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1. 发明申请

US20130197268A1 METHOD FOR PRODUCING NITROBENZENE BY ADIABATIC NITRIDING 有权
标题翻译：通过自制氮化生产硝基苯的方法
公开(公告)号：US20130197268A1
公开(公告)日：2013-08-01
申请号：US13812653
申请日：2011-07-26
申请人： Thomas Knauf , Alexandre Racoes , Andreas Karl Rausch , Dietrich Wulf
发明人： Thomas Knauf , Alexandre Racoes , Andreas Karl Rausch , Dietrich Wulf
IPC分类号： C07C201/08 , C07C209/32
CPC分类号： C07C201/08 , C07C209/325 , C07C209/36 , C07C205/06 , C07C211/46
摘要： The invention relates to a process for the continuous production of nitrobenzene by nitration of benzene with a mixture of nitric acid and sulfuric acid under adiabatic conditions, in which unreacted benzene is separated from the crude product obtained after phase separation before washing thereof, using the adiabatic heat of reaction.
摘要翻译：本发明涉及一种通过在绝热条件下用硝酸和硫酸的混合物硝化苯来连续生产硝基苯的方法，其中将未反应的苯与洗脱之前相分离后获得的粗产物分离，使用绝热反应热。

2. 发明授权

US08729309B2 Method for producing nitrobenzene by adiabatic nitriding 有权
标题翻译：通过绝热氮化生产硝基苯的方法
公开(公告)号：US08729309B2
公开(公告)日：2014-05-20
申请号：US13812653
申请日：2011-07-26
申请人： Thomas Knauf , Alexandre Racoes , Andreas Karl Rausch , Dietrich Wulf
发明人： Thomas Knauf , Alexandre Racoes , Andreas Karl Rausch , Dietrich Wulf
IPC分类号： C07B43/02 , C07C201/00 , C07C209/00
CPC分类号： C07C201/08 , C07C209/325 , C07C209/36 , C07C205/06 , C07C211/46
摘要： The invention relates to a process for the continuous production of nitrobenzene by nitration of benzene with a mixture of nitric acid and sulfuric acid under adiabatic conditions, in which unreacted benzene is separated from the crude product obtained after phase separation before washing thereof, using the adiabatic heat of reaction.
摘要翻译：本发明涉及一种通过在绝热条件下用硝酸和硫酸的混合物硝化苯来连续生产硝基苯的方法，其中将未反应的苯与洗脱之前相分离后获得的粗产物分离，使用绝热反应热。

3. 发明申请

US20090187051A1 Process for the preparation of nitrobenzene by adiabatic nitration 有权
标题翻译：通过绝热硝化制备硝基苯的方法
公开(公告)号：US20090187051A1
公开(公告)日：2009-07-23
申请号：US12315907
申请日：2008-12-08
申请人： Andreas Rausch , Thomas Knauf , Jeffrey Bolton , Alexandre Racoes
发明人： Andreas Rausch , Thomas Knauf , Jeffrey Bolton , Alexandre Racoes
IPC分类号： C07C205/06
CPC分类号： C07C201/08 , C07C205/06
摘要： This invention relates to a process for the continuous preparation of nitrobenzene. This process comprises the adiabatic nitration of benzene with a mixture of sulfuric acid and nitric acid, in which the sum of the concentrations in the reaction zone of the metal ions which form sparingly soluble metal sulfates is less than 900 mg/l, based on the volume of the aqueous phase which contains sulfuric acid.
摘要翻译：本发明涉及连续制备硝基苯的方法。该方法包括苯与硫酸和硝酸的混合物的绝热硝化，其中形成微溶金属硫酸盐的金属离子的反应区中的浓度之和小于900mg / l，基于含有硫酸的水相体积。

4. 发明授权

US07781624B2 Process for the preparation of nitrobenzene by adiabatic nitration 有权
标题翻译：通过绝热硝化制备硝基苯的方法
公开(公告)号：US07781624B2
公开(公告)日：2010-08-24
申请号：US12315907
申请日：2008-12-08
申请人： Andreas Rausch , Thomas Knauf , Jeffrey Bolton , Alexandre Racoes
发明人： Andreas Rausch , Thomas Knauf , Jeffrey Bolton , Alexandre Racoes
IPC分类号： C07C205/00
CPC分类号： C07C201/08 , C07C205/06
摘要： This invention relates to a process for the continuous preparation of nitrobenzene. This process comprises the adiabatic nitration of benzene with a mixture of sulfuric acid and nitric acid, in which the sum of the concentrations in the reaction zone of the metal ions which form sparingly soluble metal sulfates is less than 900 mg/l, based on the volume of the aqueous phase which contains sulfuric acid.
摘要翻译：本发明涉及连续制备硝基苯的方法。该方法包括苯与硫酸和硝酸的混合物的绝热硝化，其中形成微溶金属硫酸盐的金属离子的反应区中的浓度之和小于900mg / l，基于含有硫酸的水相体积。

5. 发明申请

US20130204043A1 METHOD FOR CONTINUOUSLY PRODUCING NITROBENZENE 审中-公开
标题翻译：连续生产硝基苯的方法
公开(公告)号：US20130204043A1
公开(公告)日：2013-08-08
申请号：US13812690
申请日：2011-07-26
申请人： Thomas Knauf , Michael Merkel , Andreas Karl Rausch , Peter Lehner , Jürgen Münnig
发明人： Thomas Knauf , Michael Merkel , Andreas Karl Rausch , Peter Lehner , Jürgen Münnig
IPC分类号： C07C201/14
CPC分类号： C07C201/14 , C07C201/08 , C07C201/16 , C07C209/36 , C07C205/06 , C07C211/46
摘要： The present invention relates to a continuous process for the production of nitrobenzene by nitration of benzene with nitric acid or mixtures of nitric acid and sulfuric acid to give a crude nitrobenzene, washing of the crude nitrobenzene by means of at least one of each of an acid, alkaline and neutral washing, there being obtained a pre-purified nitrobenzene which, as well as containing nitrobenzene, at least contains also low boilers, optionally middle boilers as well as high boilers and salts, wherein the pre-purified nitrobenzene is purified further by separating off low boilers in a distillation apparatus by evaporation of the low boilers, and separation of nitrobenzene from the resulting further purified nitrobenzene in a distillation apparatus by partial evaporation of nitrobenzene, wherein pure nitrobenzene is removed from the distillation apparatus in gaseous form and is subsequently condensed, and wherein the non-evaporated portion of the further purified nitrobenzene is fed back into the washing at any desired point.
摘要翻译：本发明涉及通过用硝酸或硝酸和硫酸的混合物硝化硝酸生产硝基苯的连续方法，得到粗硝基苯，通过以下各项中的至少一种酸洗粗硝基苯碱性和中性洗涤，得到预纯化的硝基苯以及含有硝基苯，至少还含有低锅炉，任选的中间锅炉以及高锅炉和盐，其中预纯化的硝基苯进一步通过通过蒸发低沸点锅炉将蒸馏装置中的低锅炉分离出来，并通过硝基苯的部分蒸发在蒸馏装置中将硝基苯与所得到的进一步纯化的硝基苯分离，其中将纯硝基苯以气态从蒸馏装置中除去，随后冷凝，并且其中进一步纯化的硝基苯的未蒸发部分进料回到任何想要的点的洗涤。

6. 发明授权

US07763759B2 Continuous process for the manufacture of nitrobenzene 有权
标题翻译：连续硝基苯生产工艺
公开(公告)号：US07763759B2
公开(公告)日：2010-07-27
申请号：US12563300
申请日：2009-09-21
申请人： Thomas Knauf , Alexandre Racoes , Wolfgang Dohmen , Andreas Rausch
发明人： Thomas Knauf , Alexandre Racoes , Wolfgang Dohmen , Andreas Rausch
IPC分类号： C07C205/00
CPC分类号： C07C201/08 , C07C205/06
摘要： The invention relates to a continuous process for the manufacture of nitrobenzene. This process comprises the nitration of benzene with nitrating acid that contains at least 3.0 wt. % of nitric acid and at least 67.0 wt. % of sulfuric acid, in a reaction space in which the start temperature of the reaction is above 100.0° C. but below 102.0° C. In addition, this process requires that the benzene and the nitrating acid are dispersed in one another several times.
摘要翻译：本发明涉及用于制造硝基苯的连续方法。该方法包括用含有至少3.0重量％的硝酸的硝化硝酸。硝酸的百分比和至少67.0重量％反应开始温度高于100.0℃但低于102.0℃的反应空间中的硫酸的含量。另外，该方法需要将苯和硝酸分散在几次中。

7. 发明申请

US20100076230A1 CONTINUOUS PROCESS FOR THE MANUFACTURE OF NITROBENZENE 有权
标题翻译：硝基苯的制造连续工艺
公开(公告)号：US20100076230A1
公开(公告)日：2010-03-25
申请号：US12563300
申请日：2009-09-21
申请人： Thomas Knauf , Alexandre Racoes , Wolfgang Dohmen , Andreas Rausch
发明人： Thomas Knauf , Alexandre Racoes , Wolfgang Dohmen , Andreas Rausch
IPC分类号： C07C205/06
CPC分类号： C07C201/08 , C07C205/06
摘要： The invention relates to a continuous process for the manufacture of nitrobenzene. This process comprises the nitration of benzene with nitrating acid that contains at least 3.0 wt. % of nitric acid and at least 67.0 wt. % of sulfuric acid, in a reaction space in which the start temperature of the reaction is above 100.0° C. but below 102.0° C. In addition, this process requires that the benzene and the nitrating acid are dispersed in one another several times.
摘要翻译：本发明涉及用于制造硝基苯的连续方法。该方法包括用含有至少3.0重量％的硝酸的硝化硝酸。硝酸的百分比和至少67.0重量％反应开始温度高于100.0℃但低于102.0℃的反应空间中的硫酸的含量。另外，该方法需要将苯和硝酸分散在几次中。

8. 发明授权

US5494983A Method for anionic polymerization of acrylic and methacrylic acid derivatives and acrylonitrile methacrylonitrile using resonance stabilized anions 失效
标题翻译：使用共振稳定阴离子进行丙烯酸和甲基丙烯酸衍生物和丙烯腈甲基丙烯腈的阴离子聚合的方法
公开(公告)号：US5494983A
公开(公告)日：1996-02-27
申请号：US737307
申请日：1991-07-31
申请人： Manfred T. Reetz , Thomas Knauf
发明人： Manfred T. Reetz , Thomas Knauf
IPC分类号： C08F2/06 , C08F4/00 , C08F20/06 , C08F20/10 , C08F20/18
CPC分类号： C08F4/00 , C08F20/06
摘要： A process for anionic polymerization of acrylic and/or methacrylic acid derivatives or their ammonium salts with easily produced initiators. Specifically, the initiators are ammonium salts of resonance-stabilized nitrogen anions. The introduction of such initiators provides a maximum amount of structural variation, while inducing the controlled anionic polymerization of monomers at room temperature. The anionic polymerization is also applicable to acrylonitrile or methacrylonitrile or their derivatives. The polymerization process of the present invention provides polymers with definite molecular weight and limited molecular weight distribution.
摘要翻译：丙烯酸和/或甲基丙烯酸衍生物或其铵盐与容易生产的引发剂进行阴离子聚合的方法。具体地，引发剂是共振稳定的氮阴离子的铵盐。这种引发剂的引入提供最大量的结构变化，同时在室温下诱导单体的受控阴离子聚合。阴离子聚合也适用于丙烯腈或甲基丙烯腈或其衍生物。本发明的聚合方法提供具有确定分子量和有限分子量分布的聚合物。

9. 发明申请

US20130296610A1 CHEMICAL REACTOR HAVING WOVEN WIRE MESH PRODUCT AS A RETAINING DEVICE FOR PARTICLES 有权
标题翻译：具有作为颗粒保留装置的WOVEN MESE产品的化学反应器
公开(公告)号：US20130296610A1
公开(公告)日：2013-11-07
申请号：US13988326
申请日：2011-11-15
申请人： Michael Merkel , Karl-Heinz Wilke , Thomas Knauf
发明人： Michael Merkel , Karl-Heinz Wilke , Thomas Knauf
IPC分类号： B01J8/02
CPC分类号： B01J8/0292 , B01J8/025 , B01J8/44 , B01J2208/00884 , Y10T428/12424
摘要： In a chemical reactor for heterogeneously catalysed reaction of a fluid, comprising a holding device for catalyst particles and/or inert particles (80, 100) through which the fluid flows, the side of the holding device lying upstream when viewed in the direction of flow of the fluid comprises knitted wire mesh fabric (50), and the average clear mesh width of the knitted wire fabric (50) is smaller than the average particle size x50.3 of the particles (80, 100). The invention furthermore relates to a process for reaction of a fluid, wherein the reaction is carried out in a reactor according to the invention in the presence of heterogeneous catalyst particles (80) and the catalyst particles (80) are arranged in the holding device for catalyst particles (80). The invention also provides the use of knitted wire mesh fabric (50) as a holding device for catalyst particles and/or inert particles (80, 100) in chemical reactors.
摘要翻译：在用于流体的异质催化反应的化学反应器中，包括用于催化剂颗粒的保持装置和/或流体流过的惰性颗粒（80,100），当从流动方向观察时，保持装置的侧面位于上游的流体包括针织丝网织物（50），并且针织线织物（50）的平均透明网格宽度小于颗粒（80,100）的平均粒径×50.3。本发明还涉及一种流体反应的方法，其中反应在非均相催化剂颗粒（80）存在的情况下在根据本发明的反应器中进行，催化剂颗粒（80）被布置在用于催化剂颗粒（80）。本发明还提供了在化学反应器中使用针织丝网织物（50）作为催化剂颗粒和/或惰性颗粒（80,100）的保持装置。

10. 发明申请

US20130131384A1 PROCESS FOR RESTORING CATALYST ACTIVITY 审中-公开
标题翻译：恢复催化剂活性的方法
公开(公告)号：US20130131384A1
公开(公告)日：2013-05-23
申请号：US13812873
申请日：2011-07-26
申请人： Michael Merkel , Thomas Knauf , Karl-Heinz Wilke
发明人： Michael Merkel , Thomas Knauf , Karl-Heinz Wilke
IPC分类号： B01J38/48
CPC分类号： B01J38/48 , B01J21/04 , B01J23/6482 , B01J23/96 , B01J35/023 , B01J35/1009 , B01J35/1014 , B01J38/02 , B01J38/10 , B01J38/14 , B01J38/20 , C07C209/36 , Y02P20/584 , C07C211/46 , C07C211/50
摘要： The present invention relates to a process for restoring the activity of spent catalysts for the hydrogenation of aromatic nitro compounds, in which a regeneration comprising at least a first burning off stage, a first washing stage, a second burning off stage and a second washing stage is carried out at periodic intervals.
摘要翻译：本发明涉及一种用于恢复芳族硝基化合物氢化的废催化剂的活性的方法，其中再生包括至少第一次燃烧阶段，第一洗涤阶段，第二次燃烧阶段和第二次洗涤阶段以周期性的间隔进行。

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