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1. 发明授权

US3911164A Novel compounds and process 失效
标题翻译：新型化合物和工艺
公开(公告)号：US3911164A
公开(公告)日：1975-10-07
申请号：US39723773
申请日：1973-09-14
申请人： UPJOHN CO
发明人： SAYIGH ADNAN A R , STUBER FRED A , ULRICH HENRI
IPC分类号： C08F8/34 , D06P1/642 , D06P5/22 , G03F7/012 , B05D3/06 , C08J7/04 , C08J7/10
CPC分类号： G03F7/012 , C08F8/34 , D06P1/6423 , D06P5/22 , Y10T428/31786 , Y10T428/31859 , Y10T428/31942 , C08F222/06 , C08F222/08
摘要： Radiation (thermal and light)-sensitive polymers are provided which are characterized by the recurring unit of the formula:

wherein R'' is lower-alkoxy or phenyl; one of R2 and R3 is hydrogen and the other is

WHEREIN A alkylene from 2 to 10 carbon atoms having 2 to 6 carbon atoms between valencies, R'''' lower-alkyl or halogen, x is 1 to 2, y is 0 to 2, and x + y 1 to 3. Water soluble salts also disclosed. The polymers are useful for chemically bonding basic dyestuffs to non-dyereceptive substrates (e.g. polyethylene) by coating the substrate with radiation sensitive polymer and exposing the coated substrate to irradiation. The treated substrate is then contacted with a basic dyestuff which bonds thereto via the free carboxylic groups in the coating. The irradiation can be carried out imagewise to produce an appropriate image on the substrate which image is developed by dissolving out unexposed radiation-sensitive polymer prior to application of the dye. Bonding of the radiation-sensitive polymers of the invention to substrates in the above manner can also be employed as a means of rendering hydrophilic a variety of substrates which are hydrophobic.
摘要翻译：提供了辐射（热和光）敏感聚合物，其特征在于下式的重复单元：R'| - CH --- CH --- CH - CH2 - | COOR2COOR3其中R' 烷氧基或苯基; R 2和R 3中的一个是氢，另一个是O（SO 2 N 3）x并联-AOC-NH-角“R”，其中A是2价之间碳原子数2至10个的碳原子之间的亚芳基，R“= 低级烷基或卤素，x为1至2，y为0至2，x + y = 1至3.还公开了水溶性盐。聚合物可用于通过用辐射敏感聚合物涂覆基底并将涂覆的基底暴露于照射来将碱性染料化学键合到非感染性底物（例如聚乙烯）。然后将经处理的基材与经由涂层中的游离羧基与其键合的碱性染料接触。照射可以成像进行，以在衬底上产生合适的图像，该图像通过在施加染料之前溶解未曝光的辐射敏感聚合物来显影。本发明的辐射敏感性聚合物以上述方式粘合到基材上也可以用作亲水性的使疏水性的各种底物的方法。

2. 发明授权

US3879463A Substituted butadiene and hexatriene photosensitizers 失效
标题翻译：取代的丁二烯和己三烯光敏剂
公开(公告)号：US3879463A
公开(公告)日：1975-04-22
申请号：US35913273
申请日：1973-05-10
申请人： UPJOHN CO
发明人： PETERS JR GERRET M , STUBER FRED A , ULRICH HENRI
IPC分类号： C07F9/40 , G03F7/008 , G03F7/031 , C07C93/14 , C07C43/20 , C07C87/50
CPC分类号： C07F9/4056 , G03F7/0085 , G03F7/031
摘要： A novel class of compounds is disclosed of the formula

WHEREIN R1 and R2 are lower-alkoxy or di(lower-alkyl)amino and R2 can be hydrogen and R3 and R4 are hydrogen, lower-alkoxy or di(lower-alkyl)amino and n is an integer from 1 to 5. The compounds are sensitizers for photosensitive compounds particularly polymers containing sulfonazido groups as the lightsensitive moiety.
摘要翻译：公开了一类新颖的化合物，其中R 1和R 2是低级烷氧基或二（低级 - 烷基）氨基，R 2可以是氢，R 3和R 4是氢，低级烷氧基或二（低级 - 烷基）氨基， n为1至5的整数。这些化合物是感光性化合物的敏化剂，特别是含有磺酰胺基作为感光部分的聚合物。

3. 发明授权

US3652504A Radiation sensitive polyurethane 失效
标题翻译：辐射敏感聚氨酯
公开(公告)号：US3652504A
公开(公告)日：1972-03-28
申请号：US3652504D
申请日：1970-03-02
申请人： UPJOHN CO
发明人： SAYIGH ADNAN A R , STUBER FRED A , ULRICH HENRI
IPC分类号： C08G18/83 , C08G18/85 , C08J7/04 , C09D175/04
CPC分类号： C08J7/047 , C08G18/83 , C08G18/85 , C08J2475/00 , C09D175/04 , C08L2666/24
摘要： POLYURETHANE COATINGS ARE CHEMICALLY BONDED TO SUBSTRATES INCLUDING POLYOLEFIN AND LIKE SBSTRATES WITH WHICH POLYURETHANE WILL NOT NORMALLY REACT, BY INCORPORATING, INTO THE POLYURETHANE COATING COMPOSITION USED TO PREPARE THE COATING, FROM 0.1 PERCENT TO 10 PERCENT BY WEIGHT, BASED ON POLYURETHANE, OF A SULONYLAZIDE OF FORMULAE:

(((R)Y,(N3-O2S-)X-PHENYL)-NH-COO)-A AND

1,3,5-TRI((R)Y,(N3-O2S-)X-PHENYL),2,4,6-TRI(O=)-HEXAHYDRO-

S-TRIAZINE

WHEREIN A IS THE RESIDUE OF AN ALIPHATIC ALCOHOL HAVING M HYDROXYL GROUPS AN A MOLECULAR WEIGHT LESS THAN 300, R IS LOWER-ALKOXY OR HALO, X IS 1 TO 2, Y IS 0 TO 2 AND X+Y IS $3, THE SO2N3 GROUPS ARE IN 3, 4, OR5-POSITIONS IN THE PHENYL RINGS PROVIDED THAT ONE SUCH POSITION IS ALWAYS UNSUBSTITUTED AND M IS 1 TO 6. THE CHEMICAL BONDING CAN BE CARRIED OUT BY IRRADIATION IMAGEWISE THEREBY MAKING THE COMPOSITIONS USEFUL IN PHOTORESIST SYSTEMS.

4. 发明授权

US3583940A Polymers derived from acrylyl-substituted alkoxy stilbenes 失效
标题翻译：从丙烯酸取代的烷基酯衍生的聚合物
公开(公告)号：US3583940A
公开(公告)日：1971-06-08
申请号：US3583940D
申请日：1969-10-06
申请人： UPJOHN CO
发明人： RAO DURVASULA V , ULRICH HENRI , STUBER FRED A , SAYIGH ADNAN A R
IPC分类号： C07C205/56 , C08F2/00 , C08F12/14 , C08F20/34 , C08F20/54 , G03F7/038 , C08F7/02
CPC分类号： G03F7/0388 , C07C205/56 , C07C265/12 , C08F2/00 , C08F20/34 , C08F20/54
摘要： STILBENES OF THE FORMULA:

(LOWER ALKOXY)N,(CH2=C(-R)-(COO-A-O)M-CO-NH-PHENYLENE-

CH=CH-)-BENZENE

WHEREIN N IS AN INTEGER FROM 1 TO 3, M IS AN INTEGER FROM 0 TO 1, A IS LOWER-ALKYLENE AND R IS HYDROGEN OR LOWERALKYL, ARE DISCLOSED, AS WELL AS HOMOPOLYMERS OF SAID COMPOUNDS, AND COPOLYMERS OF SAID COMPOUNDS WITH MONOMERS CONTAINING A POLYMERIZABLE CH2=C

5. 发明授权

US3699080A Radiation sensitive polymers 失效
标题翻译：辐射敏感聚合物
公开(公告)号：US3699080A
公开(公告)日：1972-10-17
申请号：US3699080D
申请日：1970-11-27
申请人： UPJOHN CO
发明人： SAYIGH ADNAN A R , STUBER FRED A , ULRICH HENRI
IPC分类号： C08F8/00 , C08F8/34 , G03F1/56 , G03F7/012 , G03F7/038 , C08F27/06 , C08F27/08
CPC分类号： G03F7/038 , C08F8/00 , C08F8/34 , G03F1/56 , G03F7/012 , C08F20/02
摘要： RADIATION (THERMAL AND LIGHT)-SENSITIVE POLYMERS ARE PROVIDED AND ARE CHARACTERIZED BY (1) A RECURRING UNIT OF THE FORMULA:

-CH(-X)-CH(-Y)-CH(-R2)-CH2-

WHEREIN R2 IS LOWER-ALKOXY OR PHENYL, ONE OF X AND Y IS -COOR AND THE OTHER IS -COR1, R IS AND AZIDOSULFONYLCARBANILYLOXY ALKYLENE GROUP AND R1 IS -O-DYE, -NH-DYE OR HYDROXYARYLAMINO, OR (2) A COMBINATION IN THE SAME POLYME CHAIN OF RECURRING UNITS HAVING THE FORMULAE:

-CH(-X1)-CH(-Z1)-CH(-R2)-CH2-

WHEREIN ONE OF X1 AND Z1 REPRESENTS -COOH AND THE OTHER REPRESENTS -COOR AS DEFINED ABOVE, AND

-CH(-X2)-CH(-Z2)-CH(-R2)-CH2-

WHEREIN ONE OF X2 AND Z2 REPRESENTS -COOH AND THE OTHER REPRESENTS -COR1 AS REFINED ABOVE. THE POLYMERS CAN BE CHEMICALLY BONDED TO SUBSTRATES, SUCH AS THOSE CONTAINING C-H BONDS ONLY (E.G. POLYOLEFINS), WHICH ARE NOT NORMALLY DYE RECEPTIVE. THE BONDING IS EFFECTED BY EXPOSURE TO APPROPRIATE RADIATION; THE EXPOSURE CAN BY CARRIED OUT IMAGEWISE TO PRODUCE AN APPROPRIATE IMAGE ON THE SUBSTRATE. ACCORDINGLY, THE POLYMERS OF THE INVENTION FIND USE IN THE PHOTORESIST, PRINTING AND LIKE ARTS.

6. 发明授权

US3657199A Novel compositions 失效
标题翻译：新组合
公开(公告)号：US3657199A
公开(公告)日：1972-04-18
申请号：US3657199D
申请日：1970-11-27
申请人： UPJOHN CO
发明人： SAYIGH ADNAN A R , STUBER FRED A , ULRICH HENRI
IPC分类号： C08F8/00 , G03F7/038 , C08F27/08 , C08F27/12
CPC分类号： G03F7/0388 , C08F8/00 , C08F20/02
摘要： LIGHT SENSITIVE ESTER-AMIDE POLYMERS ARE PROVIDED. THE POLYMERS ARE CHARACTERIZED BY THE RECURRING UNIT:

-CH(-CO-R1)-CH(-CO-R2)-CH(-R")-CH2-

WHEREIN ONE OF R1 AND R2 REPRESENTS-O-(LOWER-ALKYL) AND THE OTHER OF R1 AND R2 REPRESENTS-NHR WHEREIN R IS A STILBENE RESIDUE HAVING THE FORMULA:

(LOWER-ALKOXY)N-(PHENYLENE)-CH=CH-(PHENYLENE)-

N=1 TO 3, AND R"=LOWER-ALKOXY OR PHENYL. THE POLYMERS HAVE AN AVERAGE MOLECULAR WEIGHT WITHIN THE RANGE OF ABOUT 100,000 TO ABOUT 1,250,000. THE ABOVE ESTERAMIDE POLYMERS UNDERGO CROSS-LINKING ON EXPOSURE TO ULTRAVIOLET LIGHT AND CAN BE USED IN PHOTO-RESIST SYSTEMS. THE ABOVE ESTER-AMIDE POLYMERS ARE PREPARED BY REACTING THE APPROPRIATE VINYL ETHER-MLEIC ANHYDRIDE OR STYRENEMALEIC ANHDRIDE COPOLYMER WITH THE APPROPRIATE AMINOSILBENE AND ESTERIFYING THE INTERMEDIATE AMIDE AMINE SALT WITH A LOWER-ALIPHATIC ALCOHOL.

7. 发明授权

US3652505A Radiation sensitive polyurethanes 失效
标题翻译：辐射敏感聚氨酯
公开(公告)号：US3652505A
公开(公告)日：1972-03-28
申请号：US3652505D
申请日：1970-03-02
申请人： UPJOHN CO
发明人： SAYIGH ADNAN A R , STUBER FRED A , ULRICH HENRI
IPC分类号： C08G18/38 , C08G18/71 , C08G22/04 , C08G22/16
CPC分类号： C08G18/715 , C08G18/3857
摘要： WHERE A=RESIDUE OF AN ALIPHATIC ALCOHOL OF VALENCY (M+N) AND M.W.
(((R)Y,(N3-O2S-)X-PHENYL)-NH-COO)-A-(OH)N

RADIATION (BOTH HEAT AND LIGHT)-SENSITIVE POLYURETHANES ARE PROVIDED AND ARE USEFUL IN THE PREPARATION OF COATINGS WHICH CAN BE CHEMICALLY BONDED, BY EXPOSURE TO AN APPROPRIATE SOURCE OF RADIATION TO SUBSTRATES CONTAINING C-H BONDS (PREFERRED SUBSTRATE ARE POLYOLEFINS). THE EXPOSURE CAN BE CARRIED OUT SELECTIVELY IN ACCORDANCE WITH PHOTORESIST SYSTEM TECHNOLOGY OR CAN BE CARRIED OUT OVER COMPLETE SURFACES SO AS TO BOND PAINT AND LIKE SEALANT COATINGS TO SUBSTRATE SUCH AS EXTERIOR BUILDING SURFACES AND THE LIKE. THE RADIATION-SENSITIVE POLYUTETHANES ARE DERIVED BY REPLACING PART OR THE WHOLE OF THE ACTIVE HYDROGEN CONTAINING COMPONENT, CONVENTIONALLY EMPLOYED TO FORM POLYURETHANES (BY REACTION WITH POLYISOCYANATES), BY A POLOY OF THE FORMULA:

8. 发明授权

US3644289A Light sensitive polyurethanes prepared from hydroxyl containing polymer and an isocyanato-stilbene compound 失效
标题翻译：含羟基聚合物和异氰脲酸酯化合物制备的光敏聚氨酯
公开(公告)号：US3644289A
公开(公告)日：1972-02-22
申请号：US3644289D
申请日：1969-05-29
申请人： UPJOHN CO
发明人： SAYIGH ADNAN A R , STUBER FRED A , ULRICH HENRI
IPC分类号： C08G18/48 , C08G18/54 , C08G18/62 , C08G18/81 , C08G22/00 , C08G22/22
CPC分类号： C08G18/6212 , C08G18/487 , C08G18/542 , C08G18/8108 , Y10S525/905
摘要： LIGHT-SENSITIVE POLYURETHANES ARE PREPARED BY REACTING (A) A POLYMER HAVING A FREE HYDROXYL GROUP IN THE RECURRING UNIT THEREOF WITH (B) AN ISOCVANATO-STILBENE OF THE FORMULA:

(LOWER ALKOXY)N,((OCN-PHENYL)-CH=CH-)BENZENE

WHEREIN N IS AN INTEGER FROM 1 TO 3. THE ABOVE POLYURETHANES UNDERGO CROSS-LINKING ON EXPOSURE TO ULTRAVIOLET LIGHT AND, ACCORDINGLY, CAN BE USED IN PHOTORESIST SYSTEMS.

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