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1. 发明授权

US4931362A Microcapsule and micromatrix bodies and method for their formation 失效
标题翻译：微胶囊和微阵体及其形成方法
公开(公告)号：US4931362A
公开(公告)日：1990-06-05
申请号：US233667
申请日：1988-08-18
申请人： Wilhelm Zsifkovits , Burghard Gruning , Hans-Joachim Kollmeier , Dietmar Schaefer , Christian Weitemeyer
发明人： Wilhelm Zsifkovits , Burghard Gruning , Hans-Joachim Kollmeier , Dietmar Schaefer , Christian Weitemeyer
IPC分类号： B01J13/18 , B41M5/165
CPC分类号： B01J13/18 , B01J13/185 , B41M5/165 , Y10S514/963 , Y10S514/965 , Y10T428/2985 , Y10T428/2987
摘要： An organic phase which comprises a water-insoluble material to be encapsulated, a capsule-forming or matrix-forming monomer or prepolymer and, should this be desirable, a solvent, is dispersed in droplet form in an aqueous phase. The capsule-forming or matrix-forming monomer or prepolymer forms a sheath around the material to be encapsulated. As a capsule-forming or matrix-forming monomer, an organosilicon compound of the general formula ##STR1## is used, wherein R.sup.1 is a linear or branched, saturated or unsaturated, n-functional hydrocarbon moiety, which may be interrupted by groups containing oxygen, nitrogen or sulfur; R.sup.2 and R.sup.3 are the same or different and represent a hydrocarbon moiety with 1 to 6 carbon atoms or X; X is a hydroxyl group or a hydrolyzable group and n is a whole number greater than or equal to 1, with the proviso that, when n=1, R.sup.1 has at least 12 carbon atoms and R.sup.2 and R.sup.3 represent X or a prepolymer hereof. The method can be carried out easily and requires only one compound to form the capsules or micromatrix bodies. In the implementation of the method, no foam occurs and the method results in end products with an acceptable shelf life.
摘要翻译：包含待包封的水不溶性材料，胶囊形成或基质形成单体或预聚物的有机相，并且如果这是期望的话，溶剂以水滴形式分散在水相中。胶囊形成或基质形成单体或预聚物在待包被材料周围形成鞘。作为胶囊形成或基质形成单体，使用通式“IMAGE”的有机硅化合物，其中R 1是直链或支链饱和或不饱和的正构官能烃部分，其可以被含氧的基团中断，氮或硫; R2和R3相同或不同，表示具有1至6个碳原子的烃部分或X; X是羟基或可水解基团，n是大于或等于1的整数，条件是当n = 1时，R 1具有至少12个碳原子，R 2和R 3表示X或其预聚物。该方法可以容易地进行，并且仅需要一种化合物来形成胶囊或微阵列体。在该方法的实施中，不发生泡沫，并且该方法导致最终产品具有可接受的保质期。

2. 发明授权

US06268521B1 Process for preparing acrylic esters and/or methacrylic esters of polyoxyalkylenes and the use thereof 有权
标题翻译：制备聚氧化烯的丙烯酸酯和/或甲基丙烯酸酯的方法及其用途
公开(公告)号：US06268521B1
公开(公告)日：2001-07-31
申请号：US09431448
申请日：1999-11-01
申请人： Burghard Gruning , Geoffrey Hills , Wolfgang Josten , Dietmar Schaefer , Stefan Silber , Christian Weitemeyer
发明人： Burghard Gruning , Geoffrey Hills , Wolfgang Josten , Dietmar Schaefer , Stefan Silber , Christian Weitemeyer
IPC分类号： C08F6954
CPC分类号： C08G65/3322 , C12P7/62
摘要： The present invention provides a process for enzymatic preparation of acrylic esters and/or methacrylic esters of polyoxyalkylenes, and to the use thereof. The acryloyl and/or methacryloyl compounds of polyoxyalkylenes are obtainable by a process for esterifying or transesterifying acrylic and/or methacrylic acid or acrylic and/or methacrylic esters with a polyoxyalkylene of the general formula (I) wherein R1, R2, R3 and a-e are as defined in claim 1 and wherein at least one OH group is present per molecule and the sequence of the polyoxyalkylene segments (C2H4-aR2aO)b and (CcH2cO)d is arbitrary, in the presence of an enzyme which catalyzes the esterification or transesterification.
摘要翻译：本发明提供了一种用于酶制备聚氧化烯的丙烯酸酯和/或甲基丙烯酸酯的方法及其用途。聚氧化烯的丙烯酰基和/或甲基丙烯酰基化合物可通过丙烯酸和/或甲基丙烯酸或丙烯酸和/或甲基丙烯酸酯与通式（I）的聚氧化烯酯化或酯交换的方法获得，其中R1，R2，R3和ae为如在权利要求1中所定义的，并且其中每个分子存在至少一个OH基团，并且在催化酯化或酯交换的酶的存在下，聚氧化烯链段（C 2 H 4 -a R 2a）b和（C 1 H 8 C 10）d的序列是任意的。

3. 发明授权

US06288129B1 Process for preparing acrylic esters and/or methacrylic esters of hydroxy-functional siloxanes and/or polyoxyalkylene-modified siloxanes and their use 有权
标题翻译：制备羟基官能硅氧烷和/或聚氧化烯改性硅氧烷的丙烯酸酯和/或甲基丙烯酸酯的方法及其用途
公开(公告)号：US06288129B1
公开(公告)日：2001-09-11
申请号：US09431438
申请日：1999-11-01
申请人： Burghard Gruning , Geoffrey Hills , Wolfgang Josten , Dietmar Schaefer , Stefan Silber , Christian Weitemeyer
发明人： Burghard Gruning , Geoffrey Hills , Wolfgang Josten , Dietmar Schaefer , Stefan Silber , Christian Weitemeyer
IPC分类号： B01F1700
CPC分类号： C08G77/38 , C08G77/46 , C12P9/00
摘要： The present invention provides a process for esterifying or transesterifying acrylic acid and/or methacrylic acid or acrylic esters and/or methacrylic esters with hydroxy-functional and/or polyoxyalkylene-modified siloxane derivatives of the general formula (I) wherein R1 through R8 and v, w, x, y, and z are as defined herein and the esterification or transesterification reaction is catalyzed by an enzyme.
摘要翻译：本发明提供了用通式（I）的羟基官能和/或聚氧化烯改性的硅氧烷衍生物酯化或酯交换丙烯酸和/或甲基丙烯酸或丙烯酸酯和/或甲基丙烯酸酯的方法，其中R1至R8和v ，w，x，y和z如本文所定义，酯化或酯交换反应由酶催化。

4. 发明授权

US5189184A 2-(3'-butenyl)-3,4-dihydro-2H-pyrans, their synthesis and use 失效
标题翻译： 2-（3'-丁烯）-3,4-二氢-2H-吡喃，其合成和用途
公开(公告)号：US5189184A
公开(公告)日：1993-02-23
申请号：US736766
申请日：1991-07-29
申请人： Dietmar Schaefer , Andreas Weier , Christian Weitemeyer , Dietmar Wewers
发明人： Dietmar Schaefer , Andreas Weier , Christian Weitemeyer , Dietmar Wewers
IPC分类号： C07D309/22 , C08K5/15 , C08K5/1545
CPC分类号： C08K5/15 , C07D309/22 , C08K5/1545
摘要： 2-(3'-butenyl)-3,4-dihydro-2H-pyrans of the general formula ##STR1## wherein R is a hydrogen group or an alkyl group with 1 to 6 carbon atoms. Methods for the synthesis of these compounds and their use as reactive modifiers or diluents for cationically curable monomers or polymers.
摘要翻译：具有通式“IMAGE”的2-（3'-丁烯基）-3,4-二氢-2H-吡喃，其中R是氢基或具有1至6个碳原子的烷基。用于合成这些化合物的方法及其作为阳离子可固化单体或聚合物的反应性改性剂或稀释剂的用途。

5. 发明授权

US5115040A Polyacrylate esters with quaternary ammonium groups 失效
标题翻译：具有季铵盐的聚丙烯酸酯
公开(公告)号：US5115040A
公开(公告)日：1992-05-19
申请号：US718193
申请日：1991-06-20
申请人： Jurgen Fock , Dietmar Schaefer , Eberhard Esselborn
发明人： Jurgen Fock , Dietmar Schaefer , Eberhard Esselborn
IPC分类号： A61K8/72 , A61K8/00 , A61Q5/00 , A61Q5/02 , B01F17/18 , C08F8/02 , C08F8/30 , C08F8/32 , C08F8/44 , C08F20/34 , C08F220/34 , C08G81/02 , C09K3/16 , D06M15/267
CPC分类号： A61Q5/02 , A61K8/8152 , A61Q5/12 , C08F8/44
摘要： Polyacrylate esters with quaternary ammonium groups are disclosed. The esters are obtained by transesterifying alkyl polyacrylate esters with dialkylaminoalkanols, followed by quaternization.The polymers are free of physiologically questionable components and can therefore be used for the preparation of cosmetic products, preferably for hair cosmetics. The polymers furthermore are suitable for finishing fibers or of textile products.The invention is furthermore directed to polyacrylate esters with tertiary amino groups, which are formed as intermediates in the preparation of polyacrylate esters with quaternary ammonium groups.

6. 发明授权

US5004559A Polyoxyalkylene-polysiloxane block copolymers as demulsifiers for water-containing oil 失效
标题翻译：聚氧化烯 - 聚硅氧烷嵌段共聚物作为含水油的破乳剂
公开(公告)号：US5004559A
公开(公告)日：1991-04-02
申请号：US271995
申请日：1988-11-16
申请人： Gotz Koerner , Dietmar Schaefer
发明人： Gotz Koerner , Dietmar Schaefer
IPC分类号： B01D17/04 , B01D17/05 , C08G77/46 , C10G33/04
CPC分类号： C10G33/04 , B01D17/047 , C08G77/46
摘要： To demulsify water-containing crude oil, selected polyoxyalkylene-polysiloxane block copolymers are described.The demulsifiers are used in amounts of less than 200 ppm based on the crude oil.
摘要翻译：为了使含水原油破乳，描述了选择的聚氧化烯 - 聚硅氧烷嵌段共聚物。基于原油，破乳剂的用量小于200ppm。

7. 发明授权

US4921895A Preparation for finishing textile fibers and products and textile products having improved handle 失效
标题翻译：纺织纤维和产品的整理以及具有改进手感的纺织品的制备
公开(公告)号：US4921895A
公开(公告)日：1990-05-01
申请号：US298123
申请日：1989-01-17
申请人： Dietmar Schaefer , Friedhelm Nickel
发明人： Dietmar Schaefer , Friedhelm Nickel
IPC分类号： D06M15/647
CPC分类号： D06M15/647
摘要： A preparation for finishing textile fibers or products comprising textile fibers is disclosed. The preparation is liquid and contains 0.5 to 80% by weight of a mixture of modified organopolysiloxane A and B in a ratio of A:B by weight of 10:1 to 1:1, with the proviso that organpolysiloxane A is a linear siloxane containing polyether groups and having at least 40 dialkylsiloxy units, to which are linked at least 2 polyether groups, each of which has a molecular weight of 600 to 4,000 and which comprises 40 to 100 mole percent of oxyethylene units, the remainder being oxypropylene units, the ratio of the number of dialkylsiloxy units to the number of polyether groups being greater than or equal to 8. The organopolysiloxane B is a linear siloxane containing quaternary ammonium groups with at least 20 dialkylsiloxy units, to which at least 2 quaternary ammonium groups are linked over carbon atoms, the ratio of the number of dialkylsiloxy units to the number of quaternary ammonium groups being greater than or equal to 10. The remainder of the preparation comprises water or a water miscible solvent.The preparation improves the handle of the finished fibers or fiber products while, at the same time, hydrophilizing them. This improvement in handle is also achieved with firmly twisted, open-end yarns. The finished fibers or fiber products can be redyed or overdyed without difficulty. They have good antielectrostatic properties.
摘要翻译：公开了用于整理纺织纤维或包含纺织纤维的产品的制备。该制剂是液体，并且包含0.5至80重量％的改性有机聚硅氧烷A和B的混合物，其比例为10:1至1:1，重量比为A：B，条件是有机聚硅氧烷A为含有聚醚基团并且具有至少40个二烷基甲硅烷氧基单元，连接至少2个聚醚基团，每个聚醚基团的分子量为600至4,000，并且包含40至100摩尔％的氧化乙烯单元，其余为氧化丙烯单元，二烷基甲硅烷氧基单元数与聚醚基团数目之比大于或等于8.有机聚硅氧烷B是含有至少20个二烷基甲硅烷氧基单元的季铵基的直链硅氧烷，至少有2个季铵基团连接到其上碳原子，二烷基甲硅烷氧基单元的数量与季铵基团数目的比例大于或等于10.剩余的制剂包含水或水可溶性溶剂。该制剂改善成品纤维或纤维制品的处理，同时使它们亲水化。手柄的这种改进也可以用坚固扭曲的开口纱线实现。成品的纤维或纤维制品可以轻易地重新涂抹或变质。它们具有良好的抗静电性能。

8. 发明授权

US4833225A Polyquaternary polysiloxane polymers, their synthesis and use in cosmetic preparations 失效
标题翻译：聚季铵盐聚硅氧烷聚合物，它们在化妆品中的合成和应用
公开(公告)号：US4833225A
公开(公告)日：1989-05-23
申请号：US154964
申请日：1988-02-10
申请人： Dietmar Schaefer , Manfred Krakenberg
发明人： Dietmar Schaefer , Manfred Krakenberg
IPC分类号： A61K8/893 , A61K8/898 , A61Q5/02 , A61Q5/12 , C08G77/388 , C08G77/54
CPC分类号： A61Q5/12 , A61K8/898 , A61Q5/02 , C08G77/388 , C08G77/54
摘要： Polyquaternary polysiloxane polymers are disclosed comprising repeating units of ##STR1## wherein X is a bivalent hydrocarbon group with at least 4 carbon atoms, which has a hydroxyl group and may be interrupted by an oxygen atom,Y is a bivalent hydrocarbon group with at least 2 carbon atoms, which has a hydroxyl group and which may be interrupted by an oxygen or nitrogen atom,R.sup.1, R.sup.2, R.sup.3, R.sup.4 are the same or different and may be alkyl groups with at least 1 to 4 carbon atoms or benzyl groups or in which R.sup.1 and R.sup.3 or R.sup.2 and R.sup.4 may be components of a bridging alkylene group,A.crclbar. is an inorganic or organic anion,n=5 to 200m is a whole number.gtoreq.1.The compounds may be synthesized by an addition reaction between .alpha.,.omega.-hydrogenpolysiloxane of the formula ##STR2## and epoxides which have a terminal olefinic bond and reacting the product obtained with a diamine of the general formula ##STR3## The polymers may be used in cosmetic preparations, especially in hair cosmetics. They improve the ability to comb the hair wet and dry, increase the gloss and reduce the electrostatic charge on the treated hair.
摘要翻译：公开了包含重复单元的聚季铵盐聚硅氧烷聚合物，其中X是具有至少4个碳原子的二价烃基，其具有羟基并且可以被氧原子间隔，Y是具有至少2个的二价烃基碳原子，其具有羟基并且可被氧或氮原子间隔，R 1，R 2，R 3，R 4相同或不同，并且可以是具有至少1至4个碳原子的烷基或苄基或在其中R 1和R 3或R 2和R 4可以是桥连亚烷基的组分，A（ - ）是无机或有机阴离子，n = 5至200μm是整数> / = 1。该化合物可以通过下式的α，ω-氢聚硅氧烷与具有末端烯属键的环氧化物之间的加成反应合成，并使所得产物与通式为的二胺反应。聚合物可以用于化妆品，特别是头发化妆品。它们可以提高梳理头发的干燥和干燥能力，增加光泽度并减少被处理毛发上的静电电荷。

9. 发明授权

US5338485A Polyacrylate esters with long-chain hydrocarbon and polyoxyalkylene groups and their use as surface active substances 失效
标题翻译：具有长链烃和聚氧化烯基团的聚丙烯酸酯及其作为表面活性物质的用途
公开(公告)号：US5338485A
公开(公告)日：1994-08-16
申请号：US843912
申请日：1992-02-27
申请人： Jurgen Fock , Eberhard Esselborn , Dietmar Schaefer
发明人： Jurgen Fock , Eberhard Esselborn , Dietmar Schaefer
IPC分类号： B01F17/00 , B01F17/42 , C08F8/14 , C08F20/18 , C08F120/18
CPC分类号： B01F17/0028 , C08F8/14 , C08F2810/30 , Y10S516/06
摘要： Polyacrylate esters with long-chain hydrocarbon and polyoxyalkylene groups are disclosed, which are prepared by transesterification of polyacrylate alkyl esters, the alkyl groups of which have 1 to 4 carbon atoms and which were obtained by free radical polymerization, wherein the transesterification is carried out with a mixture of selected alcohols and polyoxyalkylene monools. Compared to products obtained by copolymerization, the transesterification products are largely free of undesirable low molecular weight components, have a narrow molecular weight distribution and exhibit excellent surfactant properties. They are useful especially as W/O emulsifiers for natural and synthetic oils.
摘要翻译：公开了具有长链烃和聚氧化烯基团的聚丙烯酸酯，其通过聚丙烯酸酯烷基酯（其烷基具有1至4个碳原子并通过自由基聚合获得）的酯交换制备，其中酯交换反应是用选择的醇和聚氧化烯一元醇的混合物。与通过共聚获得的产物相比，酯交换产物大部分没有不期望的低分子量组分，具有窄的分子量分布并且表现出优异的表面活性剂性质。它们特别适用于天然和合成油的W / O乳化剂。

10. 发明授权

US5246607A Methylpolysiloxanes with quaternary ammonium groups as corrosion inhibitors for preparations consisting predominantly of water 失效
标题翻译：作为腐蚀抑制剂的季铵盐组合物的甲基硅氧烷含水预处理
公开(公告)号：US5246607A
公开(公告)日：1993-09-21
申请号：US420348
申请日：1989-10-12
申请人： Dietmar Schaefer , Werner Hohner
发明人： Dietmar Schaefer , Werner Hohner
IPC分类号： C23F11/14 , C23F11/173
CPC分类号： C23F11/141 , C23F11/142 , C23F11/173
摘要： Methylpolysiloxanes are disclosed which have quaternary ammonium groups linked to silicon atoms via carbon atoms, wherein the ratio of the number of dimethylsiloxy groups to the number of quaternary ammonium groups has a value of 0.5 to 1.5. The methylpolysiloxanes are useful as corrosion inhibitors for preparations consisting predominantly of water, especially coolants, such as cooling lubricants mixed with water, in an amount of 0.01 to 0.1% by weight, based on the total preparation in the form suitable for use.
摘要翻译：公开了具有通过碳原子与硅原子连接的季铵基的甲基聚硅氧烷，其中二甲基甲硅烷氧基的数目与季铵基的数量的比值为0.5至1.5。基于以适合使用的形式的总制剂，甲基聚硅氧烷可用作主要由水组成的制剂的腐蚀抑制剂，特别是冷却剂，例如与水混合的冷却润滑剂，其量为0.01至0.1重量％。

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