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1. 发明授权

US4861895A Treatment of aqueous solutions obtained in the carbalkoxylation of olefinically unsaturated compounds 失效
标题翻译：处理在烯属不饱和化合物的碳烷基化反应中获得的水溶液
公开(公告)号：US4861895A
公开(公告)日：1989-08-29
申请号：US77630
申请日：1987-07-24
申请人： Werner Bertleff , Robert Maerkl , Peter Magnussen , Gebhard Kuehn , Peter Stops
发明人： Werner Bertleff , Robert Maerkl , Peter Magnussen , Gebhard Kuehn , Peter Stops
IPC分类号： C07C67/38 , C07C67/00 , C07C67/48 , C07C67/54 , C07C67/60 , C07C69/02 , C07C69/34 , C07C69/44 , C07C69/533 , C07D211/70 , C07D213/06
CPC分类号： C07C67/38 , C07C67/60
摘要： Aqueous solutions which are obtained in the carbalkoxylation of olefinically unsaturated compounds and contain heterocyclic aromatic nitrogen bases, their transformation products and lower fatty acids and/or their salts are treated by a process in which (a) the aqueous solution is heated to 150.degree.-300.degree. C. under from 10 to 300 bar and (b) heterocyclic aromatic nitrogen bases which are formed again from the transformation products are then separated off.
摘要翻译：通过以下方法处理在烯属不饱和化合物的碳烷基氧化中含有杂环芳族氮碱，它们的转化产物和低级脂肪酸和/或其盐的水溶液，其中（a）将水溶液加热至150℃， 300℃，10-300巴，（b）从转化产物再次形成的杂环芳基氮碱分离出来。

2. 发明授权

US4777284A Continuous preparation of carbalkoxy-containing aliphatic compounds 失效
标题翻译：连续制备含有烷氧基的脂族化合物
公开(公告)号：US4777284A
公开(公告)日：1988-10-11
申请号：US116877
申请日：1987-11-05
申请人： Robert Maerkl , Werner Bertleff , Gebhard Kuehn , Paul Panitz , Peter Stops , Rudolf Kummer , Guenter Schuch
发明人： Robert Maerkl , Werner Bertleff , Gebhard Kuehn , Paul Panitz , Peter Stops , Rudolf Kummer , Guenter Schuch
IPC分类号： B01J31/20 , B01J31/00 , C07B61/00 , C07C67/30 , C07C67/38 , C07C69/003 , C07C69/34 , C07C69/44 , C07C69/533 , C07C69/593
CPC分类号： C07C67/38
摘要： Carbalkoxy-containing aliphatic compounds are prepared continuously by reacting an olefinically unsaturated aliphatic compound with carbon monoxide and an alkanol in the presence of a cobalt carbonyl catalyst and a tertiary nitrogen base at from 80.degree. to 200.degree. C. and under from 100 to 1,200 bar by an improved process in which carbon monoxide is circulated, and a carbon dioxide content of from 0.1 to 2% by volume is maintained in the carbon monoxide fed to the reaction.
摘要翻译：在羰基催化剂和叔氮碱的存在下，在80〜200℃，100〜1200巴下，使烯属不饱和脂肪族化合物与一氧化碳和链烷醇反应制备含有链烷烃基的脂肪族化合物通过一氧化碳循环的改进方法，并且在进料到反应中的一氧化碳中维持二氧化碳含量为0.1-2体积％。

3. 发明授权

US4894474A Preparation of alkyl pentenoates 失效
标题翻译：戊烯酸烷基酯的制备
公开(公告)号：US4894474A
公开(公告)日：1990-01-16
申请号：US225823
申请日：1988-07-29
申请人： Robert Maerkl , Werner Bertleff , Hans J. Wilfinger , Gunter Schuch , Wolfgang Harder , Gebhard Kuehn , Paul Panitz
发明人： Robert Maerkl , Werner Bertleff , Hans J. Wilfinger , Gunter Schuch , Wolfgang Harder , Gebhard Kuehn , Paul Panitz
IPC分类号： C07C67/38 , B01J31/20 , C07B61/00 , C07C69/533
CPC分类号： C07C69/533
摘要： Alkyl pentenoates are prepared by reacting butadiene with carbon monoxide and an alkanol in the presence of a cobalt carbonyl complex and a tertiary, aromatic heterocyclic nitrogen base at from 80.degree. to 160.degree. C. under from 100 to 1,000 bar in the presence of from 0.1 to 10% by volume of hydrogen, based on the amount of carbon monoxide used.
摘要翻译：烷基戊烯酸酯是通过使丁二烯与一氧化碳和链烷醇在羰基钴配合物和叔芳族杂环氮碱存在下，在80-160℃，100-1,000巴下，存在0.1当量至10体积％的氢气，基于所用一氧化碳的量。

4. 发明授权

US4910328A Preparation of omega-formylalkanecarboxylic esters 失效
标题翻译： ω-甲酰基烷羧酸酯的制备
公开(公告)号：US4910328A
公开(公告)日：1990-03-20
申请号：US206752
申请日：1988-06-15
申请人： Werner Bertleff , Robert Maerkl , Michael Roeper
发明人： Werner Bertleff , Robert Maerkl , Michael Roeper
IPC分类号： C07B61/00 , B01J31/20 , C07C67/313 , C07C69/67
CPC分类号： C07C67/347
摘要： .omega.-Formylalkanecarboxylic esters are prepared by hydroformylation of an alkenecarboxylic ester with carbon monoxide and hydrogen at elevated tempertures and under superatmospheric pressure in the presence of a cobalt carbonyl complex by a process in which an .alpha.,.beta.-unsaturated alkenecarboxylic ester is hydroformylated in the presence of from 0.01 to 1 mol %, calculated as cobalt, of a cobalt carbonyl complex, while maintaining a conversion of from 10 to 70% of .alpha.,.beta.-unsaturated alkenecarboxylic esters.
摘要翻译：通过在钴羰基络合物存在下，在升高的温度和超大气压下，用一氧化碳和氢气将烯羧酸酯加氢甲酰化制备ω-甲酰基烷羧酸酯，其中α，β-不饱和烯烃羧酸酯在存在下加氢甲酰化 0.01至1摩尔％，钴计算为钴羰基络合物，同时保持10至70％的α，β-不饱和烯烃羧酸酯的转化率。

5. 发明授权

US4755625A Preparation of 1,1,2-trialkoxyethanes 失效
标题翻译： 1,1,2-三烷氧基乙醚的制备
公开(公告)号：US4755625A
公开(公告)日：1988-07-05
申请号：US73999
申请日：1987-07-16
申请人： Robert Maerkl , Werner Bertleff , Rudolf Kummer
发明人： Robert Maerkl , Werner Bertleff , Rudolf Kummer
IPC分类号： C07B61/00 , B01J31/00 , B01J31/20 , B01J31/24 , C07C41/00 , C07C41/48 , C07C43/315 , C07C67/00 , C07D317/22 , C07D319/06 , C07D321/06
CPC分类号： C07C41/48
摘要： 1,1,2-trialkoxyethanes I ##STR1## where R.sup.1, R.sup.2 and R.sup.3 are each C.sub.1 -C.sub.8 -alkyl and R.sup.1 and R.sup.2 may furthermore be bonded to one another to form a 5-membered to 7-membered ring, are prepared by reacting a formaldehyde dialkyl acetal II with carbon monoxide and hydrogen, from 0.5 to 1.5 moles of hydrogen being used per mole of carbon monoxide, and with not less than 1 mole of alcohol R.sup.3 OH per mole of formaldehyde dialkyl acetal under superatmospheric pressure and at elevated temperatures in the presence of a catalyst which is formed from a cobalt carbonyl compound and a trivalent organic compound of the formula III ##STR2## where A is phosphorus, arsenic, antimony or bismuth and R.sup.4, R.sup.5 and R.sup.6 are each an organic radical.
摘要翻译：其中R 1，R 2和R 3各自是C 1 -C 8 - 烷基，R 1和R 2可以彼此键合形成5元至7元环，通过使甲醛二烷基缩醛II与一氧化碳和氢反应，每摩尔一氧化碳使用0.5至1.5摩尔氢，并且在超大气压下每摩尔甲醛二烷基缩醛不少于1摩尔醇R3OH，在由羰基钴化合物和式III的三价有机化合物形成的催化剂存在下，在升高的温度下，其中A是磷，砷，锑或铋，并且R 4，R 5和R 6各自是有机的激进。

6. 发明授权

US5081313A Process for the preparation of 2,3-dialkoxypropanals 失效
标题翻译：制备2,3-二烷氧基丙酸的方法
公开(公告)号：US5081313A
公开(公告)日：1992-01-14
申请号：US528021
申请日：1990-05-23
申请人： Dieter Koeffer , Robert Maerkl , Werner Bertleff
发明人： Dieter Koeffer , Robert Maerkl , Werner Bertleff
IPC分类号： B01J31/04 , B01J31/20 , B01J31/24 , C07B61/00 , C07C45/49 , C07C45/50 , C07C47/198
CPC分类号： C07C45/49
摘要： The preparation of 2,3-dialkoxypropanals of the general formula I ##STR1## in which R.sup.1 and R.sup.2 denote C.sub.1 -C.sub.8 -alkyl or C.sub.5 - or C.sub.6 -cycloalkyl which may or may not bear substituents which are inert under the conditions of the reaction, wherein a 1,2-dialkoxy ethene of the general formula IIR.sup.1 O--HC.dbd.CH--OR.sup.2 (II)is reacted with carbon monoxide and hydrogen in the presence of a rhodium-containing catalyst.
摘要翻译：制备通式I（I）的2,3-二烷氧基丙醛，其中R 1和R 2表示可在或不具有在条件下为惰性的取代基的C 1 -C 8 - 烷基或C 5 - 或C 6 - 环烷基的反应，其中在含铑催化剂存在下，将通式II的R 1 -O-HC = CH-OR 2（II）的1,2-二烷氧基乙烯与一氧化碳和氢气反应。

7. 发明授权

US4740525A Preparation of ethylene glycol 失效
标题翻译：乙二醇的制备
公开(公告)号：US4740525A
公开(公告)日：1988-04-26
申请号：US900770
申请日：1986-08-26
申请人： Robert Maerkl , Werner Bertleff , Wolfgang Harder , Rudolf Kummer
发明人： Robert Maerkl , Werner Bertleff , Wolfgang Harder , Rudolf Kummer
IPC分类号： C07B61/00 , B01J31/00 , C07C29/158 , C07C27/06 , C07C31/20
CPC分类号： C07C29/158 , Y02P20/52
摘要： Ethylene glycol is prepared from carbon monoxide and hydrogen in homogeneous liquid phase under superatmospheric pressure and at elevated temperature in the presence of a rhodium-containing catalyst and in the presence of an organic solvent, the organic solvent used being a C.sub.2 -C.sub.20 -n-alkanol and the concentration of this alkanol, based on the total amount of the mixture, constantly being maintained at not less than 50% by weight.
摘要翻译：乙二醇由均一液相中的一氧化碳和氢气在超大气压和升高的温度下在含铑催化剂存在下制备，并且在有机溶剂存在下，所用的有机溶剂是C 2 -C 20正 - 链烷醇和该烷醇的浓度，基于混合物的总量，不断保持在不小于50重量％。

8. 发明授权

US06916778B1 UV absorbers with affinity for textile fiber 失效
标题翻译：对纺织纤维具有亲和力的紫外线吸收剂
公开(公告)号：US06916778B1
公开(公告)日：2005-07-12
申请号：US09926412
申请日：2000-04-17
申请人： Jürgen Detering , Werner Bertleff , Gerhard Wagenblast , Christian Ott , Elisabeth Kappes , Thorsten Habeck
发明人： Jürgen Detering , Werner Bertleff , Gerhard Wagenblast , Christian Ott , Elisabeth Kappes , Thorsten Habeck
IPC分类号： C07C235/34 , C08F8/00 , C08G73/02 , C11D3/00 , C11D3/37 , C11D3/42 , D06L3/12 , D06M13/123 , D06M13/224 , D06M13/372 , D06M13/402 , D06M13/41 , D06M13/415 , D06M13/419 , D06M13/46 , D06M15/356 , D06M15/59 , D06M15/61 , D06P5/06 , D06P5/08 , C11D3/32
CPC分类号： D06P5/08 , C07C235/34 , C08F8/00 , C08G73/0206 , C08G73/028 , C11D3/0063 , C11D3/3703 , C11D3/3715 , C11D3/3719 , C11D3/3723 , C11D3/42 , D06L4/60 , D06M13/123 , D06M13/224 , D06M13/2246 , D06M13/372 , D06M13/402 , D06M13/41 , D06M13/415 , D06M13/419 , D06M13/46 , D06M13/461 , D06M15/3562 , D06M15/59 , D06M15/61 , D06P5/06 , C08F26/02
摘要： The invention relates to the use of compounds (A) with at least one structural unit of formula (I), wherein X represents groups of formula —CR1═CR2— or a carbonyl group C═O, R1 and R2 meaning hydrogen or essentially organic radicals, Z means essentially organic radicals, n means a number from 0 to 3 and p means a number from 0 to 5, as UV absorbers with an affinity for textile fibres, for protecting the human skin from harmful UV radiation and for protecting dyed textile materials from fading.
摘要翻译：本发明涉及化合物（A）与至少一种式（I）结构单元的用途，其中X代表式-CR 1 -CR 2 - 或羰基CO，R 1和R 2表示氢或基本上有机基团，Z表示基本上有机基团，n表示0至3的数，p表示数字为0至5，作为对纺织纤维具有亲和力的紫外线吸收剂，用于保护人体皮肤免受有害紫外线辐射，并用于保护染色的纺织材料免于褪色。

9. 发明授权

US06878683B2 Polymers used as controllable dispersing agents 失效
标题翻译：聚合物用作可控分散剂
公开(公告)号：US06878683B2
公开(公告)日：2005-04-12
申请号：US10297490
申请日：2001-06-06
申请人： Peter Neumann , Werner Bertleff , Matthias Kroner , Bernard Mohr
发明人： Peter Neumann , Werner Bertleff , Matthias Kroner , Bernard Mohr
IPC分类号： C08F290/06 , C08G81/02 , C11D3/37 , C11D11/00
CPC分类号： C11D11/0082 , C11D3/3761
摘要： Polymers of a poly(meth)acrylic acid main chain in which, based on the main chain, 0 to 30% by weight of the (meth)acrylic acid basic building blocks may be replaced by maleic acid (anhydride) basic building blocks, fumaric acid basic building blocks or mixtures thereof and 0 to 10% by weight of the (meth)acrylic acid basic building blocks may be replaced by other copolymerizable ethylenic basic building blocks,and C1-30-alkylpoly-C2-4-alkylene glycols, bonded to the main chain via ester groups, having an average molecular weight of from 250 to 10 000 as side chains,where, based on the polymer, 1 to 19% by weight of the main chain and 81 to 99% by weight of the side chains are present and this ratio and the average molecular weight of the side chains are chosen such that free carboxyl groups are present in the polymer,are used as controllable dispersants for detergents or cleaners or constituents thereof.
摘要翻译：聚（甲基）丙烯酸主链的聚合物，其中以主链为基准的0〜30重量％的（甲基）丙烯酸碱性结构单元可以用马来酸（酸酐）碱性结构单元代替富马酸酸性碱性结构单元或其混合物，和0〜10重量％的（甲基）丙烯酸碱性结构单元可以被其它可共聚的烯属碱性结构单元和C1-30烷基聚-C2-4-亚烷基二醇替代，通过酯基，其平均分子量为250至10000作为侧链，其中基于聚合物，1至19重量％的主链和81至99重量％的侧面链，并且该比例和侧链的平均分子量被选择为使得游离羧基存在于聚合物中，用作洗涤剂或清洁剂或其组分的可控分散剂。

10. 发明授权

US06586010B1 Method for producing agglomerates comprising a core-shell structure 失效
标题翻译：用于生产包含核 - 壳结构的附聚物的方法
公开(公告)号：US06586010B1
公开(公告)日：2003-07-01
申请号：US09857065
申请日：2001-05-31
申请人： Werner Bertleff , Ulrich Bröckel , Helmut Fricke , Hans-Peter Harz , Reiner Witt
发明人： Werner Bertleff , Ulrich Bröckel , Helmut Fricke , Hans-Peter Harz , Reiner Witt
IPC分类号： A61K914
CPC分类号： B01J2/006
摘要： A process for producing agglomerates with a core/shell structure, in which i) initial agglomerates containing a first particulate solid are prepared; ii) a second particulate solid is agglomerated in the presence of the initial agglomerates with the addition of a binder liquid to give second stage agglomerates and, where appropriate, iii) an nth (n≧3) solid is agglomerated in the presence of the (n−1)th stage agglomerates with the addition of a binder liquid to give nth stage agglomerates.
摘要翻译：制备具有核/壳结构的附聚物的方法，其中i）含有第一颗粒固体的初始附聚物; ii）第二颗粒固体在初始附聚物存在下与添加粘合剂液体一起凝聚，得到第二阶段附聚物，并且在适当情况下，iii）第n（n> = 3）固体在存在（n-1）级附聚物，加入粘合剂液体以产生第n级附聚物。

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