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1. 发明授权

US4855309A Pyridine derivatives, agents containing same, and the use thereof as pesticides 失效
标题翻译：吡啶衍生物，含有它们的试剂，以及作为杀虫剂的用途
公开(公告)号：US4855309A
公开(公告)日：1989-08-08
申请号：US944323
申请日：1986-12-19
申请人： Volker Koch , Andreas Fuss , Werner Bonin , Werner Knauf , Anna Waltersdorfer
发明人： Volker Koch , Andreas Fuss , Werner Bonin , Werner Knauf , Anna Waltersdorfer
IPC分类号： A01N43/824 , A01N43/88 , A01N47/34 , A01N47/36 , C07D213/64 , C07D213/69 , C07D213/75 , C07D213/89 , C07D413/12
CPC分类号： C07D213/69 , A01N43/88 , A01N47/34 , C07D413/12
摘要： The compounds of the formula (I) ##STR1## in which A denotes N or N.fwdarw.0,R denotes a radical of the formula R.sup.4 --CY.sup.1 --NR.sup.5 --CY.sup.2 --NR.sup.6 --, ##STR2## R.sup.1 denotes halogen, alkyl, alkenyl, alkynyl, alkoxy, alkoxycarbonyl or alkylcarbonyl, where these radicals may be halogenated, nitro, cyano or carboxyl, R.sup.2 denotes halogenated alkoxy, halogenated alkenyloxy or halogenated alkynloxy, R.sup.3 denotes halogen, n denotes 0, 1 or 2, m denotes 0, 1, 2 or 3, and p denotes 0 or 1, and also the salts thereof, are advantageously suitable for combating noxious insects, acarides, nematodes or mollusks.
摘要翻译：式（I）化合物其中A表示N或N-> 0，R表示式为R4-CY1-NR5-CY2-NR6-，[IMAGE] R1表示卤素，烷基，烯基，炔基，烷氧基，烷氧基羰基或烷基羰基，其中这些基团可以被卤化，硝基，氰基或羧基，R2表示卤代烷氧基，卤代烯氧基或卤代炔氧基，R3表示卤素，n表示0,1或2，m表示0,1,2或3，p表示0或1，其盐也有利于对抗有害昆虫，螨类，线虫或软体动物。

2. 发明授权

US5021578A Certain perfluoroloweralkoxy-2-pyridyloxy propionates having herbicidal activity 失效
标题翻译：某些具有除草活性的全氟低级烷氧基-2-吡啶氧基丙酸酯
公开(公告)号：US5021578A
公开(公告)日：1991-06-04
申请号：US314319
申请日：1989-02-22
申请人： Volker Koch , Lothar Willms , Andreas Fuss , Klaus Bauer , Hermann Bieringer , Helmut Burstell
发明人： Volker Koch , Lothar Willms , Andreas Fuss , Klaus Bauer , Hermann Bieringer , Helmut Burstell
IPC分类号： C07D213/64 , A01N43/40 , A01N47/02 , A01N53/04 , C07D213/69 , C07D213/89
CPC分类号： C07D213/69 , A01N43/40 , A01N47/02
摘要： Compounds of the formula ##STR1## in which R.sup.1 denotes haloalkyl, haloalkenyl or haloalkynyl, (R.sup.2).sub.n denotes H or up to 3 halogens, A denotes N or N.fwdarw.0, R.sup.3 denotes H or alkyl, and Z denotes, inter alia, a carboxyl group or a functional derivative thereof, are valuable herbicides and growth regulators.
摘要翻译：其中R 1表示卤代烷基，卤代烯基或卤代炔基的式Ⅰ的化合物，（R2）n表示H或最多3个卤素，A表示N或N-> 0，R3表示H或烷基，Z表示羧基或其功能衍生物，特别是有价值的除草剂和生长调节剂。

3. 发明授权

US4756739A Pyridine derivatives and the N-oxides thereof, and the use thereof as intermediates for the synthesis of plant protecting agents 失效
标题翻译：吡啶衍生物及其N-氧化物及其作为植物保护剂合成中间体的用途
公开(公告)号：US4756739A
公开(公告)日：1988-07-12
申请号：US944547
申请日：1986-12-19
申请人： Andreas Fuss , Volker Koch
发明人： Andreas Fuss , Volker Koch
IPC分类号： A01N43/40 , A01N47/02 , A01N47/40 , C07D213/65 , C07D213/68 , C07D213/69 , C07D213/73 , C07D213/77 , C07D213/89 , C07D213/60 , C07D213/62 , C07F9/28
CPC分类号： C07D213/69 , A01N43/40 , A01N47/02 , A01N47/40 , C07D213/65 , C07D213/73 , C07D213/77 , C07D213/89
摘要： The compounds of the formula I ##STR1## in which A denotes N or N.fwdarw.O, Z denotes O or NH, R denotes H, (halo)alkyl, (halo)alkenyl, (halo)alkynyl or alkoxycarbonyl, R.sup.1 denotes hydrogen, halogen, amino, --NHOH, hydroxyl, (substituted) phenylazo or a radical of the formulae Y=C=N--, Y.sup.1 Y.sup.2 C.dbd.N--, Y.sup.3 NH-- or ##STR2## K denotes 0 or 1, and m and n, independently of one another, denote a number from 1 to 4, with the proviso that, when Z-R denotes OH or NH.sub.2, (R.sup.1).sub.n denotes at least one radical of the formula ##STR3## or represents two radicals, in the 5 or 6 position of the heterocyclic ring, which, in the 5 position, denote halogen and, in the 6 position, denote a radical of the group comprising halogen, amino, hydroxyl or phenylazo, which may be substituted as specified above, are valuable intermediates in the synthesis of plant protection agents.
摘要翻译：式I的化合物（I）其中A表示N或N-> O，Z表示O或NH，R表示H，（卤代）烷基，（卤代）烯基，（卤代）炔基或烷氧基羰基， R1表示氢，卤素，氨基，-NHOH，羟基，（取代的）苯偶氮或式Y = C = N-，Y1Y2C = N-，Y3NH-或K表示0或1的基团，m和 n彼此独立地表示1至4的数，条件是当ZR表示OH或NH 2时，（R1）n表示至少一个下式的基团，或表示两个基团，在5 或6位，其在5位表示卤素，并且在6位表示可以如上所述被取代的包含卤素，氨基，羟基或苯偶氮的基团的基团是有价值的中间体在植物保护剂的合成中。

4. 发明授权

US4727142A Process for the preparation of imidates 失效
标题翻译：亚胺化物的制备方法
公开(公告)号：US4727142A
公开(公告)日：1988-02-23
申请号：US853635
申请日：1986-04-18
申请人： Andreas Fuss , Gunter Siegemund
发明人： Andreas Fuss , Gunter Siegemund
IPC分类号： C07D207/34 , B01J27/00 , C07B61/00 , C07C67/00 , C07C241/00 , C07C253/00 , C07C255/61 , C07C257/04 , C07C325/00 , C07C327/58 , C07D207/32 , C07D207/335 , C07D213/53 , C07D213/65 , C07D213/69 , C07D213/81 , C07D213/82 , C07D277/74 , C07D295/13 , C07D307/68 , C07D333/22 , C07D333/38 , C07D521/00 , C07C119/18 , C07C119/20 , C07D401/00 , C07D409/00
CPC分类号： C07D207/335 , C07D213/53 , C07D213/69 , C07D295/13 , C07D307/68 , C07D333/22
摘要： The invention relates to a process for the preparation of compounds of the formula I and salts or acid addition compounds thereof ##STR1## in which R denotes hydrogen, (halogenated) alkyl with the exception of CF.sub.3, a (substituted) aromatic radical, (substituted) heteroaryl, (substituted) phenoxy, (substituted) phenylthio, (substituted) phenylamino, halogen, hydroxyl, alkoxy, mercapto, (halogenated) cycloalkyl, alkylmercapto, amino, monoalkylamino or dialkylamino,R.sup.1 denotes (substituted alkyl, (substituted) phenyl or naphthyl, alkenyl, alkinyl, cycloalkyl, (substituted) benzyl or heteroaryl, and X denotes oxygen or sulfur, which comprises reacting a nitrile of the formula II with a compound of the formula IIIR--C.tbd.N (II)R.sup.1 --XH (III) in the presence of anhydrous hydrofluoric acid, a perfluoroalkanecarboxylic acid, a perfluoralkanesulfonic acid or a perfluorinated ion exchanger containing sulfonic acids, and converting the resulting salts of the formula I, if appropriate by the addition of bases, into the free imidates of the formula I and, if approximate, converting the latter subsequently into further salts or acid addition compounds. The invention also relates to the new compounds of the formula I in which R.sup.1 denotes a (substituted) phenyl radical and R and X have the meanings mentioned. The compounds of the formula I are valuable intermediate products in the preparation of plant protection agents and pharmaceuticals.
摘要翻译：本发明涉及一种制备式I化合物的方法及其盐或酸加成化合物，其中R表示氢，（卤代）烷基，除CF 3，（取代的）芳族基团，（取代的）杂芳基，（取代的）苯氧基，（取代的）苯硫基，（取代的）苯基氨基，卤素，羟基，烷氧基，巯基，（卤代）环烷基，烷基巯基，氨基，单烷基氨基或二烷基氨基，）苯基或萘基，烯基，炔基，环烷基，（取代的）苄基或杂芳基，X表示氧或硫，其包括使式II的腈与式III的化合物RC 3BOND N（II）R1-XH （III）在无水氢氟酸，全氟烷烃羧酸，全氟烷基磺酸或含有磺酸的全氟化离子交换剂的存在下，如果合适的话，将所得的式I的盐转化成将碱的加入到式I的游离亚胺基中，并且如果接近，则将其转化成其后的盐或酸加成化合物。本发明还涉及式I的新化合物，其中R 1表示（取代的）苯基，R和X具有上述含义。式I的化合物是制备植物保护剂和药物的有价值的中间产物。

5. 发明授权

US5087725A Process for the preparation of alkyl nitrobenzoates 失效
标题翻译：制备硝基苯甲酸烷基酯的方法
公开(公告)号：US5087725A
公开(公告)日：1992-02-11
申请号：US513661
申请日：1990-04-24
申请人： Theodor Papenfuhs , Reiner Hess , Andreas Fuss
发明人： Theodor Papenfuhs , Reiner Hess , Andreas Fuss
IPC分类号： B01J31/02 , C07B61/00 , C07C201/12 , C07C205/57
CPC分类号： C07C201/12
摘要： A process for the preparation of alkyl (C.sub.1 -C.sub.3) nitrobenzoates by reacting the nitrobenzoic acid to be esterified with an excess of about 300 to about 600 mol % of an alkanol (C.sub.1 -C.sub.3) in a solvent which is inert towards the starting compounds and the reaction product in the presence of a polyfluoroalkanesulfonic acid of the general formula (1)Y(C.sub.n F.sub.2n)SO.sub.3 H (1)in which Y is a hydrogen or fluorine atom, with the proviso that, if Y is H, this hydrogen atom is in the .beta.-position relative to the sulfo group, or the hydrate thereof as catalyst in an amount of about 0.1 to about 20 mol %, relative to the nitrobenzoic acid used, at temperatures from about 60.degree. to about 120.degree. C.
摘要翻译：通过在对起始化合物是惰性的溶剂中使待酯化的硝基苯甲酸与过量约300至约600mol％的链烷醇（C1-C3）反应制备烷基（C 1 -C 3）硝基苯甲酸酯的方法和其中Y为氢或氟原子的通式（1）Y（C n F 2n）SO 3 H（1）的多氟烷基磺酸存在下的反应产物，条件是如果Y为H，则该氢原子为相对于所使用的硝基苯甲酸，在相对于磺基的β-位或其水合物作为催化剂的量为约0.1至约20mol％，温度为约60℃至约120℃。

6. 发明授权

US4924014A Process for the preparation of halogen-containing aromatic compounds 失效
标题翻译：制备含卤素芳香族化合物的方法
公开(公告)号：US4924014A
公开(公告)日：1990-05-08
申请号：US316794
申请日：1989-02-28
申请人： Andreas Fuss , Gunter Siegemund
发明人： Andreas Fuss , Gunter Siegemund
IPC分类号： C07D333/38 , B01J27/12 , C07B61/00 , C07C45/00 , C07C45/46 , C07C45/47 , C07C49/813 , C07C49/84 , C07C67/00 , C07C315/00 , C07C315/04 , C07C317/14 , C07D213/50
CPC分类号： C07C45/46 , C07C45/47 , C07C49/813 , C07C49/84
摘要： A process for the preparation of halogen-containing aromatic compounds of the formula I ##STR1## wherein Hal represents halogen,R represents H, C.sub.1 -C.sub.3 -alkyl, phenyl, halogen or trifluoromethyl,Y represents CO or SO.sub.2 andZ represents an aromatic or heteroaromatic group, andY-Z-Y together may also be CO or SO.sub.2, which comprises reacting a haloaromatic compound of the formula RC.sub.6 H.sub.4 Hal (II) with a halide of a bisacid having the formula Hal-Y-Z-Y-Hal (III) in a molar ratio of at least 2:1 in the presence of hydrogen fluoride and or boron trifluoride, in formulae II and III Hal, R, Y and Z having the aforementioned meaning.
摘要翻译：制备式I的含卤芳香族化合物的方法（I）其中Hal表示卤素，R表示H，C1-C3-烷基，苯基，卤素或三氟甲基，Y表示CO或SO2，Z表示芳族或杂芳族基团，YZY一起也可以是CO或SO 2，其包括使式RC6H4Hal（II）的卤代芳族化合物与式Hal-YZY-Hal（III）的二酸的卤化物的摩尔比在氟化氢和三氟化硼的存在下，在式II和III中具有上述含义的Hal，R，Y和Z的至少2:1。

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