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1. 发明申请

US20120137965A1 VITREOUS SILICA CRUCIBLE FOR PULLING SILICON SINGLE CRYSTAL 有权
标题翻译：用于拉丝硅单晶的耐腐蚀二氧化硅
公开(公告)号：US20120137965A1
公开(公告)日：2012-06-07
申请号：US13387384
申请日：2010-07-28
申请人： Toshiaki Sudo , Masaru Sato
发明人： Toshiaki Sudo , Masaru Sato
IPC分类号： C30B15/10
CPC分类号： C03B19/095 , C30B15/10 , C30B29/06 , C30B35/002 , Y02P40/57 , Y10T117/1032
摘要： There is provided a vitreous silica crucible whose strength at high temperature is high, and which allows easy taking-out from a susceptor after completion of pulling. The vitreous silica crucible 10 includes a vitreous silica outer layer 13a provided on the outer surface side of the crucible, a vitreous silica inner layer 13c provided on the inner surface side of the crucible, and an vitreous silica intermediate layer 13b provided between the vitreous silica outer layer 13a and the vitreous silica inner layer 13c. The vitreous silica outer layer 13a has a mineralizer concentration of 100 ppm or more, and the vitreous silica intermediate layer 13b and the vitreous silica inner layer 13c has a mineralizer concentration of 50 ppm or less. It is preferred that the vitreous silica outer layer 13a and the vitreous silica intermediate layer 13b are made of natural silica, and the vitreous silica inner layer 13c is made of high-purity natural silica or synthetic silica. The thickness of the vitreous silica outer layer 13a is 0.5 mm to 2.0 mm on the bottom portion 10B, and the thickness on the sidewall portion 10A of the vitreous silica outer layer 13a is larger than that on the bottom portion 10B.
摘要翻译：本发明提供一种高温高强度的石英玻璃坩埚，能够在拉伸完成后从基座容易地取出。石英玻璃坩埚10包括设置在坩埚的外表面侧的玻璃态石英外层13a，设置在坩埚的内表面侧的玻璃态二氧化硅内层13c和设置在玻璃状二氧化硅外层13a和二氧化硅内层13c。氧化硅外层13a的矿化剂浓度为100ppm以上，玻璃状二氧化硅中间层13b和玻璃状内壁层13c的矿化剂浓度为50ppm以下。玻璃状二氧化硅外层13a和玻璃态二氧化硅中间层13b优选由天然二氧化硅制成，玻璃状内壁层13c由高纯度天然二氧化硅或合成二氧化硅制成。玻璃状二氧化硅外层13a的厚度在底部10B上为0.5mm〜2.0mm，玻璃状石英外层13a的侧壁部10A的厚度大于底部10B的厚度。

2. 发明授权

US09187357B2 Vitreous silica crucible having outer, intermediate, and inner layers 有权
标题翻译：具有外层，中层和内层的玻璃硅石坩埚
公开(公告)号：US09187357B2
公开(公告)日：2015-11-17
申请号：US13387384
申请日：2010-07-28
申请人： Toshiaki Sudo , Masaru Sato
发明人： Toshiaki Sudo , Masaru Sato
IPC分类号： C30B15/10 , C03B19/09 , C30B29/06 , C30B35/00
CPC分类号： C03B19/095 , C30B15/10 , C30B29/06 , C30B35/002 , Y02P40/57 , Y10T117/1032
摘要： A vitreous silica crucible has high strength at high temperature, and allows easy taking-out from a susceptor after completion of pulling. The vitreous silica crucible includes a vitreous silica outer layer provided on the outer surface side of the crucible, a vitreous silica inner layer provided on the inner surface side of the crucible, and an vitreous silica intermediate layer provided between the vitreous silica outer layer and the vitreous silica inner layer. The vitreous silica outer layer has a mineralizer concentration of 100 ppm or more, and the vitreous silica intermediate layer and the vitreous silica inner layer has a mineralizer concentration of 50 ppm or less. The thickness of the vitreous silica outer layer is 0.5 mm to 2.0 mm on the bottom portion, and the thickness on the sidewall portion of the vitreous silica outer layer is larger than that on the bottom portion.
摘要翻译：石英玻璃坩埚在高温下具有高强度，并且在拉伸完成之后容易从基座中取出。石英玻璃坩埚包括设置在坩埚的外表面侧的玻璃态石英外层，设置在坩埚的内表面侧的玻璃态二氧化硅内层和设置在玻璃状石英外层与玻璃状石英外层之间的玻璃态二氧化硅中间层，玻璃体二氧化硅内层。氧化硅玻璃外层的矿化剂浓度为100ppm以上，玻璃状二氧化硅中间层和玻璃状二氧化硅内层的矿化剂浓度为50ppm以下。玻璃体外层的厚度在底部为0.5mm〜2.0mm，玻璃状二氧化硅外层的侧壁部的厚度大于底部的厚度。

3. 发明授权

US09284207B2 Method of manufacturing granulated silica powder, method of manufacturing vitreous silica crucible 有权
标题翻译：造粒二氧化硅粉末的制造方法，石英坩埚的制造方法
公开(公告)号：US09284207B2
公开(公告)日：2016-03-15
申请号：US13308223
申请日：2011-11-30
申请人： Toshiaki Sudo , Takuma Yoshioka , Koichi Suzuki , Shinsuke Yamazaki
发明人： Toshiaki Sudo , Takuma Yoshioka , Koichi Suzuki , Shinsuke Yamazaki
IPC分类号： C03B19/01 , C03B19/09 , C03B19/06 , C03B20/00 , B02C23/00 , C03B1/02
CPC分类号： C03B1/02 , C03B19/095 , Y02P40/52
摘要： The present invention provides a method of manufacturing a vitreous silica crucible having a transparent layer by use of waste vitreous silica, and silica powder suitable for the manufacturing. According to the present invention, there is provided a method of manufacturing granulated silica powder comprising a process for pulverizing waste vitreous silica generated in the manufacturing process of a crucible to form silica fine powder having an average particle diameter of 100 μm or less, and a process for granulating the silica fine powder to obtain granulated silica powder having an average particle diameter of 50 μm or more under helium atmosphere.
摘要翻译：本发明提供一种通过使用废二氧化硅二氧化硅制造具有透明层的石英玻璃坩埚和适于制造的二氧化硅粉末的方法。根据本发明，提供了一种制造粒状二氧化硅粉末的方法，其包括在坩埚的制造过程中产生的废二氧化硅二氧化硅的粉碎方法，以形成平均粒径为100μm以下的二氧化硅细粉末，在二氧化硅细粉末上造粒的方法，得到氦气氛下平均粒径为50μm以上的粒状二氧化硅粉末。

4. 发明申请

US20120160155A1 COMPOSITE CRUCIBLE, METHOD OF MANUFACTURING THE SAME, AND METHOD OF MANUFACTURING SILICON CRYSTAL 有权
标题翻译：复合硬质合金，其制造方法和制造硅晶体的方法
公开(公告)号：US20120160155A1
公开(公告)日：2012-06-28
申请号：US13394268
申请日：2010-08-20
申请人： Toshiaki Sudo , Takuma Yoshioka , Hiroshi Kishi , Takeshi Fujita , Minoru Kanda , Koichi Suzuki , Ken Kitahara
发明人： Toshiaki Sudo , Takuma Yoshioka , Hiroshi Kishi , Takeshi Fujita , Minoru Kanda , Koichi Suzuki , Ken Kitahara
IPC分类号： C30B15/10 , C03B19/02 , C03B20/00
CPC分类号： C04B41/5022 , C03B5/025 , C03B19/02 , C03B19/09 , C03B19/095 , C03C17/004 , C03C17/02 , C03C2217/213 , C03C2218/13 , C03C2218/17 , C04B35/185 , C04B41/009 , C04B41/86 , C04B2235/6027 , C30B15/10 , C30B29/06 , C30B35/002 , Y02P40/57 , Y10T117/1032 , C04B41/4527
摘要： The purpose of the present invention is to provide a crucible which has high viscosity at high temperature, and can be used for a long time, and can be manufactured at low cost, and a method of manufacturing the same. The composite crucible 10 is characterized in the use of mullite (3Al2O3.2SiO2) as the basic material of the crucible. The composite crucible 10 has the crucible body 11 made of mullite material whose main component is alumina and silica, and a transparent vitreous silica layer 12 formed on the inner surface of the crucible body 11. The thickness of the transparent vitreous silica layer 12 is smaller than that of the crucible body 11. The crucible body 11 can be formed by the slip casting method, and the transparent vitreous silica layer 12 can be formed by the thermal spraying method.
摘要翻译：本发明的目的是提供一种在高温下具有高粘度且长时间使用并且可以低成本制造的坩埚及其制造方法。复合坩埚10的特征在于使用莫来石（3Al2O3.2SiO2）作为坩埚的基本材料。复合坩埚10具有由主成分为氧化铝和二氧化硅的莫来石材料制成的坩埚体11和形成在坩埚体11的内表面上的透明玻璃状石英层12.透明玻璃状石英层12的厚度较小坩埚主体11可以通过流延法形成，透明玻璃状二氧化硅层12可以通过热喷涂法形成。

5. 发明申请

US20120137732A1 METHOD OF MANUFACTURING GRANULATED SILICA POWDER, METHOD OF MANUFACTURING VITREOUS SILICA CRUCIBLE 有权
标题翻译：制造颗粒状二氧化硅粉末的方法，制造维生素二氧化硅可溶性的方法
公开(公告)号：US20120137732A1
公开(公告)日：2012-06-07
申请号：US13308223
申请日：2011-11-30
申请人： Toshiaki Sudo , Takuma Yoshioka , Koichi Suzuki , Shinsuke Yamazaki
发明人： Toshiaki Sudo , Takuma Yoshioka , Koichi Suzuki , Shinsuke Yamazaki
IPC分类号： C03B20/00 , B02C23/00 , C03B19/09 , C03B19/01 , C03B19/06
CPC分类号： C03B1/02 , C03B19/095 , Y02P40/52
摘要： The present invention provides a method of manufacturing a vitreous silica crucible having a transparent layer by use of waste vitreous silica, and silica powder suitable for the manufacturing. According to the present invention, there is provided a method of manufacturing granulated silica powder comprising a process for pulverizing waste vitreous silica generated in the manufacturing process of a crucible to form silica fine powder having an average particle diameter of 100 μm or less, and a process for granulating the silica fine powder to obtain granulated silica powder having an average particle diameter of 50 μm or more under helium atmosphere.
摘要翻译：本发明提供一种通过使用废二氧化硅二氧化硅制造具有透明层的石英玻璃坩埚和适于制造的二氧化硅粉末的方法。根据本发明，提供了一种制造粒状二氧化硅粉末的方法，其包括在坩埚的制造过程中产生的废二氧化硅二氧化硅的粉碎方法，以形成平均粒径为100μm以下的二氧化硅细粉末，在二氧化硅细粉末上造粒的方法，得到氦气氛下平均粒径为50μm以上的粒状二氧化硅粉末。

6. 发明申请

US20110295405A1 METHOD OF CALCULATING TEMPERATURE DISTRIBUTION OF CRUCIBLE 有权
标题翻译：计算可分解温度分布的方法
公开(公告)号：US20110295405A1
公开(公告)日：2011-12-01
申请号：US13147736
申请日：2010-12-14
申请人： Toshiaki Sudo , Eriko Suzuki , Naoki Ono
发明人： Toshiaki Sudo , Eriko Suzuki , Naoki Ono
IPC分类号： G06F19/00
CPC分类号： C03B19/095 , C30B15/10 , G06F17/5018 , G06F2217/80
摘要： Provided is a method of calculating a temperature distribution with higher accuracy than a conventional method, which calculates a temperature distribution of an inner surface of a silica powder molded body during manufacturing based on boundary conditions corrected in accordance with the actually measured temperature in consideration of plasma radiation by arc discharge and heat radiation of arc discharge.According to a method of calculating a temperature distribution of a crucible during manufacturing, includes a temperature calculation process in which a temperature calculator calculates temperature distribution in an inner surface of a silica powder molded body through a numerical calculation method which mesh-divides an object to be calculated, by calculating heat flux from heat plasma modeled by a gas flow and radiation of heat plasma radiated from arc electrodes, wherein the temperature distribution is calculated by adjusting gas flow and radiation conditions in a way that the calculated temperature distribution and the actually measured temperature distribution of an inner surface of a silica powder molded body becomes similar, and reading, from a correspondence table, gas flow and radiation conditions corresponding each step of a control sequence for producing a crucible.
摘要翻译：提供了一种比传统方法更高精度地计算温度分布的方法，该方法基于考虑到等离子体而根据实际测量的温度校正的边界条件计算制造期间二氧化硅粉末成型体的内表面的温度分布电弧放电辐射和放电电弧放电。根据制造时的坩埚的温度分布的计算方法，包括温度计算处理，其中温度计算器通过数值计算方法计算二氧化硅粉末成形体的内表面的温度分布，通过计算由通过气流和从电弧电极辐射的热等离子体的辐射建立的热等离子体的热通量来计算，其中通过以计算的温度分布和实际测量的方式调节气体流量和辐射条件来计算温度分布二氧化硅粉末成型体的内表面的温度分布变得相似，并且从对应表读取对应于用于制造坩埚的控制顺序的每个步骤的气体流量和辐射条件。

7. 发明授权

US4718016A Method of and system for controlling idling speed in electronically controlled engine 失效
标题翻译：电控发动机空转速度控制方法及系统
公开(公告)号：US4718016A
公开(公告)日：1988-01-05
申请号：US884905
申请日：1986-07-14
申请人： Toshiaki Sudo
发明人： Toshiaki Sudo
IPC分类号： F02D41/16 , F02D41/08 , F02D41/22 , F02D45/00 , F02D33/00
CPC分类号： F02D41/08 , F02D41/222 , Y02T10/40
摘要： In a method of and system for controlling an idling speed in an electronically controlled engine, wherein the idling speed is feedback-controlled in accordance with the operating condition of the engine, an idling speed feedback process and an engine speed upper limit setting process are prohibited when a vehicle speed detecting system has failed, so that erroneous control of the idling speed can be prevented from occurring during running of a vehicle.
摘要翻译：在电子控制发动机的怠速控制方法和系统中，怠速根据发动机的运转状况进行反馈控制，怠速反馈处理和发动机转速上限设定处理被禁止当车速检测系统发生故障时，能够防止在行驶中发生怠速的错误控制。

8. 发明授权

US09534318B2 Vitreous silica crucible and method of manufacturing the same 有权
标题翻译：石英玻璃坩埚及其制造方法
公开(公告)号：US09534318B2
公开(公告)日：2017-01-03
申请号：US13335885
申请日：2011-12-22
申请人： Toshiaki Sudo , Taira Sato , Shuichi Ikehata , Manabu Shonai , Takuji Nishi , Takaya Satou , Shinsuke Yamazaki
发明人： Toshiaki Sudo , Taira Sato , Shuichi Ikehata , Manabu Shonai , Takuji Nishi , Takaya Satou , Shinsuke Yamazaki
IPC分类号： C30B19/02 , C30B35/00 , C30B15/00
CPC分类号： C03C23/0025 , C03B19/095 , C30B15/00 , C30B15/10 , C30B35/002 , Y10T117/10
摘要： The present invention provides a method of manufacturing a vitreous silica crucible including: a taking-out process of taking out the vitreous silica crucible from the mold, a honing process of removing the unfused silica powder layer on the outer surface of the vitreous silica crucible, and further comprising, after the taking-out process and before the honing process, a marking process of marking an identifier comprised of one or more groove line on the outer surface of the vitreous silica crucible, wherein the groove line after the honing process has a depth of 0.2 to 0.5 mm, and a width of 0.8 mm or more at the opening of the groove line.
摘要翻译：本发明提供了一种制造石英玻璃坩埚的方法，包括：从模具中取出玻璃状石英坩埚的取出工序，除去石英玻璃坩埚外表面的未熔融二氧化硅粉末层的珩磨处理，并且还包括在所述取出处理之后并且在所述珩磨处理之前，对所述石英玻璃坩埚的外表面上的由一条或多条槽线组成的标识符进行标记处理，其中，所述珩磨处理后的所述槽线具有深度为0.2〜0.5mm，宽度为0.8mm以上。

9. 发明授权

US09115019B2 Vitreous silica crucible and method of manufacturing the same 有权
标题翻译：石英玻璃坩埚及其制造方法
公开(公告)号：US09115019B2
公开(公告)日：2015-08-25
申请号：US13145094
申请日：2010-12-14
申请人： Toshiaki Sudo , Hiroshi Kishi , Eriko Suzuki
发明人： Toshiaki Sudo , Hiroshi Kishi , Eriko Suzuki
IPC分类号： C03B19/06 , C03B19/09 , C03C15/00 , C03C23/00 , C30B15/10 , C30B29/06 , C30B35/00 , C03C17/23
CPC分类号： C03B19/095 , C03C15/00 , C03C17/23 , C03C23/0025 , C03C23/007 , C03C2218/345 , C30B15/10 , C30B29/06 , C30B35/002 , Y02P40/57 , Y10T117/1032
摘要： Provided is a method of manufacturing a vitreous silica crucible for pulling a silicon single crystal which can suppress melt surface vibration of silicon melt filled therein and has a long lifetime. The crucible includes a peripheral wall portion, a curved portion and a bottom portion, and has a plurality of micro recesses on the specific region of the inner surface of the peripheral wall portion.
摘要翻译：提供一种制造用于拉制硅单晶的石英玻璃坩埚的方法，其可以抑制填充在其中的硅熔体的熔融表面振动并且具有长的寿命。坩埚包括周壁部分，弯曲部分和底部部分，并且在周壁部分的内表面的特定区域上具有多个微凹部。

10. 发明授权

US09085480B2 Method of manufacturing vitreous silica crucible 有权
标题翻译：石英玻璃坩埚的制造方法
公开(公告)号：US09085480B2
公开(公告)日：2015-07-21
申请号：US13337918
申请日：2011-12-27
申请人： Toshiaki Sudo , Eriko Suzuki
发明人： Toshiaki Sudo , Eriko Suzuki
IPC分类号： C03B20/00 , C03B19/09
CPC分类号： C03B19/095
摘要： There is provided a method of manufacturing a vitreous silica crucible having a suitably controlled inner surface property. The present invention provides a method of manufacturing a vitreous silica crucible by heating and fusing a silica powder layer in a rotating mold by arc discharge generated by carbon electrodes including: a preparation process for determining optimal fusing temperatures during heating and fusing the silica powder layer at plural points of different heights of the silica powder layer; a temperature measuring process for measuring actual temperatures during heating and fusing the silica powder layer at the plural points; a temperature controlling process for controlling the actual temperatures at the plural points so that the actual temperatures matches the optimal fusing temperatures at the respective points.
摘要翻译：提供了一种具有适当控制的内表面性能的石英玻璃坩埚的制造方法。本发明提供一种通过碳化硅电极产生的电弧放电加热熔融旋转模具中的二氧化硅粉末层而制造石英玻璃坩埚的方法，包括：在加热和熔融二氧化硅粉末层期间确定最佳定影温度的制备方法二氧化硅粉末层的不同高度的多个点; 用于在多个点加热和熔融二氧化硅粉末层期间测量实际温度的温度测量过程; 用于控制多个点处的实际温度的温度控制过程，使得实际温度与各个点处的最佳定影温度相匹配。

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