a resid or other heavy oil feed can be achieved using slurry hydroconversion to convert at least about 90 wt % of the feed. The converted portion of the feed can then be passed into one or more hydroprocessing stages. An initial processing stage can be a hydrotreatment stage for additional removal of contaminants and for passivation of high activity functional groups that may be created during slurry hydroconversion. The hydrotreatment effluent can then be fractionated to separate naphtha boiling range fractions from distillate fuel boiling range fractions and lubricant boiling range fractions. At least the lubricant boiling range fraction can then be hydrocracked to improve the viscosity properties. The hydrocracking effluent can also be dewaxed to improve the cold flow properties. The hydrocracked and/or dewaxed product can then be optionally hydrofinished.
摘要翻译：可以使用浆料加氢转化来转化至少约90重量％的进料，从渣油或其他重油进料中提高燃料和/或润滑剂的产率。然后将进料的转化部分进入一个或多个加氢处理阶段。初始处理阶段可以是加氢处理阶段，用于额外去除污染物和钝化可能在浆料加氢转化过程中产生的高活性官能团。然后可以将加氢处理流出物进行分馏，从馏出燃料沸点馏分和润滑剂沸程馏分中分离出石脑油沸程。至少可以将润滑剂沸程级分进行加氢裂化以提高粘度特性。加氢裂化流出物也可以脱蜡以改善冷流特性。加氢裂化和/或脱蜡产物可以任选加氢处理。

10. 发明授权

US10035959B2 Slurry hydroconversion using enhanced slurry catalysts 有权
公开(公告)号：US10035959B2
公开(公告)日：2018-07-31
申请号：US14308905
申请日：2014-06-19
申请人： Ramanathan Sundararaman , Thomas Francis Degnan, Jr. , Rustom Merwan Billimoria , Natalie Ann Fassbender , Manuel A. Francisco , Anjaneya Sarma Kovvali , Randolph J. Smiley , John Peter Greeley , William Ernest Lewis , Roby Bearden, Jr.
发明人： Ramanathan Sundararaman , Thomas Francis Degnan, Jr. , Rustom Merwan Billimoria , Natalie Ann Fassbender , Manuel A. Francisco , Anjaneya Sarma Kovvali , Randolph J. Smiley , John Peter Greeley , William Ernest Lewis , Roby Bearden, Jr.
IPC分类号： C10G47/26 , C10G49/06 , C10G49/12 , C10G69/14 , C10G49/04 , C10G69/06 , C10G9/00
CPC分类号： C10G49/12 , C10G9/005 , C10G49/04 , C10G49/06 , C10G69/06 , C10G69/14
摘要： Systems and methods are provided for slurry hydroconversion of a heavy oil feed, such as an atmospheric or vacuum resid. The systems and methods allow for slurry hydroconversion using catalysts with enhanced activity and/or catalysts that can be recycled as a side product from a complementary refinery process.

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