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1. 发明授权

US07122605B2 Method for selective graft polymerization 有权
公开(公告)号：US07122605B2
公开(公告)日：2006-10-17
申请号：US09998365
申请日：2001-11-29
申请人： Walter H. Ohrbom , Patricia A. Herrel , John W. Rehfuss
发明人： Walter H. Ohrbom , Patricia A. Herrel , John W. Rehfuss
IPC分类号： C08F283/01 , C08F265/04 , C08F8/32
CPC分类号： C08F8/30
摘要： The invention relates to a method of making an acrylic graft polymer, especially a urethanized acrylic graft polymer. The method of the invention requires an ethylenically unsaturated monomer mixture (a) comprising a monomer (ai) of a particular structure having at least one cyclic carbonate group and the polymerization of the monomer mixture (a) under free radical polymerization conditions to make an acrylic backbone polymer (b) comprising one or more cyclic carbonate functional groups (bi). At least one grafting moiety (c) is then provided, said grafting moiety (c) comprising at least one amine group (ci) selected from primary amines, secondary amines, and mixtures of both primary and secondary amines. The grafting moiety (c) is then grafted onto acrylic backbone polymer (b) via reaction between the at least one amine group (ci) and cyclic carbonate functional groups (bi) so as to make an urethanized acrylic graft polymer.

2. 发明授权

US06825286B2 Method for determining the water solubility or water dispersibility of waterborne beta-hydroxy primary carbamate functional graft materials 失效
标题翻译：测定水性β-羟基伯氨基甲酸酯官能接枝材料的水溶性或水分散性的方法
公开(公告)号：US06825286B2
公开(公告)日：2004-11-30
申请号：US10325301
申请日：2002-12-20
申请人： Walter H. Ohrbom , Patricia A. Herrel
发明人： Walter H. Ohrbom , Patricia A. Herrel
IPC分类号： C08F830
CPC分类号： C08G18/792 , C08F8/30 , C08G18/284 , C08G71/04
摘要： The invention relates to a method of making waterborne multifunctional materials, especially waterborne multifunctional materials comprising at least one primary carbamate group and a grafting moiety (cii). The method of the invention requires the successive or simultaneous reactions of a material P with a grafting material (c) and ammonia. Material P comprises two or more cyclic carbonate groups (bi). Grafting material (c) comprises at least one amine group (ci) and a grafting moiety (cii). The amine group (ci) is selected from primary amines, secondary amines, and mixtures thereof. The resulting waterborne multifunctional materials may be water dispersible, water soluble and/or useful in electrodeposition coatings.
摘要翻译：本发明涉及一种制备水性多功能材料的方法，特别是包含至少一种伯氨基甲酸酯基和接枝部分（cii）的水性多功能材料。本发明的方法需要材料P与接枝材料（c）和氨的连续或同时的反应。材料P包含两个或更多个环状碳酸酯基团（bi）。接枝材料（c）包含至少一个胺基（ci）和接枝部分（cii）。胺基（ci）选自伯胺，仲胺及其混合物。所得到的水性多功能材料可以是水分散性的，水溶性的和/或可用于电沉积涂料。

3. 发明授权

US06624241B2 Waterborne coating compositions containing materials dispersed with water-soluble carbamate materials 失效
公开(公告)号：US06624241B2
公开(公告)日：2003-09-23
申请号：US10061013
申请日：2002-01-30
申请人： Robert D. Weise , Walter H. Ohrbom , Patricia A. Herrel , David J. Law
发明人： Robert D. Weise , Walter H. Ohrbom , Patricia A. Herrel , David J. Law
IPC分类号： C08G1806
CPC分类号： C07C271/12 , C08F20/36 , C08G18/282 , C08G18/3831 , C09D161/28 , C09D201/025 , Y10T428/31551 , Y10T428/31605 , Y10T428/31725 , Y10T428/31855
摘要： The invention provides an aqueous coating composition containing a dispersed, emulsified, or dissolved material (organic compound, resin, or polymer), in which the material is dispersed, emulsified, or dissolved with a water-soluble, carbamate-functional material. The invention further provides a coating prepared from the coating composition and a coated substrate, especially an automotive substrate, having the coating thereon.

4. 发明授权

US06346591B1 Monomer and polymerization process 有权
公开(公告)号：US06346591B1
公开(公告)日：2002-02-12
申请号：US09316591
申请日：1999-05-21
申请人： Walter H Ohrbom , Patricia A. Herrel
发明人： Walter H Ohrbom , Patricia A. Herrel
IPC分类号： C08F22602
CPC分类号： C07C271/12 , C08F20/36 , C09D201/025
摘要： The &bgr;-hydroxy carbamate, ethylenically unsaturated monomer of the invention can be polymerized as a homopolymer or copolymerized with other monomers. The polymerization can be carried out in an aqueous medium. The &bgr;-hydroxy carbamate monomer is polymerized to form water-soluble homopolymers or, if polymerized as a mixture with one or more comonomers, copolymers that are soluble, emulsifiable, or dispersible in water. The &bgr;-hydroxy carbamate monomer can be used as a replacement monomer for acrylamide.

5. 发明授权

US06962730B2 Coating composition containing crosslinkable monomeric difunctional compounds having at least thirty carbon atoms 有权
标题翻译：包含具有至少30个碳原子的可交联单体双官能化合物的涂料组合物
公开(公告)号：US06962730B2
公开(公告)日：2005-11-08
申请号：US10351079
申请日：2003-01-23
申请人： Walter H. Ohrbom , John A. Gilbert , Patricia A. Herrel , Marvin L. Green , Joanne Casale , Thomas G. Savino
发明人： Walter H. Ohrbom , John A. Gilbert , Patricia A. Herrel , Marvin L. Green , Joanne Casale , Thomas G. Savino
IPC分类号： C09D5/02 , C09D133/14 , C09D201/00 , C09D201/02 , B05D3/00
CPC分类号： C09D5/02 , C09D133/14 , C09D201/00 , C09D201/02 , C09D201/025
摘要： The invention provides coating compositions comprising a reactive component (a) which is substantially free of any heteratoms and is a not a crystalline solid at room temperature and which comprises from (i) 12 to 72 carbon atoms, and (ii) at least two functional groups, and (b) a crosslinking agent comprising a plurality of functional groups (iii) reactive with the functional groups (ii) of compound (a), wherein functional groups (ii) and (iii) are selected such that reaction there between produces a thermally irreversible chemical linkage. The coating compositions of the invention provide improved solids, chip resistance, flexibility and/or scratch & mar resistance while maintaining desirable and/or improved performance characteristics with regard to environmental etch, relative humidity, QCT, chip resistance, thermoshock resistance, cold crack resistance, adhesion and the like.
摘要翻译：本发明提供涂料组合物，其包含基本上不含任何杂原子的反应性组分（a），并且在室温下不是结晶固体，并且其包含（i）12至72个碳原子，和（ii）至少两个官能基团，和（b）包含与化合物（a）的官能团（ⅱ）反应的多个官能团（ⅲ）的交联剂，其中选择官能团（ⅱ）和（ⅲ），使得其中的反应产生热不可逆化学键。本发明的涂料组合物在环境蚀刻，相对湿度，QCT，芯片电阻，耐热裂纹性，耐寒裂纹性方面保持理想和/或改进的性能特征，提供了改进的固体，耐芯片性，柔性和/ ，粘合等。

6. 发明授权

US06838530B2 Method of preparing various multifunctional materials using limited starting reactants 失效
标题翻译：使用有限起始反应物制备各种多功能材料的方法
公开(公告)号：US06838530B2
公开(公告)日：2005-01-04
申请号：US10325328
申请日：2002-12-20
申请人： Walter H. Ohrbom , Patricia A. Herrel
发明人： Walter H. Ohrbom , Patricia A. Herrel
IPC分类号： C08F2/00 , C08F8/30 , C08F8/32
CPC分类号： C08F8/30 , C08F8/32
摘要： The invention provides a method of making a number of different multifunctional acrylic materials from a limited number of starting materials. The method of the invention requires the product of a masterbatch of an acrylic oligomer or polymer having two or more cyclic carbonate functional groups. A first portion of the masterbatch is then reacted with ammonia and a grafting material (c) in either successive or simultaneous reactions to provide a first multifunctional acrylic oligomer or polymer. Additional portions of the masterbatch may be reacted with ammonia and other grafting materials (c), different from the first grafting material (c), in either successive or simultaneous reactions to provide different multifunctional acrylic oligomers or polymers.
摘要翻译：本发明提供从有限数量的原料制备许多不同的多官能丙烯酸类材料的方法。本发明的方法需要具有两个或更多个环状碳酸酯官能团的丙烯酸类低聚物或聚合物的母料的产品。然后在连续或同时反应中将母料的第一部分与氨和接枝材料（c）反应以提供第一多官能丙烯酸低聚物或聚合物。在连续或同时反应中，母料的另外部分可与氨和不同于第一接枝材料（c）的其它接枝材料（c）反应以提供不同的多官能丙烯酸低聚物或聚合物。

7. 发明授权

US06624279B2 Water-soluble carbamate materials 有权
公开(公告)号：US06624279B2
公开(公告)日：2003-09-23
申请号：US10042820
申请日：2002-01-09
申请人： Walter H. Ohrbom , David J. Law , Patricia A. Herrel
发明人： Walter H. Ohrbom , David J. Law , Patricia A. Herrel
IPC分类号： C08G1806
CPC分类号： C07C271/12 , C08F20/36 , C08G18/2815 , C08G18/3831 , C09D161/28 , C09D201/025 , Y10T428/31551 , Y10T428/31725 , Y10T428/31855
摘要： The invention provides water-soluble, &bgr;-hydroxy carbamate-functional materials and coating compositions, especially waterborne coating compositions, containing the carbamate-functional materials. The invention further provide a coating prepared from the coating composition and a coated substrate, especially an automotive substrate, having the coating thereon.

8. 发明授权

US07087675B2 Monomer and polymerization process 有权
公开(公告)号：US07087675B2
公开(公告)日：2006-08-08
申请号：US10391839
申请日：2003-03-19
申请人： Walter H. Ohrbom , Patricia A. Herrel
发明人： Walter H. Ohrbom , Patricia A. Herrel
IPC分类号： C08J3/00
CPC分类号： C07C271/12 , C08F20/36 , C09D201/025
摘要： The β-hydroxy carbamate, ethylenically unsaturated monomer of the invention can be polymerized as a homopolymer or copolymerized with other monomers. The polymerization can be carried out in an aqueous medium. The β-hydroxy carbamate monomer is polymerized to form water-soluble homopolymers or, if polymerized as a mixture with one or more comonomers, copolymers that are soluble, emulsifiable, or dispersible in water. The β-hydroxy carbamate monomer can be used as a replacement monomer for acrylamide.

9. 发明授权

US06566476B2 Monomer and polymerization process 有权
公开(公告)号：US06566476B2
公开(公告)日：2003-05-20
申请号：US09970752
申请日：2001-10-04
申请人： Walter H Ohrbom , Patricia A. Herrel
发明人： Walter H Ohrbom , Patricia A. Herrel
IPC分类号： C08F22602
CPC分类号： C07C271/12 , C08F20/36 , C09D201/025
摘要： The &bgr;-hydroxy carbamate, ethylenically unsaturated monomer of the invention can be polymerized as a homopolymer or copolymerized with other monomers. The polymerization can be carried out in an aqueous medium. The &bgr;-hydroxy carbamate monomer is polymerized to form water-soluble homopolymers or, if polymerized as a mixture with one or more comonomers, copolymers that are soluble, emulsifiable, or dispersible in water. The &bgr;-hydroxy carbamate monomer can be used as a replacement monomer for acrylamide.

10. 发明授权

US06812300B2 Method for making multifunctional materials 失效
标题翻译：制作多功能材料的方法
公开(公告)号：US06812300B2
公开(公告)日：2004-11-02
申请号：US10325304
申请日：2002-12-20
申请人： Walter H. Ohrbom , Patricia A. Herrel
发明人： Walter H. Ohrbom , Patricia A. Herrel
IPC分类号： C08F830
CPC分类号： C08F8/30
摘要： The invention relates to a method of making multifunctional materials, especially materials comprising at least one primary carbamate group and a grafting moiety (cii). The method of the invention requires the successive or simultaneous reactions of a material P with a grafting material (c) and ammonia. Material P comprises two or more cyclic carbonate groups (bi). Grafting material (c) comprises at least one amine group (ci) and a grafting moiety (cii). The amine group (ci) is selected from primary amines, secondary amines, and mixtures thereof. The resulting multifunctional materials are useful in a variety of curable coating compositions, including solventborne, waterborne, electrodeposition, liquid solvent free coatings, powder, and powder slurry.
摘要翻译：本发明涉及制备多功能材料的方法，特别是包含至少一种伯氨基甲酸酯基团和接枝部分（cii）的材料。本发明的方法需要材料P与接枝材料（c）和氨的连续或同时的反应。材料P包含两个或更多个环状碳酸酯基团（bi）。接枝材料（c）包含至少一个胺基（ci）和接枝部分（cii）。胺基（ci）选自伯胺，仲胺及其混合物。所得多功能材料可用于各种可固化涂料组合物，包括溶剂型，水性，电沉积，液体无溶剂涂料，粉末和粉末浆料。

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