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1. 发明授权

US5055550A Polymers prepared from 4,4'-bis(2-[3,4(dicarboxyphenyl)hexafluoroisopropyl] diphenyl ether dianhydride 失效
标题翻译：由4,4'-双（2- [3,4（二羧基苯基）六氟异丙基]二苯醚二酐制备的聚合物
公开(公告)号：US5055550A
公开(公告)日：1991-10-08
申请号：US497081
申请日：1990-03-21
申请人： Werner H. Mueller , Dinesh N. Khanna , Rohitkumar H. Vora , Ruediger J. Erckel
发明人： Werner H. Mueller , Dinesh N. Khanna , Rohitkumar H. Vora , Ruediger J. Erckel
IPC分类号： C07C65/24 , C08G69/40 , C08G73/10 , C08G73/12 , G03F7/038
CPC分类号： C07C65/24 , C08G69/40 , C08G73/105 , C08G73/1057 , C08G73/1064 , C08G73/12 , G03F7/0387 , Y10T428/31721
摘要： This invention relates to new fluorine-containing polyimides, polyamide-acids/esters, polyamides, addition polyimides and imide oligomers which exhibit low melting points, better solubilities, low dielectric constants, superior thermal and thermal oxidative stability, and improved processing characteristics.The products of this invention are characterized by the fact that they are derived from 4,4'-bis[2-(3,4-(dicarboxyphenyl)hexafluoroisopropyl]diphenyl ether dianhydride.
摘要翻译：本发明涉及显示低熔点，更好的溶解度，低介电常数，优异的热和热氧化稳定性以及改进的加工特性的新的含氟聚酰亚胺，聚酰胺酸/酯，聚酰胺，加成聚酰亚胺和酰亚胺低聚物。本发明的产物的特征在于它们衍生自4,4'-双[2-（3,4-（二羧基苯基）六氟异丙基]二苯醚二酐。

2. 发明授权

US4931540A Polymers prepared from 4,4'-bis[2-(3,4-(dicarboxyphenyl)hexafluoroisopropyl] diphenyl ether dianhydride 失效
标题翻译：由4,4'-双[2-（3,4-（二羧基苯基）六氟异丙基]二苯醚二酐制备的聚合物
公开(公告)号：US4931540A
公开(公告)日：1990-06-05
申请号：US124720
申请日：1987-11-24
申请人： Werner H. Mueller , Dinesh N. Khanna , Rohitkumar H. Vora , Ruediger J. Erckel
发明人： Werner H. Mueller , Dinesh N. Khanna , Rohitkumar H. Vora , Ruediger J. Erckel
IPC分类号： G03F7/037 , C07C65/24 , C08F290/00 , C08F299/00 , C08G69/40 , C08G73/10 , C08G73/12 , C08L79/08 , G03F7/038
CPC分类号： C07C65/24 , C08G69/40 , C08G73/105 , C08G73/1057 , C08G73/1064 , C08G73/12 , G03F7/0387
摘要： This invention relates to new fluorine-containing polyimides, polyamide-acids/esters, polyamides, addition polyimides and imide oligomers which exhibit low melting points, better solubilities, low dielectric constants, superior thermal and thermal oxidative stability, and improved processing characteristics.The products of this invention are characterized by the fact that they are derived from 4,4'-bis[2-(3,4-(dicarboxyphenyl)hexafluoroisopropyl]diphenyl ether dianhydride.

3. 发明授权

US5037949A Polymers prepared from 4,4'-bis[2-(amino (halo) phenoxyphenyl) hexafluoroisopropyl]diphenyl ether 失效
标题翻译：由4,4'-双[2-（氨基（卤代）苯氧基苯基）六氟异丙基]二苯基醚制备的聚合物
公开(公告)号：US5037949A
公开(公告)日：1991-08-06
申请号：US489448
申请日：1990-03-06
申请人： Werner H. Mueller , Dinesh N. Khanna , Rohitkumar H. Vora , Ruediger J. Erckel
发明人： Werner H. Mueller , Dinesh N. Khanna , Rohitkumar H. Vora , Ruediger J. Erckel
IPC分类号： C07C65/24 , C07C217/90 , C08G69/40 , C08G73/10 , C08G73/12 , G03F7/038
CPC分类号： C07C65/24 , C07C217/90 , C08G69/40 , C08G73/105 , C08G73/1057 , C08G73/1064 , C08G73/123 , C08G73/124 , G03F7/0387
摘要： This invention relates to new fluorine-containing polyimides, polyamide-acids/esters, polyamides, addition polyimides and imide oligomers which exhibit low melting points, better solubilities, low dielectric constants, superior thermal and thermal oxidative stability, and improved processing characteristics.The products of this invention are characterized by the fact that they are derived from 4,4'-bis[2-(amino(halo)phenoxyphenyl)hexafluoroisopropyl]diphenyl ether.
摘要翻译：本发明涉及显示低熔点，更好的溶解度，低介电常数，优异的热和热氧化稳定性以及改善的加工特性的新的含氟聚酰亚胺，聚酰胺酸/酯，聚酰胺，加成聚酰亚胺和酰亚胺低聚物。本发明的产物的特征在于它们衍生自4,4'-双[2-（氨基（卤代）苯氧基苯基）六氟异丙基]二苯醚。

4. 发明授权

US4925915A Polymers prepared from 4,4'-bis(2-(amino(halo) phenoxyphenyl) hexafluoroisopropyl) diphenyl ether 失效
标题翻译：由4,4'-双（2-（氨基（卤代）苯氧基苯基）六氟异丙基）二苯基醚制备的聚合物
公开(公告)号：US4925915A
公开(公告)日：1990-05-15
申请号：US124704
申请日：1987-11-24
申请人： Werner H. Mueller , Dinesh N. Khanna , Rohitkumar H. Vora , Ruediger J. Erckel
发明人： Werner H. Mueller , Dinesh N. Khanna , Rohitkumar H. Vora , Ruediger J. Erckel
IPC分类号： C07C65/24 , C07C217/90 , C08G69/40 , C08G73/10 , C08G73/12 , G03F7/038
CPC分类号： C08G69/40 , C07C217/90 , C07C65/24 , C08G73/105 , C08G73/1057 , C08G73/1064 , C08G73/123 , C08G73/124 , G03F7/0387
摘要： This invention relates to new fluorine-containing polyimides, polyamide-acids/esters, polyamides, addition polyimides and imide oligomers which exhibit low melting points, better solubilities, low dielectric constants, superior thermal and thermal oxidative stability, and improved processing characteristics.The product of this invention are characterized by the fact that they are derived from 4,4'-bis[2-(amino(halo)phenoxyphenyl)-hexafluoroisopropyl]diphenyl ether.

5. 发明授权

US4978738A High molecular weight, thermally soluble polyimides 失效
标题翻译：高分子量的热可溶性聚酰亚胺
公开(公告)号：US4978738A
公开(公告)日：1990-12-18
申请号：US217914
申请日：1988-07-12
申请人： Werner H. Mueller , Rohitkumar H. Vora , Dinesh N. Khanna
发明人： Werner H. Mueller , Rohitkumar H. Vora , Dinesh N. Khanna
IPC分类号： C08G73/10
CPC分类号： C08G73/1042 , C08G73/1039
摘要： High molecular weight polyimides are formed by polycondensation of 2,2-bis(4-aminophenyl) hexafluoropropane or 2,2-bis(3-aminophenyl) hexafluoropropane with one or more of bis-(3,4 dicarboxyphenyl) ether dianhydride; 3,3', 4,4' benzophenone tetracarboxylic acid dianhydride; 3,3', 4,4' diphenyl tetracarboxylic acid dianhydride and 2,2-bis(3,4 dicarboxyphenyl) hexafluoropropane dianhydride. Generally, the polymers of the present invention are characterized by a molecular weight of more than about 90,000.

6. 发明授权

US4803147A Photosensitive polyimide polymer compositions 失效
标题翻译：感光聚酰亚胺聚合物组合物
公开(公告)号：US4803147A
公开(公告)日：1989-02-07
申请号：US124742
申请日：1987-11-24
申请人： Werner H. Mueller , Dinesh N. Khanna , Rohitkumar H. Vora
发明人： Werner H. Mueller , Dinesh N. Khanna , Rohitkumar H. Vora
IPC分类号： C08G73/10 , C08G73/12 , C08L79/08 , G03F7/037 , H01L21/027 , H01L21/312 , G03C1/68
CPC分类号： C08G73/105 , C08G73/1039 , C08G73/123 , C08L79/08 , G03F7/037 , Y10S430/107
摘要： A photosensitive polyimide polymer composition comprising a solvent soluble polyimide condensation product of an aromatic dianhydride and an aromatic diamine, a polyfunctional ethylenically unsaturated monomer and a photoinitiator. The solvent soluble polyimides of the composition are prepared from at least one compound selected from 2,2-hexafluoro-bis-(3,4-dicarboxyphenyl)tetracarboxylic dianhydride; 1,1-bis-[4-(1,2-dicarboxyphenyl)]-1-phenyl-2,2,2-trifluoroethane dianhydride; 2,2-hexafluoro-bis(3-aminophenyl)propane; 2,2-hexafluoro-bis(4-aminophenyl)propane; 2,2-hexafluoro-bis-[4-(3-aminophenoxy)phenyl]propane; 2,2-hexafluoro-bis-[4-(4-aminophenoxy)phenyl]propane and 1,1-bis-(4-aminopheny)-1-phenyl-2,2,2-trifluoroethane or mixtures thereof.

7. 发明授权

US5061784A Polymers prepared from 4,4'-bis(3,4-dicarboxyphenyl) hexafluoroisopropyl) diphenyl dianhydride 失效
标题翻译：由4,4'-双（3,4-二羧基苯基）六氟异丙基）二苯基二酐制备的聚合物
公开(公告)号：US5061784A
公开(公告)日：1991-10-29
申请号：US543232
申请日：1990-08-06
申请人： Werner H. Mueller , Rohitkumar H. Vora
发明人： Werner H. Mueller , Rohitkumar H. Vora
IPC分类号： C08G73/10
CPC分类号： C08G73/1039
摘要： Polyimides and polyamide-acids having improved solubility and processing characteristics and high glass transition temperatures are provided, having incorporated into the polymeric chain the novel aromatic dianhydride compound 4,4'-bis[2-(3,4-dicarboxyphenyl) hexafluoroisopropyl] diphenyl dianhydride. The polyamide-acids and polyimides are prepared by reacting the 12F-Diphenyl DA with aromatic or aliphatic diamines. It has been found that the polyimides of this invention have improved solubility characteristics, good dielectric properties while at the same time exhibiting relatively high glass transition temperatures, and superior thermal and thermo-oxidative stability. The polymers may be processed into films, fibers or compression molded or fabricated into composites at moderate temperatures and pressures.
摘要翻译：提供了具有改进的溶解性和加工特性以及高玻璃化转变温度的聚酰亚胺和聚酰胺酸，其已经引入到聚合物链中，新的芳族二酐化合物4,4'-双[2-（3,4-二羧基苯基）六氟异丙基]二苯基二酐。聚酰胺酸和聚酰亚胺通过12F-二苯基DA与芳族或脂族二胺反应来制备。已经发现，本发明的聚酰亚胺具有改善的溶解性，良好的介电性能，同时具有较高的玻璃化转变温度，以及优异的热和热氧化稳定性。聚合物可以加工成薄膜，纤维或在中等温度和压力下压塑或制成复合材料。

8. 发明授权

US4978742A Polymers prepared from 2-(3-aminophenyl)-2-(4-aminophenyl) hexafluoro propane 失效
标题翻译：由2-（3-氨基苯基）-2-（4-氨基苯基）六氟丙烷制备的聚合物
公开(公告)号：US4978742A
公开(公告)日：1990-12-18
申请号：US252428
申请日：1988-09-30
申请人： Rohitkumar H. Vora , Werner H. Mueller
发明人： Rohitkumar H. Vora , Werner H. Mueller
IPC分类号： B29C43/00 , B29K79/00 , C08G73/10 , C08J5/18 , D01F6/74
CPC分类号： C08G73/1039
摘要： Polyimides and polyamide-acids having improved solubility and processing characterisitcs are provided having incorporated into the polymeric chain as a novel aromatic diamine compound, 2-(3-aminophenyl)-2-(4-aminophenyl) hexafluoropropane (3,4'-6F Diamine). The polyamide-acids and polyimides are prepared by reacting the 3,4'-6F Diamine with aromatic tetracarboxylic acids or anhydrides thereof. It has been found that the polyimides of this invention have improved solubility characterisitics, low dielectric constants and improved thermal flow properties as a consequence of the meta/para positioning of the amino groups on the diamine, which renders these polymers more readily melt spinnable for the production of fibers. The polymers may also be compression molded and fabricated into composites at moderate temperatures and pressures. Solutions of the polyimides may be cast into films.

9. 发明授权

US5077378A Polyamide containing the hexafluoroisopropylidene group 失效
标题翻译：含有六氟异亚丙基的聚酰胺
公开(公告)号：US5077378A
公开(公告)日：1991-12-31
申请号：US526583
申请日：1990-05-21
申请人： Werner H. Mueller , Dinesh N. Khanna , Bernd Hupfer
发明人： Werner H. Mueller , Dinesh N. Khanna , Bernd Hupfer
IPC分类号： C08G69/26 , C08G69/32 , G03F7/023
CPC分类号： G03F7/0233 , C08G69/26 , C08G69/32
摘要： This invention is that of high temperature polyamides containing the hexafluoroisopropylidene group. The high temperature polyamides of the invention and photo or radiation sensitizers provide improved high temperature positive resists which can be developed in aqueous alkaline developer and thermally anneal to form heat resistant, polyoxazole relief structures suitable for use in microelectronic and printing applications. The positive photoresists of the invention have improved solubility in coating solvents and improved photospeed. The polyamides of the invention can be prepared by conventional condensation reactions; e.g. the condensation of a diamine and diacid chloride. In addition the polyamides of this invention provide high temperature protective coatings with superior adhesion properties in applications other than the photoresist area.
摘要翻译：本发明是含有六氟异亚丙基的高温聚酰胺。本发明的高温聚酰胺和光或辐射敏化剂提供改进的高温正性抗蚀剂，其可以在含水碱性显影剂中显影并热退火以形成适用于微电子和印刷应用的耐热的聚恶唑消除结构。本发明的正性光致抗蚀剂具有改进的涂料溶剂溶度和改进的感光速度。本发明的聚酰胺可以通过常规的缩合反应制备; 例如二胺和二酰氯的缩合。此外，本发明的聚酰胺提供了除光刻胶区域之外的应用中具有优异粘合性能的高温保护涂层。

10. 发明授权

US4939215A Heat resistant polybenzoxazole from bis-((aminohydroxyphenyl)hexafluoroisopropyl)diphenyl ether 失效
标题翻译：来自双 - （（氨基羟基苯基）六氟异丙基）二苯基醚的耐热聚苯并恶唑
公开(公告)号：US4939215A
公开(公告)日：1990-07-03
申请号：US327761
申请日：1989-03-23
申请人： Werner H. Mueller , Dinesh N. Khanna
发明人： Werner H. Mueller , Dinesh N. Khanna
IPC分类号： C08G69/26 , C08G69/32 , C08G73/22 , G02F1/1337 , G03F7/023 , G03F7/037 , H01B3/30
CPC分类号： G02F1/133723 , C08G69/26 , C08G69/32 , C08G73/22 , G03F7/0233 , G03F7/037 , H01B3/303 , Y10T428/10
摘要： Heat resistant, shapable, hydroxy and/or alkoxy-substituted polyamides derived from at least one diamine selected from unsubstituted and substituted 4,4'-bis[2-(4-amino-3-hydroxyphenyl)hexafluoroisopropyl)]diphenyl ether 4,4'-bis-[2-(3-amino-4-hydroxyphenyl)hexafluoroisopropyl]diphenyl ether and a dicarboxylic acid or a derivative thereof e.g. its acid halo or ester. The polyamides of the invention may be thermally cured to form polybenzoxazoles of higher heat resistance which are stable to hydrolytic, chemical and radiation attack.The polyamides of the invention may be formed into shaped articles by molding, extrusion and solvent casting processes preferably in the presence of a solvent or diluent and then optionally converted into heat resistant, insoluble polybenzoxazoles. These shaped articles are useful in aircraft, electronic and other commercial applications where heat, chemical and radiation resistance are desired in conjunction with good mechanical and electrical properties.
摘要翻译：衍生自至少一种选自未取代的和取代的4,4'-双[2-（4-氨基-3-羟基苯基）六氟异丙基）]二苯基醚4,4'-二胺的二胺的耐热，可成形的羟基和/或烷氧基取代的聚酰胺 ' - 双 - [2-（3-氨基-4-羟基苯基）六氟异丙基]二苯醚和二羧酸或其衍生物例如其酸卤素或酯。本发明的聚酰胺可以被热固化以形成对于水解，化学和辐射攻击是稳定的较高耐热性的聚苯并恶唑。本发明的聚酰胺可以通过模制，挤出和溶剂浇铸方法形成成型制品，优选在溶剂或稀释剂的存在下，然后任选地转化成耐热不溶性聚苯并恶唑。这些成型制品在飞机，电子和其他商业应用中是有用的，其中需要耐热，耐化学性和耐辐射性以及良好的机械和电学性能。

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