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1. 发明授权

US5663395A Process for the selective synthesis of silylalkyldisulphides 失效
标题翻译：选择性合成甲硅烷基烷基二硫化物的方法
公开(公告)号：US5663395A
公开(公告)日：1997-09-02
申请号：US743842
申请日：1996-11-05
申请人： Thomas Gobel , Jorg Munzenberg
发明人： Thomas Gobel , Jorg Munzenberg
IPC分类号： C07F7/08 , C07F7/18
CPC分类号： C07F7/1892
摘要： A process is disclosed for the selective synthesis of silylalkyldisulphides by desulphurization of the corresponding polysulphides using nucleophilic reagents.
摘要翻译：公开了通过使用亲核试剂使相应的多硫化物脱硫来选择性合成甲硅烷基烷基二硫化物的方法。

2. 发明授权

US5936112A Mixtures consisting of bis (silylorganyl) polysulfans and silyorganylthiocyanates, their production, and use 失效
标题翻译：由双（甲硅烷基有机基）多硫化物和硫氰酸西硫酯组成的混合物，其生产和使用
公开(公告)号：US5936112A
公开(公告)日：1999-08-10
申请号：US113151
申请日：1998-07-10
申请人： Thomas Gobel , Ulrich Deschler , Jorg Munzenberg , Gerd Zezulka
发明人： Thomas Gobel , Ulrich Deschler , Jorg Munzenberg , Gerd Zezulka
IPC分类号： C07F7/18 , C08L101/00 , C07F7/08 , C07F7/10 , C08K9/06
CPC分类号： C07F7/1836 , Y10T152/10
摘要： Mixtures are disclosed of bis(silylorganyl)polysulfanes and silylorganylthiocyanates, which are produced by reacting polysulfanes with cyanides. The inorganic thiocyanate formed is subsequently allowed to react with a haloalkylalkoxysilane to form the silylorganylthiocyanate. These substances are used in plastic and rubber mixtures reinforced with silica and optionally carbon black.
摘要翻译：公开了通过使多硫烷与氰化物反应制备的双（甲硅烷基有机基）聚硅烷和甲硅烷基有机硫氰酸酯的混合物。随后使形成的无机硫氰酸盐与卤代烷基烷氧基硅烷反应形成甲硅烷基的有机基硫氰酸酯。这些物质用于用二氧化硅和任选的炭黑增强的塑料和橡胶混合物中。

3. 发明授权

US07795442B2 Preparation of thiazoles 失效
标题翻译：噻唑的制备
公开(公告)号：US07795442B2
公开(公告)日：2010-09-14
申请号：US12424594
申请日：2009-04-16
申请人： Thomas Pitterna , Henry Szczepanski , Peter Mainenfisch , Ottmar Franz Huter , Thomas Rapold , Marcel Senn , Thomas Gobel , Anthony Cornelius O'Sullivan
发明人： Thomas Pitterna , Henry Szczepanski , Peter Mainenfisch , Ottmar Franz Huter , Thomas Rapold , Marcel Senn , Thomas Gobel , Anthony Cornelius O'Sullivan
IPC分类号： C07D277/32
CPC分类号： C07D277/32 , C07D277/16 , C07D277/36 , C07D277/70 , C07D277/74
摘要： A process is provided for preparing compounds having the general formula I wherein R is a range of organic groups and X is a leaving group. The process comprises reacting a compound of formula II with a water-removing reagent. When X is halogen or a sulfonate, the compound of formula I may be prepared by reacting a compound of the formula III with a halogenating agent or a sulfonylating agent. Alternatively, when X is halogen, the compound of formula I can be prepared by reacting a compound of the formula IV where R2 and R2 are defined organic groups, with a compound of the formula halogen-C(—O)—O—C1-C8alkyl, halogen-C(—O)—O-aryl or halogen-C(—O)—O-benzyl.
摘要翻译：提供了一种制备具有通式I的化合物的方法，其中R是有机基团的范围，X是离去基团。该方法包括使式II化合物与除水试剂反应。当X是卤素或磺酸盐时，式I化合物可以通过使式III化合物与卤化剂或磺酰化剂反应来制备。或者，当X是卤素时，式I化合物可以通过其中R2和R2定义为有机基团的式IV化合物与式卤化-C（ - ） - O-C1- C8烷基，卤素-C（ - ） - O-芳基或卤素-C（ - ） - O-苄基。

4. 发明授权

US5429873A Surface-modified silicon dioxides 失效
标题翻译：表面改性二氧化硅
公开(公告)号：US5429873A
公开(公告)日：1995-07-04
申请号：US957362
申请日：1992-10-07
申请人： Hans Deusser , Thomas Gobel , Jurgen Meyer , Michael Gunther , Andreas Stubbe
发明人： Hans Deusser , Thomas Gobel , Jurgen Meyer , Michael Gunther , Andreas Stubbe
IPC分类号： C01B33/12 , C01B33/18 , C07F7/18 , C09C1/28 , C09C1/30 , G03G9/08 , G03G9/097 , B32B5/16
CPC分类号： B82Y30/00 , C07F7/182 , C07F7/1836 , C09C1/3081 , G03G9/09716 , C01P2004/64 , C01P2004/80 , C01P2006/10 , C01P2006/12 , C01P2006/60 , C01P2006/80 , C01P2006/90 , Y10T428/2995
摘要： Surface-modified, pyrogenically produced silicon dioxide is obtained by placing a pyrogenically produced silicon dioxide in a know mixing device, spraying it with a chemical compound from the group:CHF.sub.2 --CF.sub.2 --O--(CH.sub.2).sub.3 --Si(OCH.sub.3).sub.3CF.sub.3 --CHF--CF.sub.2 --O--(CH.sub.2).sub.3 --Si(OCH.sub.3).sub.3C.sub.4 F.sub.9 --CH.sub.2 --CH.sub.2 --Si(OCH.sub.3).sub.3C.sub.6 F.sub.13 --CH.sub.2 --CH.sub.2 --Si(OCH.sub.3).sub.3with intensive mixing, subsequently mixing it and tempering the mixture obtained for a fairly long time.
摘要翻译：通过将热解产生的二氧化硅置于已知的混合装置中，将其喷雾成化学化合物，得自CHF2-CF2-O-（CH2）3-Si（OCH3）3 CF3，得到表面改性的热解法生产的二氧化硅 -CH 2 -CH 2 -O（CH 2）3 -Si（OCH 3）3 C 4 F 9 -CH 2 -CH 2 -Si（OCH 3）3 C 6 F 13 -CH 2 -CH 2 -Si（OCH 3）3，随后混合并回火混合物获得了相当长的时间。

5. 发明申请

US20070055063A1 PREPARATION OF THIAZOLES 失效
标题翻译：制备THIAZOLES
公开(公告)号：US20070055063A1
公开(公告)日：2007-03-08
申请号：US11552255
申请日：2006-10-24
申请人： Thomas Pitterna , Henry Szczepanski , Peter Maienfisch , Ottmar Huter , Thomas Rapold , Marcel Senn , Thomas Gobel , Anthony O'Sullivan
发明人： Thomas Pitterna , Henry Szczepanski , Peter Maienfisch , Ottmar Huter , Thomas Rapold , Marcel Senn , Thomas Gobel , Anthony O'Sullivan
IPC分类号： C07D417/02
CPC分类号： C07D277/32 , C07D277/16 , C07D277/36 , C07D277/70 , C07D277/74
摘要： A process for the preparation of a compound of the formula and, where applicable, its E/Z-isomers, mixtures of E/Z-isomers and/or tautomers and acid addition products thereof, in each case in free form or in salt form, wherein: R is unsubstituted or substituted C1-C12alkyl, unsubstituted or substituted C2-C4alkenyl, unsubstituted or substituted C2-C4alkynyl, unsubstituted or substituted C3-C6cycloalkyl, unsubstituted or substituted aryl, unsubstituted or substituted heteroaryl, or —SR1; R1 is unsubstituted or substituted C1-C12alkyl, unsubstituted or substituted C2-C4alkenyl, unsubstituted or substituted C2-C4alkynyl, unsubstituted or substituted cycloalkyl, unsubstituted or substituted aryl or unsubstituted or substituted heteroaryl; and X is a leaving group; The process comprises reacting a compound of the formula: with a halogenating agent or a sulfonylating agent. Alternatively, when X is a selected halogen, the process can comprise reacting a compound of the formula with a compound having a formula selected from the group consisting of halogen-C(═O)—O—C1-C8alkyl; halogen-C(═O)—O-aryl; and halogen-C(═O)—O-benzyl.
摘要翻译：制备下式化合物及其E / Z-异构体的方法，E / Z-异构体和/或互变异构体的混合物及其酸加成产物，各自为游离形式或盐形式，其中：R是未取代或取代的C 1 -C 12烷基，未取代或取代的C 2 -C 4 烯基，未取代或取代的C 2 -C 4炔基，未取代或取代的C 3 -C 6环烷基，未取代或取代的芳基，未取代或取代的杂芳基或-SR 1 N; R 1是未取代或取代的C 1 -C 12烷基，未取代或取代的C 2 -C 3 未取代或取代的C 2 -C 4炔基，未取代或取代的环烷基，未取代或取代的芳基或未取代或取代的杂芳基; X为离去群; 该方法包括使下式化合物与卤化剂或磺酰化剂反应。或者，当X是选择的卤素时，该方法可以包括使下式的化合物与具有选自以下的式的化合物反应：卤素-C（ - ） - O-C 1 -C 烷基; 卤素-C（ - ） - O-芳基; 和卤素-C（ - ） - O-苄基。

6. 发明授权

US07323564B2 Preparation of thiazoles 失效
标题翻译：噻唑的制备
公开(公告)号：US07323564B2
公开(公告)日：2008-01-29
申请号：US11552255
申请日：2006-10-24
申请人： Thomas Pitterna , Henry Szczepanski , Peter Maienfisch , Ottmar Franz Huter , Thomas Rapold , Marcel Senn , Thomas Gobel , Anthony O'Sullivan
发明人： Thomas Pitterna , Henry Szczepanski , Peter Maienfisch , Ottmar Franz Huter , Thomas Rapold , Marcel Senn , Thomas Gobel , Anthony O'Sullivan
IPC分类号： C07D413/14 , C07D277/74 , C07D277/36
CPC分类号： C07D277/32 , C07D277/16 , C07D277/36 , C07D277/70 , C07D277/74
摘要： The present invention is directed to a process for preparing a compound having the formula: wherein R is a range of organic groups and X is a leaving group. The process may include reacting a compound of the formula with a water-removing reagent. Also, when X is a halogen, the process may include reacting a compound of the formula with a halogenating agent or a sulfonylating agent. Alternatively, when X is a halogen, the process may be carried out by reacting a compound of the formula IV where R2 and R3 are defined organic groups with a compound of the formula halogen-C(—O)—O—C1 -C8alkyl, halogen-C(—O)—O-aryl or halogen-C(—O)—O-benzyl.
摘要翻译：本发明涉及制备具有下式的化合物的方法：其中R是有机基团的范围，X是离去基团。该方法可以包括使式的化合物与除水试剂反应。此外，当X是卤素时，该方法可以包括使式的化合物与卤化剂或磺酰化剂反应。或者，当X是卤素时，该方法可以通过使式IV化合物（其中R 2和R 3定义为有机基团）与化合物式中卤素-C（-O）-O-C 1 -C 8烷基，卤素-C（-O）-O-芳基或卤素-C（ - ） - O-苄基。

7. 发明申请

US20090198054A1 PREPARATION OF THIAZOLES 失效
标题翻译：制备THIAZOLES
公开(公告)号：US20090198054A1
公开(公告)日：2009-08-06
申请号：US12424594
申请日：2009-04-16
申请人： Thomas Pitterna , Henry Szczepanski , Peter Maienfisch , Ottmar Franz Huter , Thomas Rapold , Marcel Senn , Thomas Gobel , Anthony Cornelius O'Sullivan
发明人： Thomas Pitterna , Henry Szczepanski , Peter Maienfisch , Ottmar Franz Huter , Thomas Rapold , Marcel Senn , Thomas Gobel , Anthony Cornelius O'Sullivan
IPC分类号： C07D413/02 , C07D277/20 , C07D277/70
CPC分类号： C07D277/32 , C07D277/16 , C07D277/36 , C07D277/70 , C07D277/74
摘要： The present disclosure is directed to a process for the preparation of a compound having the formula: wherein R is unsubstituted or substituted C1-C12alkyl, unsubstituted or substituted C2-C4alkenyl, unsubstituted or substituted C2-C4alkynyl, unsubstituted or substituted C3-C6cycloalkyl, unsubstituted or substituted aryl, unsubstituted or substituted heteroaryl, or —SR1; R1 is unsubstituted or substituted C1-C12alkyl, unsubstituted or substituted C2-C4alkenyl, unsubstituted or substituted C2-C4alkynyl, unsubstituted or substituted cycloalkyl, unsubstituted or substituted aryl or unsubstituted or substituted heteroaryl; and X is a selected leaving group that is not halogen, and may specifically be methylsulfonate, trifluoromethylsulfonate, and p-toluenesulfonate. These compounds are valuable intermediates useful in the synthesis of compounds having pesticidal activity. Generally, the process includes reacting a water-removing reagent, with a compound having the formula Water-removing agents that may be used include thionyl chloride (SOCl2), thionyl bromide (SOBr2), phosphorus oxychloride (POCl3), phosphorus oxybromide (POBr3), phosphorus pentachloride or a sulfonic acid chloride or bromide.
摘要翻译：本公开涉及制备具有下式的化合物的方法：其中R是未取代的或取代的C 1 -C 12烷基，未取代或取代的C 2 -C 4烯基，未取代或取代的C 2 -C 4炔基，未取代或取代的C 3 -C 6环烷基，未取代的或取代的芳基，未取代或取代的杂芳基或-SR1; C 1 -C 12烷基，未取代或取代的C 2 -C 4烯基，未取代或取代的C 2 -C 4炔基，未取代或取代的环烷基，未取代或取代的芳基或未取代或取代的杂芳基; X是不是卤素的选择的离去基团，可以具体为甲基磺酸酯，三氟甲基磺酸酯和对甲苯磺酸酯。这些化合物是有用的合成具有杀虫活性的化合物的中间体。通常，该方法包括使除水试剂与具有式的化合物反应可以使用的除水剂包括亚硫酰氯（SOCl 2），亚硫酰溴（SOBr 2），三氯氧化磷（POCl 3），三溴氧化磷（POBr 3），五氯化磷或磺酰氯或溴化物。

8. 发明授权

US07538229B2 Preparation of thiazoles 失效
标题翻译：噻唑的制备
公开(公告)号：US07538229B2
公开(公告)日：2009-05-26
申请号：US11947891
申请日：2007-11-30
申请人： Thomas Pitterna , Henry Szczepanski , Peter Maienfisch , Ottmar Franz Huter , Thomas Rapold , Marcel Senn , Thomas Gobel , Anthony Cornelius O'Sullivan
发明人： Thomas Pitterna , Henry Szczepanski , Peter Maienfisch , Ottmar Franz Huter , Thomas Rapold , Marcel Senn , Thomas Gobel , Anthony Cornelius O'Sullivan
IPC分类号： C07D277/36
CPC分类号： C07D277/32 , C07D277/16 , C07D277/36 , C07D277/70 , C07D277/74
摘要： A process for the preparation of a compound of formula I wherein R is a range of organic groups and X is a leaving group which process comprises a) reacting a compound of the formula II where R is defined for formula (I) with a water-removing reagent; or b) for the preparation of a compound of formula (I) wherein K is halogen or a sulfonate, reacting a compound of the formula III where R is defined for formula (I) with a halogenating agent or a sulfonylating agent; or c) for the preparation of a compound of formula (I) wherein X is halogen, reacting a compound of the formula IV where R is as defined for formula (I) and R2 and R3 are defined organic groups with a compound of the formula halogen-C(—O)—O—C1-C8alkyl, halogen-C(—O)—O-aryl or halogen-C(—O)—O-benzyl.
摘要翻译：一种制备式I化合物的方法，其中R是有机基团的范围，X是离去基团，该方法包括：a）将式II化合物（其中R定义为式（I））与水 - 去除试剂; 或b）用于制备其中K为卤素或磺酸盐的式（I）化合物，其中R为式（I）所定义的式III化合物与卤化剂或磺酰化剂反应; 或c）用于制备其中X为卤素的式（I）化合物，使式IV化合物（其中R如式（I）所定义）与R 2和R 3定义为有机基团的化合物与式卤素-C（-O）-O-C 1 -C 8烷基，卤素-C（-O）-O-芳基或卤素-C（ - ） - O-苄基。

9. 发明授权

US6139622A Process for the production of integrally waterproofed concrete 有权
标题翻译：整体防水混凝土生产工艺
公开(公告)号：US6139622A
公开(公告)日：2000-10-31
申请号：US182522
申请日：1998-10-30
申请人： Thomas Gobel , Wolfgang Lortz , Reiner Storger , Folker Wittmann , Andreas Gerdes
发明人： Thomas Gobel , Wolfgang Lortz , Reiner Storger , Folker Wittmann , Andreas Gerdes
IPC分类号： C04B24/42 , C04B103/65 , C04B24/40 , C09K3/18
CPC分类号： C04B24/42
摘要： This invention relates to a process for the production of a homogeneously waterproofed concrete (integrally waterproofed concrete) in which an aqueous hydrolysable, emulsion containing organosilicon compounds is added before curing to the fresh concrete mix prepared from water, inorganic and optionally organic constituents, which emulsion contains at least one alkoxysilane and optionally an organosilicon compound acting as a surfactant.
摘要翻译：本发明涉及一种用于生产均匀防水混凝土（整体防水混凝土）的方法，其中将含水可水解的含有机硅化合物的乳液在固化之前加入到由水，无机和任选的有机成分制备的新鲜混凝土混合物中，该乳液含有至少一种烷氧基硅烷和任选的作为表面活性剂的有机硅化合物。

10. 发明授权

US6121455A Process for the preparation of thiazole derivatives 有权
标题翻译：噻唑衍生物的制备方法
公开(公告)号：US6121455A
公开(公告)日：2000-09-19
申请号：US331432
申请日：1999-08-13
申请人： Thomas Pitterna , Henry Szczepanski , Peter Maienfisch , Ottmar Franz Huter , Thomas Rapold , Marcel Senn , Thomas Gobel , Anthony Cornelius O'Sullivan , Gottfried Seifert
发明人： Thomas Pitterna , Henry Szczepanski , Peter Maienfisch , Ottmar Franz Huter , Thomas Rapold , Marcel Senn , Thomas Gobel , Anthony Cornelius O'Sullivan , Gottfried Seifert
IPC分类号： C07D277/16 , C07D277/20 , C07D277/22 , C07D277/28 , C07D277/32 , C07D277/36 , C07D277/74 , C07D417/06 , C07D417/14
CPC分类号： C07D277/32 , C07D277/16 , C07D277/36 , C07D417/06
摘要： The invention relates to a process for the preparation of a compound of the formula ##STR1## and, where applicable, its E/Z-isomers, mixtures of E/Z-isomers and/or tautomers, in each case in free form or in salt form, whereinQ is CH or N,Y is NO.sub.2 or CN,Z is CHR.sub.3, O, NR.sub.3 or S,R.sub.1 and R.sub.2 are either each independently of the other hydrogen or unsubstituted or R.sub.4 -substituted C.sub.1 -C.sub.8 alkyl, or together form an alkylene bridge having two or three carbon atoms, and said alkylene bridge may additionally contain a hetero atom selected from the group consisting of NR.sub.5, O and S,R.sub.3 is H or unsubstituted or R.sub.4 -substituted C.sub.1 -C.sub.12 alkyl,R.sub.4 is unsubstituted or substituted aryl or heteroaryl, andR.sub.5 is H or C.sub.1 -C.sub.12 alkyl; which comprisesa) reacting a compound of the formula ##STR2## and, where applicable, its E/Z-isomers, mixtures of E/Z-isomers and/or tautomers, in each case in free form or in salt form, which is known or can be prepared by processes known.
摘要翻译： PCT No.PCT / EP97 / 07087第 371日期1999年8月13日 102（e）日期1999年8月13日PCT 1997年12月17日PCT公布。第WO98 / 27074号公报日期1998年6月25日本发明涉及一种制备下式化合物和（如适用的话）其E / Z-异构体，E / Z-异构体和/或互变异构体的混合物的方法，在每种情况下为游离形式或盐形式，其中Q是CH或N，Y是NO 2或CN，Z是CHR 3，O，NR 3或S，R 1和R 2各自独立地是另一个氢或未取代的或者R 4取代的C 1 -C 8烷基，或一起形成具有两个或三个碳原子的亚烷基桥，并且所述亚烷基桥可以另外含有选自NR5，O和S的杂原子，R3是H或未取代的或R4取代的C1-C12烷基，R4是未取代的或取代的芳基或杂芳基，R5是H或C1-C12烷基; 其包括：a）使游离形式或盐形式的下式化合物和/或其可能的E / Z-异构体，E / Z-异构体和/或互变异构体的混合物在各种情况下反应，其为已知或可以由已知的方法准备。

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