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1. 发明申请

US20090227784A1 Processing method for nano-miniaturizing chitosan of modifying property 有权
标题翻译：壳聚糖纳米小型化改性的加工方法
公开(公告)号：US20090227784A1
公开(公告)日：2009-09-10
申请号：US12318550
申请日：2008-12-31
申请人： Wen-Tung Chou , Ming-Yi Lai , Kun-Shan Huang , Wei-Chun Chen
发明人： Wen-Tung Chou , Ming-Yi Lai , Kun-Shan Huang , Wei-Chun Chen
IPC分类号： C07H1/00
CPC分类号： C07H1/00 , C08B37/003 , C08L5/08
摘要： The present invention relates a processing method for nano-miniaturizing chitosan of modifying property, which degrades the chitosan of high molecular weight down to the chitosan of middle and low molecular weight, then primarily nano-miniaturizes the interim chitosan by quaternary ammonium salt/synthesis, finally yield the nano-miniaturized chitosan of modified property by sol-gel method to have features in good biocompatibility and bioactivity to be served as additive material in products of cosmetics, medical treatment, hygiene, health care, biomedicine, agriculture, textile, food and so like so that not only the antiseptic, moisture-retentive and deodorizing capabilities can be promoted but also the processing cost can be reduced due to easiness of the mass production.
摘要翻译：本发明涉及壳聚糖纳米小型改性性能的加工方法，其将高分子量壳聚糖降解为中低分子量的壳聚糖，然后主要通过季铵盐/合成来使临时壳聚糖纳米微小化，最终通过溶胶 - 凝胶法生产具有良好生物相容性和生物活性的纳米小型化壳聚糖，作为化妆品，医疗，卫生，保健，生物医药，农业，纺织，食品和食品等产品中的添加剂。所以不仅可以促进防腐，保湿和除臭的能力，而且由于大量生产的容易性，可以降低加工成本。

2. 发明授权

US08193325B2 Processing method for nano-miniaturizing chitosan of modifying property 有权
标题翻译：壳聚糖纳米小型化改性的加工方法
公开(公告)号：US08193325B2
公开(公告)日：2012-06-05
申请号：US12318550
申请日：2008-12-31
申请人： Wen-Tung Chou , Ming-Yi Lai , Kun-Shan Huang , Wei-Chun Chen
发明人： Wen-Tung Chou , Ming-Yi Lai , Kun-Shan Huang , Wei-Chun Chen
IPC分类号： C08B37/08 , C07H5/06
CPC分类号： C07H1/00 , C08B37/003 , C08L5/08
摘要： The present invention relates a processing method for nano-miniaturizing chitosan of modifying property, which degrades the chitosan of high molecular weight down to the chitosan of middle and low molecular weight, then primarily nano-miniaturizes the interim chitosan by quaternary ammonium salt/synthesis, finally yield the nano-miniaturized chitosan of modified property by sol-gel method to have features in good biocompatibility and bioactivity to be served as additive material in products of cosmetics, medical treatment, hygiene, health care, biomedicine, agriculture, textile, food and so like so that not only the antiseptic, moisture-retentive and deodorizing capabilities can be promoted but also the processing cost can be reduced due to easiness of the mass production.
摘要翻译：本发明涉及壳聚糖纳米小型改性性能的加工方法，其将高分子量壳聚糖降解为中低分子量的壳聚糖，然后主要通过季铵盐/合成来使临时壳聚糖纳米微小化，最终通过溶胶 - 凝胶法生产具有良好生物相容性和生物活性的纳米小型化壳聚糖，作为化妆品，医疗，卫生，保健，生物医药，农业，纺织，食品和食品等产品中的添加剂。所以不仅可以促进防腐，保湿和除臭的能力，而且由于大量生产的容易性，可以降低加工成本。

3. 发明授权

US09090997B2 Fabrication of natural cellulose fiber with flame-retarding capability 有权
标题翻译：具有阻燃性能的天然纤维素纤维的制造
公开(公告)号：US09090997B2
公开(公告)日：2015-07-28
申请号：US13411775
申请日：2012-03-05
申请人： Wen-Tung Chou , Ming-Yi Lai , Kun-Shan Huang
发明人： Wen-Tung Chou , Ming-Yi Lai , Kun-Shan Huang
IPC分类号： D01D5/06 , D01F2/00 , D01D10/02 , D01D7/00 , D01F2/02 , D01D10/06 , D01D5/26 , D01F1/07 , D06M13/282 , D01F13/02
CPC分类号： D01F2/00 , D01D5/26 , D01D7/00 , D01D10/02 , D01D10/06 , D01F1/07 , D01F2/02 , D01F11/02 , D01F13/02 , D06M13/282 , D06M13/447 , D06M2101/06 , D06M2200/30 , Y02P70/627
摘要： A fabrication of natural cellulose fiber with flame-retarding capability comprises following steps. Blend pulp and solvent of N-methylmorpholine N-oxide (NMMO) to form slurry. Evaporate extra water content from slurry by a Thin Film Evaporator (TFE) to form dope. By Dry-Jet Wet Spinning, spin and extrude dope for coagulating and regenerating. Water-rinse and dry to form natural cellulose fiber. Soaking roll natural cellulose fiber by flame retardant of N-(hydroxymethyl)-3-(methoxy phosphorus acyl). Orderly dry, bake, neutralize, soaping clean, water rinse, baking dry, soaking rolled, alkaline clean, water rinse, dry and oil the natural cellulose fiber to produce natural cellulose fiber of flame retarding capacity. Because of cross-linking reaction for the flame retardant of N-(hydroxymethyl)-3-(methoxy phosphorus acyl) with natural cellulose fiber, the flame-retarding capability thereof meet requirements of testing standards in American ASTM D6413-1999 and ASTM D2863-1995. Moreover, the wastes thereof meet the requirements of environment protections without harm.
摘要翻译：具有阻燃性能的天然纤维素纤维的制造包括以下步骤。混合纸浆和N-甲基吗啉N-氧化物（NMMO）的溶剂形成浆料。通过薄膜蒸发器（TFE）从浆料中蒸发额外的水分以形成涂料。通过干喷射湿纺丝，旋转和挤出胶束用于凝结和再生。水冲洗干燥，形成天然纤维素纤维。通过N-（羟甲基）-3-（甲氧基磷酰基）的阻燃剂浸泡辊天然纤维素纤维。有序干燥，烘烤，中和，皂洗清洁，水冲洗，烘干，浸泡滚动，碱性清洁，水冲洗，干燥和油状天然纤维素纤维，生产天然纤维素纤维的阻燃能力。由于N-（羟甲基）-3-（甲氧基磷酰基）与天然纤维素纤维的阻燃剂的交联反应，其阻燃性能符合美国ASTM D6413-1999和ASTM D2863- 1995年。此外，其废物符合环保要求，无损害。

4. 发明授权

US08420005B2 Meltblown wetlaid method for producing non-woven fabrics with anti-mildew, anti-bacteria and deodorizing capabilities from natural cellulose 有权
标题翻译：用于生产具有抗天然纤维素抗霉菌，抗细菌和除臭能力的无纺织物的熔喷湿法方法
公开(公告)号：US08420005B2
公开(公告)日：2013-04-16
申请号：US12879042
申请日：2010-09-10
申请人： Wen-Tung Chou , Ming-Yi Lai , Kun-Shan Huang
发明人： Wen-Tung Chou , Ming-Yi Lai , Kun-Shan Huang
IPC分类号： D01D5/06 , D01D10/06 , D01F2/02 , D04H3/10
CPC分类号： D04H3/015 , D01D5/06 , D01D5/14 , D01F2/00 , D04H3/013 , D04H3/105
摘要： The present invention provides a meltblown wetlaid method for producing non-woven fabrics with anti-mildew, anti-bacteria and deodorizing capabilities from natural cellulose. The method comprises selecting wood pulp as raw material and using N-methylmorpholine N-oxide (NMMO) as dissolving solvent and 1,3-phenylene-bis 2-oxazoline (BOX) as stabilizer to form mixed cellulose mucilage as well as using modified and nano-miniaturized natural chitosan as additive for blending and dissolution to form cellulose dope. By meltblown method, the dope is extruded out of spinnerets to form filament bundle, then by ejecting mist aerosol of water, the filament bundle is coagulated with regeneration. After post treatments of water rinsing, hydro-entangled needle punching, drying, winding-up and the like having been orderly applied, then final product for nonwoven fabric of continuous filament with anti-mildew, anti-bacteria and deodorizing capabilities is produced.
摘要翻译：本发明提供一种用于生产具有抗天然纤维素的抗霉菌，抗细菌和除臭能力的无纺织物的熔喷湿法湿法。该方法包括选择木浆为原料，以N-甲基吗啉N-氧化物（NMMO）为溶剂，1,3-亚苯基 - 双2-恶唑啉（BOX）为稳定剂，形成混合纤维素胶浆，纳米微型化天然壳聚糖作为掺合和溶解形成纤维素掺杂剂的添加剂。通过熔喷方法，将纺丝液从喷丝头挤出形成丝束，然后通过喷雾雾气雾化，丝束与再生凝结。经过有序应用的水洗，水缠结针刺，干燥，卷绕等后处理后，生产具有抗霉菌，抗细菌和除臭能力的连续长丝无纺织物的最终产品。

5. 发明申请

US20130228949A1 FABRICATION OF NATURAL CELLULOSE FIBER WITH FLAME-RETARDING CAPABILITY 有权
标题翻译：具有阻燃能力的天然纤维素纤维的制备
公开(公告)号：US20130228949A1
公开(公告)日：2013-09-05
申请号：US13411775
申请日：2012-03-05
申请人： Wen-Tung CHOU , Ming-Yi Lai , Kun-Shan Huang
发明人： Wen-Tung CHOU , Ming-Yi Lai , Kun-Shan Huang
IPC分类号： D01F2/02
CPC分类号： D01F2/00 , D01D5/26 , D01D7/00 , D01D10/02 , D01D10/06 , D01F1/07 , D01F2/02 , D01F11/02 , D01F13/02 , D06M13/282 , D06M13/447 , D06M2101/06 , D06M2200/30 , Y02P70/627
摘要： A fabrication of natural cellulose fiber with flame-retarding capability comprises following steps. Blend pulp and solvent of N-methylmorpholine N-oxide (NMMO) to form slurry. Evaporate extra water content from slurry by a Thin Film Evaporator (TFE) to form dope. By Dry-Jet Wet Spinning, spin and extrude dope for coagulating and regenerating. Water-rinse and dry to form natural cellulose fiber. Soaking roll natural cellulose fiber by flame retardant of N-(hydroxymethyl)-3-(methoxy phosphorus acyl). Orderly dry, bake, neutralize, soaping clean, water rinse, baking dry, soaking rolled, alkaline clean, water rinse, dry and oil the natural cellulose fiber to produce natural cellulose fiber of flame retarding capacity. Because of cross-linking reaction for the flame retardant of N-(hydroxymethyl)-3-(methoxy phosphorus acyl) with natural cellulose fiber, the flame-retarding capability thereof meet requirements of testing standards in American ASTM D6413-1999 and ASTM D2863-1995. Moreover, the wastes thereof meet the requirements of environment protections without harm.
摘要翻译：具有阻燃性能的天然纤维素纤维的制造包括以下步骤。混合纸浆和N-甲基吗啉N-氧化物（NMMO）的溶剂形成浆料。通过薄膜蒸发器（TFE）从浆料中蒸发额外的水分以形成涂料。通过干喷射湿纺丝，旋转和挤出胶束用于凝结和再生。水冲洗干燥，形成天然纤维素纤维。通过N-（羟甲基）-3-（甲氧基磷酰基）的阻燃剂浸泡辊天然纤维素纤维。有序干燥，烘烤，中和，皂洗清洁，水冲洗，烘干，浸泡滚动，碱性清洁，水冲洗，干燥和油状天然纤维素纤维，生产天然纤维素纤维的阻燃能力。由于N-（羟甲基）-3-（甲氧基磷酰基）与天然纤维素纤维的阻燃剂的交联反应，其阻燃性能符合美国ASTM D6413-1999和ASTM D2863- 1995年。此外，其废物符合环保要求，无损害。

6. 发明授权

US08366988B2 Spunbond wetlaid method for producing non-woven fabrics from natural cellulose 有权
标题翻译：用天然纤维素生产无纺织物的纺粘湿法成网法
公开(公告)号：US08366988B2
公开(公告)日：2013-02-05
申请号：US12873343
申请日：2010-09-01
申请人： Wen-Tung Chou , Ming-Yi Lai , Kun-Shan Huang
发明人： Wen-Tung Chou , Ming-Yi Lai , Kun-Shan Huang
IPC分类号： D01D5/06 , D01D5/12 , D01D10/06 , D01F2/02 , D04H3/10
CPC分类号： D01F2/00 , B29C47/0014 , B29C47/8895 , C08B1/003 , D01D5/06 , D01D5/14 , D04H3/013 , D04H3/11 , D04H3/16
摘要： The present invention provides a “spunbond wetlaid method for producing non-woven fabrics from natural cellulose” using pulp as raw material and N-methylmorpholine N-oxide (NMMO) as solvent for dissolving into dope. Then, the dope is extruded out of a spinneret to form filament bundle by spunbond method. The dope is extruded out of a spinneret bank of grouped spinnerets to form filament bundle for further stretching process under quench condition. The filament bundle is coagulated with regeneration in a coagulating solution. The coagulated filament bundle is rapidly stretched under high pressure by an air draw-off machine. The stretched filament bundle is collected and stacked on a collecting net as web nonwoven. After post treatments of water rinsing, hydro-entangled needle punching, drying, winding-up and the like have been orderly applied then final product of nonwoven fabrics with continuous filament are produced from natural cellulose.
摘要翻译：本发明提供一种纺丝湿法成网方法，用于使用纸浆作原料和N-甲基吗啉N-氧化物（NMMO）作为用于溶解的溶剂的天然纤维素生产无纺布。然后将纺丝液从喷丝头挤出，通过纺粘法形成丝束。将纺丝液从喷丝板组中挤出，形成丝束，以在骤冷条件下进一步拉伸。细丝束在凝固溶液中再生凝结。凝结丝束在高压下通过空气抽出机快速拉伸。将拉伸的长丝束收集并堆叠在作为纤维网无纺布的收集网上。经过水洗后处理，水缠结针刺，干燥，卷绕等有序应用，然后由天然纤维素生产具有连续长丝的非织造织物的最终产品。

7. 发明申请

US20110156299A1 MELTBLOWN WETLAID METHOD FOR PRODUCING NON-WOVEN FABRICS WITH ANTI-MILDEW, ANTI-BACTERIA AND DEODORIZING CAPABILITIES FROM NATURAL CELLULOSE 有权
标题翻译：用于生产具有抗微生物，抗细菌和从天然纤维素中除去能力的非织造织物的熔融湿巾方法
公开(公告)号：US20110156299A1
公开(公告)日：2011-06-30
申请号：US12879042
申请日：2010-09-10
申请人： Wen-Tung CHOU , Ming-Yi Lai , Kun-Shan Huang
发明人： Wen-Tung CHOU , Ming-Yi Lai , Kun-Shan Huang
IPC分类号： D04H3/10
CPC分类号： D04H3/015 , D01D5/06 , D01D5/14 , D01F2/00 , D04H3/013 , D04H3/105
摘要： The present invention provides a meltblown wetlaid method for producing non-woven fabrics with anti-mildew, anti-bacteria and deodorizing capabilities from natural cellulose. The method comprises selecting wood pulp as raw material and using N-methylmorpholine N-oxide (NMMO) as dissolving solvent and 1,3-phenylene-bis 2-oxazoline (BOX) as stabilizer to form mixed cellulose mucilage as well as using modified and nano-miniaturized natural chitosan as additive for blending and dissolution to form cellulose dope. By meltblown method, the dope is extruded out of spinnerets to form filament bundle, then by ejecting mist aerosol of water, the filament bundle is coagulated with regeneration. After post treatments of water rinsing, hydro-entangled needle punching, drying, winding-up and the like having been orderly applied, then final product for nonwoven fabric of continuous filament with anti-mildew, anti-bacteria and deodorizing capabilities is produced.
摘要翻译：本发明提供一种用于生产具有抗天然纤维素的抗霉菌，抗细菌和除臭能力的无纺织物的熔喷湿法湿法。该方法包括选择木浆为原料，以N-甲基吗啉N-氧化物（NMMO）为溶剂，1,3-亚苯基 - 双2-恶唑啉（BOX）为稳定剂，形成混合纤维素胶浆，纳米微型化天然壳聚糖作为掺合和溶解形成纤维素掺杂剂的添加剂。通过熔喷方法，将纺丝液从喷丝头挤出形成丝束，然后通过喷雾雾气雾化，丝束与再生凝结。经过有序应用的水洗，水缠结针刺，干燥，卷绕等后处理后，生产具有抗霉菌，抗细菌和除臭能力的连续长丝无纺织物的最终产品。

8. 发明授权

US08092732B2 Processing method of the natural cellulose fiber with feature for enhancing the capability of antifungi, antibacteria and deodorization 有权
标题翻译：天然纤维素纤维的加工方法具有增强抗真菌，抗细菌和除臭能力的特点
公开(公告)号：US08092732B2
公开(公告)日：2012-01-10
申请号：US12318549
申请日：2008-12-31
申请人： Wen-Tung Chou , Ming-Yi Lai , Kun-Shan Huang
发明人： Wen-Tung Chou , Ming-Yi Lai , Kun-Shan Huang
IPC分类号： B29C47/00 , C08B37/08 , D01D5/12 , C07H1/00
CPC分类号： D01F2/00 , C08B37/003 , C08L5/08
摘要： The present invention provides a processing method of the natural cellulose fiber with feature for enhancing the capability of antifungi, antibacteria and deodorization. The procedure is that firstly modify and reduce the properties of the natural chitosan of high polymer material to nanometer scale; secondly dunk the chitosan into the syrup-like mixture of wood pulp and NMMO solvent to yield quasi-dope; thirdly dehydrate the quasi-dope of paste mixture to form the mud-like dope; fourthly spin the dope by dryjet wet spinning method; fifthly regenerate the filament in coagulation bath, water rinse and dry; finally water rinse, dry, apply the lubricant to finish. The water soluble chitosan, which has been treated by property modification and reduced to nanometer scale, can effectively and completely solve in the cellulose of low DP to offer wider extent of selection in the DP and better flexibility of adding percentage in content of modified chitosan.
摘要翻译：本发明提供天然纤维素纤维的加工方法，其特征在于提高抗真菌，抗细菌和除臭的能力。该方法首先将高分子材料天然壳聚糖的性能修饰降低至纳米级; 二次将壳聚糖浸入木浆和NMMO溶剂的糖浆状混合物中以产生准涂料; 第三次将糊状混合物的糊状物脱水形成泥状涂料; 第四次通过干喷射湿法纺丝纺丝原料; 第五次在凝固浴中再生细丝，水冲洗干燥; 最后用水冲洗干燥，涂抹润滑剂。已经通过性能改性处理并降低到纳米级的水溶性壳聚糖可以在低DP纤维素中有效和完全地解决DP，在DP中提供更广泛的选择范围，并且更好地增加改性壳聚糖含量百分比的灵活性。

9. 发明申请

US20110156303A1 SPUNBOND WETLAID METHOD FOR PRODUCING NON-WOVEN FABRICS FROM NATURAL CELLULOSE 有权
标题翻译：用于从天然纤维素生产非织造布的SPUNBOND WETLAID方法
公开(公告)号：US20110156303A1
公开(公告)日：2011-06-30
申请号：US12873343
申请日：2010-09-01
申请人： Wen-Tung CHOU , Ming-Yi Lai , Kun-Shan Huang
发明人： Wen-Tung CHOU , Ming-Yi Lai , Kun-Shan Huang
IPC分类号： B29C47/88
CPC分类号： D01F2/00 , B29C47/0014 , B29C47/8895 , C08B1/003 , D01D5/06 , D01D5/14 , D04H3/013 , D04H3/11 , D04H3/16
摘要： The present invention provides a “spunbond wetlaid method for producing non-woven fabrics from natural cellulose” using pulp as raw material and N-methylmorpholine N-oxide (NMMO) as solvent for dissolving into dope. Then, the dope is extruded out of a spinneret to form filament bundle by spunbond method. The dope is extruded out of a spinneret bank of grouped spinnerets to form filament bundle for further stretching process under quench condition. The filament bundle is coagulated with regeneration in a coagulating solution. The coagulated filament bundle is rapidly stretched under high pressure by an air draw-off machine. The stretched filament bundle is collected and stacked on a collecting net as web nonwoven. After post treatments of water rinsing, hydro-entangled needle punching, drying, winding-up and the like have been orderly applied then final product of nonwoven fabrics with continuous filament are produced from natural cellulose.
摘要翻译：本发明提供了使用纸浆作为原料的“天然纤维素的无纺织物的纺粘湿法成网法”和N-甲基吗啉N-氧化物（NMMO）作为溶剂溶解的溶剂。然后，将纺丝液从喷丝头挤出，通过纺粘法形成丝束。将纺丝液从喷丝板组中挤出，形成丝束，以在骤冷条件下进一步拉伸。细丝束在凝固溶液中再生凝结。凝结丝束在高压下通过空气抽出机快速拉伸。将拉伸的丝束收集并堆叠在作为纤维网无纺布的收集网上。经过水洗后处理，水缠结针刺，干燥，卷绕等有序应用，然后由天然纤维素生产具有连续长丝的非织造布的最终产品。

10. 发明申请

US20090166916A1 Processing method of the natural cellulose fiber with feature for enhancing the capability of antifungi, antibacteria and deodorization 有权
标题翻译：天然纤维素纤维的加工方法具有增强抗真菌，抗细菌和除臭能力的特点
公开(公告)号：US20090166916A1
公开(公告)日：2009-07-02
申请号：US12318549
申请日：2008-12-31
申请人： Wen-Tung Chou , Ming-Yi Lai , Kun-Shan Huang
发明人： Wen-Tung Chou , Ming-Yi Lai , Kun-Shan Huang
IPC分类号： B29C47/00
CPC分类号： D01F2/00 , C08B37/003 , C08L5/08
摘要： The present invention provides a processing method of the natural cellulose fiber with feature for enhancing the capability of antifungi, antibacteria and deodorization. The procedure is that firstly modify and reduce the properties of the natural chitosan of high polymer material to nanometer scale; secondly dunk the chitosan into the syrup-like mixture of wood pulp and NMMO solvent to yield quasi-dope; thirdly dehydrate the quasi-dope of paste mixture to form the mud-like dope; fourthly spin the dope by dryjet wet spinning method; fifthly regenerate the filament in coagulation bath, water rinse and dry; finally water rinse, dry, apply the lubricant to finish. The water soluble chitosan, which has been treated by property modification and reduced to nanometer scale, can effectively and completely solve in the cellulose of low DP to offer wider extent of selection in the DP and better flexibility of adding percentage in content of modified chitosan.
摘要翻译：本发明提供天然纤维素纤维的加工方法，其特征在于提高抗真菌，抗细菌和除臭的能力。该方法首先将高分子材料天然壳聚糖的性能修饰降低至纳米级; 二次将壳聚糖浸入木浆和NMMO溶剂的糖浆状混合物中以产生准涂料; 第三次将糊状混合物的糊状物脱水形成泥状涂料; 第四次通过干喷射湿法纺丝纺丝原料; 第五次在凝固浴中再生细丝，水冲洗干燥; 最后用水冲洗干燥，涂抹润滑剂。已经通过性能改性处理并降低到纳米级的水溶性壳聚糖可以在低DP纤维素中有效和完全地解决DP，在DP中提供更广泛的选择范围，并且更好地增加改性壳聚糖含量百分比的灵活性。

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