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1. 发明授权

US08834603B2 Method for determining the degree of saturation of solid ammonia storage materials in containers 有权
标题翻译：确定容器中固体氨储存材料饱和度的方法
公开(公告)号：US08834603B2
公开(公告)日：2014-09-16
申请号：US13579375
申请日：2011-02-14
申请人： Tue Johannessen , Johnny Johansen , Jacob Hjerrild Zeuthen , Henning Schmidt , Ulrich Joachim Quaade
发明人： Tue Johannessen , Johnny Johansen , Jacob Hjerrild Zeuthen , Henning Schmidt , Ulrich Joachim Quaade
IPC分类号： F17C11/00 , C01C1/00
CPC分类号： B01D53/9495 , C01C1/006 , F01N3/208 , F01N2610/02 , F01N2610/06 , F01N2610/10 , F01N2610/1406 , F01N2900/0408 , F01N2900/1808 , F01N2900/1811 , G01N7/16 , Y02A50/2325 , Y02T10/24
摘要： A method is provided for estimating the degree of saturation (S) of a reversible solid ammonia storage material (3) in a storage unit (1). The storage unit (1) is equipped with a heater (2) to release ammonia and a connected tube (4) for ammonia flow. The initial temperature (TINIT) is measured with a sensor (9) in or around the storage unit (1) before any heating is initiated. Heating is initiated while recording the active time of heating (t) or the amount of energy (Q) released by the heater. The desorption pressure created by solid storage material in the storage unit (1) is measured via a pressure sensor (8) in fluid communication with the storage unit (1). The time (tTARGET), or the heat (QTARGET) where the pressure reaches a certain target pressure (PTARGET) is recorded. The values of the target-pressure time (tTARGET), or the target-pressure heat (QTARGET), and the initial temperature (TINIT) are used to compute an approximate degree of saturation (S).
摘要翻译：提供了一种用于估计存储单元（1）中的可逆固体氨储存材料（3）的饱和度（S）的方法。存储单元（1）配备有用于释放氨的加热器（2）和用于氨流动的连接管（4）。在开始任何加热之前，用存储单元（1）中或周围的传感器（9）测量初始温度（TINIT）。在记录加热的活动时间（t）或由加热器释放的能量（Q）的量时开始加热。通过与存储单元（1）流体连通的压力传感器（8）测量由储存单元（1）中的固体储存材料产生的解吸压力。记录压力达到一定目标压力（PTARGET）的时间（tTARGET）或热量（QTARGET）。使用目标压力时间（tTARGET）或目标压力热（QTARGET）和初始温度（TINIT）的值来计算近似饱和度（S）。

2. 发明申请

US20130209316A1 METHOD FOR DETERMINING THE DEGREE OF SATURATION OF SOLID AMMONIA STORAGE MATERIALS IN CONTAINERS 有权
标题翻译：用于确定容器中固体氨质储存材料饱和度的方法
公开(公告)号：US20130209316A1
公开(公告)日：2013-08-15
申请号：US13579375
申请日：2011-02-14
申请人： Tue Johannessen , Johnny Johansen , Jacob Hjerrild Zeuthen , Henning Schmidt , Ulrich Joachim Quaade
发明人： Tue Johannessen , Johnny Johansen , Jacob Hjerrild Zeuthen , Henning Schmidt , Ulrich Joachim Quaade
IPC分类号： B01D53/94 , G01N7/16
CPC分类号： B01D53/9495 , C01C1/006 , F01N3/208 , F01N2610/02 , F01N2610/06 , F01N2610/10 , F01N2610/1406 , F01N2900/0408 , F01N2900/1808 , F01N2900/1811 , G01N7/16 , Y02A50/2325 , Y02T10/24
摘要： A method is provided for estimating the degree of saturation (S) of a reversible solid ammonia storage material (3) in a storage unit (1). The storage unit (1) is equipped with a heater (2) to release ammonia and a connected tube (4) for ammonia flow. The initial temperature (TINIT) is measured with a sensor (9) in or around the storage unit (1) before any heating is initiated. Heating is initiated while recording the active time of heating (t) or the amount of energy (Q) released by the heater. The desorption pressure created by solid storage material in the storage unit (1) is measured via a pressure sensor (8) in fluid communication with the storage unit (1). The time (tTARGET), or the heat (QTARGET) where the pressure reaches a certain target pressure (PTARGET) is recorded. The values of the target-pressure time (tTARGET), or the target-pressure heat (QTARGET), and the initial temperature (TINIT) are used to compute an approximate degree of saturation (S).
摘要翻译：提供了一种用于估计存储单元（1）中的可逆固体氨储存材料（3）的饱和度（S）的方法。存储单元（1）配备有用于释放氨的加热器（2）和用于氨流动的连接管（4）。在开始任何加热之前，用存储单元（1）中或周围的传感器（9）测量初始温度（TINIT）。在记录加热的活动时间（t）或由加热器释放的能量（Q）的量时开始加热。通过与存储单元（1）流体连通的压力传感器（8）测量由储存单元（1）中的固体储存材料产生的解吸压力。记录压力达到一定目标压力（PTARGET）的时间（tTARGET）或热量（QTARGET）。使用目标压力时间（tTARGET）或目标压力热（QTARGET）和初始温度（TINIT）的值来计算近似饱和度（S）。

3. 发明申请

US20120288774A1 SYSTEM FOR STORING AMMONIA IN AND RELEASING AMMONIA FROM A STORAGE MATERIAL AND METHOD FOR STORING AND RELEASING AMMONIA 有权
标题翻译：用于储存氨和从存储材料中释放氨的系统和用于存储和释放氨的方法
公开(公告)号：US20120288774A1
公开(公告)日：2012-11-15
申请号：US13479402
申请日：2012-05-24
申请人： Tue Johannessen , Henning Schmidt
发明人： Tue Johannessen , Henning Schmidt
IPC分类号： B01J19/00 , B01D53/56 , C01C1/02 , H01M8/06
CPC分类号： F17C11/00 , B01D53/8631 , B01D53/90 , B01D53/9431 , B01D53/9495 , B01D2251/2062 , C01C1/006 , F01N3/2066 , F01N3/208 , F01N11/00 , F01N2560/026 , F01N2610/02 , F01N2610/06 , F01N2610/10 , F01N2610/14 , F01N2610/1406 , F01N2610/146 , F01N2900/0411 , F01N2900/08 , F01N2900/12 , F01N2900/1808 , F01N2900/1811 , F17C13/00 , F17C2221/01 , F17C2227/0302 , F17C2270/0581 , H01M8/0606 , H01M8/222 , Y02A50/2325 , Y02E60/321 , Y02T10/24
摘要： A system for storing ammonia in and releasing ammonia from a storage material capable of binding and releasing ammonia reversibly by adsorption or absorption for a process with a gradual ammonia demand that can vary over the time. The system has a container capable of housing the ammonia-containing storage material; a heating source arranged to supply heat for the desorption of ammonia from the solid storage medium; and a controller arranged to control the heating source to release ammonia. The heating source is arranged inside the container and surrounded by ammonia storage material. A controllable dosing valve is arranged to dose released ammonia according to the ammonia demand. The controller comprises a feed-forward control arranged to control the heat supplied by the heating source, based on the ammonia demand.
摘要翻译：一种用于将氨从储存材料中储存和释放氨的系统，该储存材料能够通过吸附或吸收可逆地结合和释放氨，以达到可随时间变化的逐渐氨需求的过程。该系统具有能容纳含氨储存材料的容器; 加热源，其设置用于从固体储存介质中提供氨以解吸氨; 以及控制器，其布置成控制加热源以释放氨。加热源设置在容器的内部并被氨储存材料包围。布置可控计量阀以根据氨需求量剂量释放氨。该控制器包括一个前馈控制装置，其基于氨的需求来控制由加热源供应的热量。

4. 发明申请

US20100086467A1 Release of Stored Ammonia at Start-Up 有权
标题翻译：储存氨在启动时释放
公开(公告)号：US20100086467A1
公开(公告)日：2010-04-08
申请号：US12553173
申请日：2009-09-03
申请人： Johnny Johansen , Jan Oeschsle , Henning Schmidt , Tue Johannessen , Jakob Svagin
发明人： Johnny Johansen , Jan Oeschsle , Henning Schmidt , Tue Johannessen , Jakob Svagin
IPC分类号： C01C1/00 , F17C9/02 , F17C11/00
CPC分类号： C01C1/006 , B01D2251/2062 , B01D2258/012 , B01D2258/014 , B01D2258/018 , F01N3/208 , F01N2610/02 , F01N2610/06 , F01N2610/10 , F01N2610/1406 , F01N2900/1808 , H01M8/04216 , H01M8/0606 , H01M8/222 , Y02T10/24
摘要： A system for storage and dosing of ammonia, including a solid ammonia storage material capable of binding and releasing ammonia reversibly by adsorption/absorption. The system is able to release ammonia gradually according to a demand that can vary over time with intermediate periods of no ammonia demand. A main storage unit and a start-up storage unit are provided. The storage units hold ammonia storage material. At least one one-way valve is provided via which the one main storage unit is in communication with the start-up storage unit. The one-way valve prevents any back-flow of ammonia from the start-up storage unit to the main storage unit. Heating devices are arranged to heat the main storage unit and the start-up storage unit separately to generate gaseous ammonia by thermal desorption from the solid storage material. A controller controls the heating power of the main storage unit and the start-up storage unit, thereby enabling ammonia release from at least one of the start-up and/or the main storage unit. A dosing valve controls ammonia flow from the storage units according to a demand.
摘要翻译：用于存储和计量氨的系统，包括能够通过吸附/吸收可逆地结合和释放氨的固体氨储存材料。该系统能够根据随时间变化的需求逐渐释放氨，而不需要氨中期。提供主存储单元和启动存储单元。储存装置容纳氨储存材料。提供至少一个单向阀，一个主存储单元通过该单向阀与启动存储单元连通。单向阀防止氨从启动存储单元向主存储单元的逆流。加热装置被布置成分开地加热主存储单元和启动存储单元，以通过从固体存储材料的热解吸产生气态氨。控制器控制主存储单元和启动存储单元的加热功率，从而能够从启动和/或主存储单元中的至少一个释放氨。计量阀根据需要控制存储单元的氨流量。

5. 发明申请

US20100050615A1 Efficient Release of Ammonia from a Solid Ammonia Storage Medium 审中-公开
标题翻译：从固体氨储存介质中高效释放氨
公开(公告)号：US20100050615A1
公开(公告)日：2010-03-04
申请号：US12374448
申请日：2007-07-19
申请人： Tue Johannessen , Henning Schmidt , Jens Kehlef Norskov , Claus Hviid Christensen
发明人： Tue Johannessen , Henning Schmidt , Jens Kehlef Norskov , Claus Hviid Christensen
IPC分类号： B01D53/94 , F01N3/20 , B01D53/90 , C01C1/02
CPC分类号： B01D53/90 , B01D53/9409 , C01C1/006 , F01N3/206 , F01N2610/06 , H01M8/04216 , H01M8/0606 , H01M8/222 , Y02A50/2325 , Y02T10/24
摘要： Solid metal ammine complexes are applied for safe and high-density storage of ammonia to be released for use as reducing agent in selective catalytic reduction of NOx in exhaust gases or as an energy carrier for fuel cell applications. The compositional formula of the metal ammine complexes is M(NH3)nXz, where Mz+ represents one or more metal ions capable of binding ammonia, X represents one or more anions, n is the coordination number (from 2 to 12), and z the valency of the metal ion (and thus the total number of compensating anion charges). Ammonia is released by controlled dosing of water into the storage container whereby ammonia is released because water replaces ammonia on the active sites capable of binding ammonia. Consequently, ammonia can be released without applying a normal thermal desorption of ammonia and the operating temperature of the system is reduced as well as the energy needed for releasing ammonia.
摘要翻译：应用固体金属氨络合物来安全和高密度地储存氨，以用作废气中NOx的选择性催化还原或作为燃料电池应用的能量载体的还原剂。金属络合物的组成式为M（NH 3）n X z，其中M z +表示一种或多种能结合氨的金属离子，X表示一种或多种阴离子，n为配位数（2至12），z为金属离子的化合价（因此补偿阴离子电荷的总数）。氨通过控制计量的水释放到储存容器中而释放，由此氨释放出能够结合氨的活性位上的氨。因此，可以释放氨，而不会对氨进行正常的热解吸，同时降低系统的工作温度以及释放氨所需的能量。

6. 发明授权

US08491842B2 Release of stored ammonia at start-up 有权
标题翻译：储存氨在启动时释放
公开(公告)号：US08491842B2
公开(公告)日：2013-07-23
申请号：US12553173
申请日：2009-09-03
申请人： Johnny Johansen , Jan Oechsle , Henning Schmidt , Tue Johannessen , Jakob Svagin
发明人： Johnny Johansen , Jan Oechsle , Henning Schmidt , Tue Johannessen , Jakob Svagin
IPC分类号： B01J19/00 , G05D23/00 , G05D16/00
CPC分类号： C01C1/006 , B01D2251/2062 , B01D2258/012 , B01D2258/014 , B01D2258/018 , F01N3/208 , F01N2610/02 , F01N2610/06 , F01N2610/10 , F01N2610/1406 , F01N2900/1808 , H01M8/04216 , H01M8/0606 , H01M8/222 , Y02T10/24
摘要： A system for storage and dosing of ammonia, including a solid ammonia storage material capable of binding and releasing ammonia reversibly by adsorption/absorption. The system is able to release ammonia gradually according to a demand that can vary over time with intermediate periods of no ammonia demand. A main storage unit and a start-up storage unit are provided. The storage units hold ammonia storage material. At least one one-way valve is provided via which the one main storage unit is in communication with the start-up storage unit. The one-way valve prevents any back-flow of ammonia from the start-up storage unit to the main storage unit. Heating devices are arranged to heat the main storage unit and the start-up storage unit separately to generate gaseous ammonia by thermal desorption from the solid storage material. A controller controls the heating power of the main storage unit and the start-up storage unit, thereby enabling ammonia release from at least one of the start-up and/or the main storage unit. A dosing valve controls ammonia flow from the storage units according to a demand.
摘要翻译：用于存储和计量氨的系统，包括能够通过吸附/吸收可逆地结合和释放氨的固体氨储存材料。该系统能够根据随时间变化的需求逐渐释放氨，而不需要氨中期。提供主存储单元和启动存储单元。储存装置容纳氨储存材料。提供至少一个单向阀，一个主存储单元通过该单向阀与启动存储单元连通。单向阀防止氨从启动存储单元向主存储单元的逆流。加热装置被布置成分开地加热主存储单元和启动存储单元，以通过从固体存储材料的热解吸产生气态氨。控制器控制主存储单元和启动存储单元的加热功率，从而能够从启动和/或主存储单元中的至少一个释放氨。计量阀根据需要控制存储单元的氨流量。

7. 发明申请

US20090313976A1 Method of Storing and Delivering Ammonia and the Use of Electromagnetic Radiation for Desorption of Ammonia from a Chemical Complex 有权
标题翻译：存储和提供氨的方法和使用电磁辐射从化学配合物中解吸氨
公开(公告)号：US20090313976A1
公开(公告)日：2009-12-24
申请号：US12279233
申请日：2002-02-27
申请人： Tue Johannessen , Rasmus Zink Sørensen , Claus Hviid Christensen , Ulrich Quaade , Jens Kehlet Nørskov , Henning Schmidt
发明人： Tue Johannessen , Rasmus Zink Sørensen , Claus Hviid Christensen , Ulrich Quaade , Jens Kehlet Nørskov , Henning Schmidt
IPC分类号： B01D53/90 , F17C9/02 , F17C11/00 , F01N3/20
CPC分类号： G09F19/22 , B01D53/90 , B01D53/9431 , B01D2251/2062 , B01D2259/80 , B01D2259/802 , B01D2259/804 , B01D2259/806 , B01J20/046 , B01J20/3433 , B01J20/3441 , C01C1/006 , F01N3/2066 , F01N2610/02 , F01N2610/06 , F01N2610/10 , F01N2610/1406 , G09F9/305 , G09F19/18 , Y02A50/2325 , Y02C20/10 , Y02T10/24
摘要： A method of storing and delivering ammonia and the use of electromagnetic radiation for desorption of ammonia from a chemical complex. Solid metal ammine complexes are applied for safe and high-density storage of ammonia to be released for use as reducing agent in selective catalytic reduction of NOx in exhaust gases. The compositional formula of the metal ammine complexes is M(NH3)nXz, where M2+ represents one or more metal ions capable of binding ammonia, X represents one or more anions, n is the coordination number (from 2 to 12), and z the valency of the metal ion (and thus the total number of compensating anion charges). Ammonia is released non-thermally by photon-activation using electromagnetic irradiation of the complex bond between ammonia coordinated to the metal ion
摘要翻译：一种储存和输送氨的方法，以及使用电磁辐射从化学络合物中解氨的方法。应用固体金属氨络合物用于安全和高密度地储存氨，以用作废气中选择性催化还原NOx的还原剂。金属络合物的组成式为M（NH 3）n X z，其中M 2 +表示一个或多个能结合氨的金属离子，X表示一个或多个阴离子，n为配位数（2至12），z为金属离子的化合价（因此补偿阴离子电荷的总数）。通过使用与金属离子配位的氨之间的复合键的电磁照射，通过光子激活而非热释放氨

8. 发明申请

US20150252949A1 SYSTEM FOR STORING AMMONIA IN AND RELEASING AMMONIA FROM A STORAGE MATERIAL AND METHOD FOR STORING AND RELEASING AMMONIA 审中-公开
标题翻译：用于储存氨和从存储材料中释放氨的系统和用于存储和释放氨的方法
公开(公告)号：US20150252949A1
公开(公告)日：2015-09-10
申请号：US14662910
申请日：2015-03-19
申请人： Tue Johannessen , Henning Schmidt
发明人： Tue Johannessen , Henning Schmidt
IPC分类号： F17C11/00 , F01N3/20 , F17C13/00 , H01M8/22 , B01D53/94 , F01N11/00 , H01M8/06
CPC分类号： F17C11/00 , B01D53/8631 , B01D53/90 , B01D53/9431 , B01D53/9495 , B01D2251/2062 , C01C1/006 , F01N3/2066 , F01N3/208 , F01N11/00 , F01N2560/026 , F01N2610/02 , F01N2610/06 , F01N2610/10 , F01N2610/14 , F01N2610/1406 , F01N2610/146 , F01N2900/0411 , F01N2900/08 , F01N2900/12 , F01N2900/1808 , F01N2900/1811 , F17C13/00 , F17C2221/01 , F17C2227/0302 , F17C2270/0581 , H01M8/0606 , H01M8/222 , Y02A50/2325 , Y02E60/321 , Y02T10/24
摘要： A system for storing ammonia in and releasing ammonia from a storage material capable of binding and releasing ammonia reversibly by adsorption or absorption for a process with a gradual ammonia demand that can vary over the time. The system has a container capable of housing the ammonia-containing storage material; a heating source arranged to supply heat for the desorption of ammonia from the solid storage medium; and a controller arranged to control the heating source to release ammonia. The heating source may be arranged inside the container and surrounded by ammonia storage material. A controllable dosing valve is arranged to dose released ammonia according to the ammonia demand. The controller comprises a feed-forward control arranged to control the heat supplied by the heating source, based on the ammonia demand.
摘要翻译：一种用于将氨从储存材料中储存和释放氨的系统，该储存材料能够通过吸附或吸收可逆地结合和释放氨，以达到可随时间变化的逐渐氨需求的过程。该系统具有能容纳含氨储存材料的容器; 加热源，其设置用于从固体储存介质中提供氨以解吸氨; 以及控制器，其布置成控制加热源以释放氨。加热源可以布置在容器内部并被氨储存材料包围。布置可控计量阀以根据氨需求量剂量释放氨。该控制器包括一个前馈控制装置，其基于氨的需求来控制由加热源供应的热量。

9. 发明授权

US08931262B2 Method and device for controlling effective heat transfer in a solid gas storage system 有权
标题翻译：用于控制固体气体存储系统中有效传热的方法和装置
公开(公告)号：US08931262B2
公开(公告)日：2015-01-13
申请号：US13634298
申请日：2011-03-16
申请人： Ulrich Joachim Quaade , Tue Johannessen , Jacob Hjerrild Zeuthen , Henning Schmidt
发明人： Ulrich Joachim Quaade , Tue Johannessen , Jacob Hjerrild Zeuthen , Henning Schmidt
IPC分类号： F01N3/00 , F01N3/10 , B01D53/02 , B01D53/12 , B65D85/00 , B65B3/00 , F01N3/20 , B01D53/04 , C01C1/00 , F17C11/00
CPC分类号： F01N3/208 , B01D53/0438 , B01D53/0454 , B01D2251/2062 , B01D2259/4525 , C01C1/006 , F17C11/00 , Y02P20/129
摘要： A method for controlling the effective heat transfer from a storage unit (1). During gas release from storage material (3) in the storage unit the storage material is heated by a heater (2). During re-saturation of the storage material (3) with gas the heater is off. Controlling of the effective heat transfer from the storage unit (1) is performed, during gas release, by ceasing convection of a convection gas and, during re-saturation, by performing or enabling convection of a convection gas to cool the storage unit (1).
摘要翻译：一种用于控制来自存储单元（1）的有效热传递的方法。在从存储单元中的储存材料（3）释放气体期间，储存材料由加热器（2）加热。在用气体重新饱和存储材料（3）时，加热器关闭。在气体释放期间，通过停止对流气体的对流并且在再饱和期间，通过执行或使对流气体对流以冷却存储单元（1）来控制来自存储单元（1）的有效热传递）。

10. 发明授权

US08578702B2 Method of storing and delivering ammonia and the use of electromagnetic radiation for desorption of ammonia from a chemical complex 有权
标题翻译：储存和输送氨的方法以及使用电磁辐射来从化学复合物中解氨
公开(公告)号：US08578702B2
公开(公告)日：2013-11-12
申请号：US12279233
申请日：2007-02-27
申请人： Tue Johannessen , Rasmus Zink Sørensen , Claus Hviid Christensen , Ulrich Quaade , Jens Kehlet Nørskov , Henning Schmidt
发明人： Tue Johannessen , Rasmus Zink Sørensen , Claus Hviid Christensen , Ulrich Quaade , Jens Kehlet Nørskov , Henning Schmidt
IPC分类号： F01N3/10
CPC分类号： G09F19/22 , B01D53/90 , B01D53/9431 , B01D2251/2062 , B01D2259/80 , B01D2259/802 , B01D2259/804 , B01D2259/806 , B01J20/046 , B01J20/3433 , B01J20/3441 , C01C1/006 , F01N3/2066 , F01N2610/02 , F01N2610/06 , F01N2610/10 , F01N2610/1406 , G09F9/305 , G09F19/18 , Y02A50/2325 , Y02C20/10 , Y02T10/24
摘要： A method of storing and delivering ammonia and the use of electromagnetic radiation for desorption of ammonia from a chemical complex. Solid metal ammine complexes are applied for safe and high-density storage of ammonia to be released for use as reducing agent in selective catalytic reduction of NOx in exhaust gases. The compositional formula of the metal ammine complexes is M(NH3)nXz, where M2+ represents one or more metal ions capable of binding ammonia, X represents one or more anions, n is the coordination number (from 2 to 12), and z the valency of the metal ion (and thus the total number of compensating anion charges). Ammonia is released non-thermally by photon-activation using electromagnetic irradiation of the complex bond between ammonia coordinated to the metal ion.
摘要翻译：一种储存和输送氨的方法，以及使用电磁辐射从化学络合物中解氨的方法。应用固体金属氨络合物用于安全和高密度地储存氨，以用作废气中选择性催化还原NOx的还原剂。金属络合物的组成式为M（NH 3）n X z，其中M 2 +表示一个或多个能结合氨的金属离子，X表示一个或多个阴离子，n为配位数（2至12），z为金属离子的化合价（因此补偿阴离子电荷的总数）。通过使用与金属离子配位的氨之间的复合键的电磁照射，通过光子激活而非热释放氨。

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