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1. 发明授权

US08361628B2 Process for producing metal film 有权
标题翻译：金属膜生产工艺
公开(公告)号：US08361628B2
公开(公告)日：2013-01-29
申请号：US12675579
申请日：2008-11-14
申请人： Seiji Nakajima , Tetsuo Hayase , Tetsuya Mori
发明人： Seiji Nakajima , Tetsuo Hayase , Tetsuya Mori
IPC分类号： B32B15/08 , B32B15/04 , B05D3/10 , C08G63/00
CPC分类号： H05K3/387 , C23C18/06 , C23C18/08 , C23C18/14 , C23C18/1667 , C23C18/1678 , C23C18/1893 , C23C18/2086 , C23C18/31 , G02B5/0808 , G02B27/1073 , G02B27/144 , H05K3/181 , H05K2203/1157 , H05K2203/121 , Y10T428/31678 , Y10T428/31681 , Y10T428/31692
摘要： The present invention provides (i) a process for producing a metal film with which process a metal film and a metal pattern can be formed, at low cost, on an arbitrary substrate, (ii) a primer composition, (iii) a metal film, and (iv) use of the metal film. The process includes the steps of: forming an organic film with use of a primer composition which contains (i) an addition polymerizable compound including three or more reactive groups, (ii) an addition polymerizable compound including an acid group, (iii) an addition polymerizable compound including a basic group, and (iv) an addition polymerizable compound including a hydrophilic functional group; form a metal (M1) salt from the acid group; substituting the metal (M1) salt of the acid group with a metal (M2) salt by processing with a metal (M2) ion aqueous solution containing a metal (M2) ion which has a less ionization tendency than the metal (M1) ion; and reducing the metal (M2) ion so that a metal film is formed on a surface of the organic film.
摘要翻译：本发明提供（i）金属膜的制造方法，可以在任意的基材上以低成本形成金属膜和金属图案，（ii）底漆组合物，（iii）金属膜，和（iv）使用金属膜。该方法包括以下步骤：使用底漆组合物形成有机膜，该底漆组合物包含（i）包含三个或更多个反应性基团的加成聚合性化合物，（ii）包含酸基的加聚性化合物，（iii）包含碱性基团的可聚合化合物，和（iv）包含亲水官能团的加成聚合性化合物; 从酸基形成金属（M1）盐; 用含金属（M2）离子的金属（M2）离子水溶液加工，用金属（M2）盐代替金属（M1）盐，电离倾向比金属（M1）离子少; 并且还原金属（M2）离子，使得在有机膜的表面上形成金属膜。

2. 发明申请

US20100230643A1 PROCESS FOR PRODUCING METAL FILM, METAL FILM AND USE OF THE METAL FILM 有权
标题翻译：生产金属膜，金属膜和金属膜的使用方法
公开(公告)号：US20100230643A1
公开(公告)日：2010-09-16
申请号：US12675438
申请日：2008-11-14
申请人： Seiji Nakajima , Tetsuo Hayase , Tetsuya Mori
发明人： Seiji Nakajima , Tetsuo Hayase , Tetsuya Mori
IPC分类号： H01B1/02 , B05D5/12
CPC分类号： C23C18/14 , C23C18/06 , C23C18/08 , C23C18/1667 , C23C18/1678 , C23C18/1696 , C23C18/1893 , C23C18/2086 , Y10T428/31678 , Y10T428/31681 , Y10T428/31692
摘要： The process of the present invention for producing a metal film includes: forming an organic film using a primer composition containing an addition polymerizable compound including three or more reactive groups, an acid group-including addition polymerizable compound, and a hydrophilic functional group-including addition polymerizable compound; forming a metal (M1) salt from the acid group; substituting the metal (M1) salt of the acid group with a metal (M2) salt by processing the organic film with a metal (M2) ion aqueous solution containing a metal (M2) ion having less ionization tendency than the metal (M1) ion; reducing the metal (M2) ion so that a metal film is formed on a surface of the organic film; and oxidizing the metal film. This provides (i) a process for producing a metal film and a metal pattern, at low cost, on an arbitrary substrate, (ii) a metal film, and (iii) use of the meta film.
摘要翻译：本发明的金属膜的制造方法包括：使用含有含有3个以上反应性基团的加聚性化合物的底漆组合物，含有酸基的加成聚合性化合物和含有亲水性官能团的添加剂形成有机膜可聚合化合物; 从酸基形成金属（M1）盐; 通过用含有比金属（M1）离子离子化倾向小的金属（M2）离子的金属（M2）离子水溶液处理有机膜，用金属（M2）盐代替酸基金属（M1）盐 ; 减少金属（M2）离子，使得在有机膜的表面上形成金属膜; 并氧化金属膜。这提供（i）在任意基板上以低成本制造金属膜和金属图案的方法，（ii）金属膜，以及（iii）使用间位膜。

3. 发明申请

US20130341534A1 SENSOR PROVIDED WITH METAL OXIDE FILM AND USE THEREOF 有权
标题翻译：传感器提供金属氧化物膜及其使用
公开(公告)号：US20130341534A1
公开(公告)日：2013-12-26
申请号：US14002640
申请日：2011-03-18
申请人： Keisuke Ohmae , Tetsuya Mori , Tetsuo Hayase , Seiji Nakajima , Mariko Nishiguchi
发明人： Keisuke Ohmae , Tetsuya Mori , Tetsuo Hayase , Seiji Nakajima , Mariko Nishiguchi
IPC分类号： H01L31/0248
CPC分类号： H01L31/0248 , G01L9/02 , G01L11/02 , G01N27/126 , G01N33/005
摘要： A sensor capable of detecting light, hydrogen gas, and air pressure includes a metal oxide film produced by a process including the steps of: (a) forming an organic film by using a primer composition containing (i) an addition polymerizable compound including three or more reactive groups, (ii) an addition polymerizable compound including an acid group, and (iii) an addition polymerizable compound including a hydrophilic functional group; (b) forming a metal (M1) salt from the acid group; (c) substituting the metal (M1) salt of the acid group with a metal (M2) salt by treating the organic film with a metal (M2) ion aqueous solution; (d) reducing the metal (M2) ion so that a metal film is formed on a surface of the organic film; and (e) oxidizing the metal film.
摘要翻译：能够检测光，氢气和空气压力的传感器包括通过包括以下步骤的方法制造的金属氧化物膜：（a）通过使用底漆组合物形成有机膜，所述底漆组合物包含（i）包含三个或更多的反应性基团，（ii）包含酸基的加成聚合性化合物，和（iii）包含亲水性官能团的加成聚合性化合物; （b）从酸基形成金属（M1）盐; （c）用金属（M2）盐代替金属（M1）盐，用金属（M2）离子水溶液处理有机膜; （d）还原金属（M2）离子，使得在有机膜的表面上形成金属膜; 和（e）氧化金属膜。

4. 发明授权

US08361629B2 Half mirror and process for producing same 失效
标题翻译：半反射镜和生产过程
公开(公告)号：US08361629B2
公开(公告)日：2013-01-29
申请号：US13059718
申请日：2009-09-10
申请人： Seiji Nakajima , Tetsuya Mori , Tetsuo Hayase , Keisuke Oomae
发明人： Seiji Nakajima , Tetsuya Mori , Tetsuo Hayase , Keisuke Oomae
IPC分类号： B32B15/08 , B32B15/04 , B05D3/10 , C08G63/00
CPC分类号： B32B15/08 , C23C18/1658 , C23C18/1893 , C23C18/2086 , C23C18/31 , G02B5/08 , Y10T428/31678 , Y10T428/31681 , Y10T428/31692
摘要： A half mirror has a shape on a substrate and excels in appearance and design and is fabricated by a method. The method includes forming an organic film by applying, onto a transparent substrate or film, a primer composition containing an addition-polymerizable compound having three or more reactive groups, an addition-polymerizable compound having an acidic group, and an addition-polymerizable compound having a hydrophilic functional group, and polymerizing the primer composition. The method includes turning the acidic group into a metal (M1) salt by treating the organic film with an aqueous solution containing metal (M1) ions, and turning the metal (M1) salt into a metal (M2) salt by treating the organic film with a metal (M2) ion aqueous solution containing metal (M2) ions that are lower in ionization tendency than metal (M1) ions, and (d) reducing metal (M2) ions to form a metal film on a surface of the organic film.
摘要翻译：半反射镜在基板上具有形状，外观和设计优异，并且通过一种方法制造。该方法包括通过在透明基板或膜上涂布含有具有三个或更多个反应性基团的可加成聚合化合物的底漆组合物，具有酸性基团的可加成聚合的化合物和可加成聚合的化合物，形成有机薄膜，亲水性官能团，并使底漆组合物聚合。该方法包括通过用含有金属（M1）离子的水溶液处理有机膜，将金属（M1）盐转化为金属（M1）盐，通过处理有机膜与金属（M2）离子的金属（M2）离子水溶液的离子化倾向比金属（M1）离子低，和（d）还原金属（M2）离子以在有机膜的表面上形成金属膜。

5. 发明授权

US08273461B2 Method of producing metal film 有权
标题翻译：金属膜生产方法
公开(公告)号：US08273461B2
公开(公告)日：2012-09-25
申请号：US12304220
申请日：2007-06-13
申请人： Tetsuya Mori , Seiji Nakajima
发明人： Tetsuya Mori , Seiji Nakajima
IPC分类号： B32B15/08 , B32B15/04 , B05D3/10 , C08G63/00
CPC分类号： H05K3/387 , C23C18/14 , C23C18/1605 , C23C18/1608 , C23C18/1658 , C23C18/1667 , C23C18/1678 , C23C18/1844 , C23C18/2086 , C23C18/31 , C23C18/44 , H05K3/181 , H05K2203/1157 , H05K2203/121 , Y10T428/31678 , Y10T428/31681 , Y10T428/31692
摘要： The method of producing a metal film in accordance with the present invention includes: the organic film forming step of applying, onto a substrate or a film, an underlayer composition containing an addition polymerizable compound having three or more reactive groups, an addition polymerizable compound having acid groups, and an addition polymerizable compound having hydrophilic functional groups and polymerizing the composition, to form an organic film; the metal salt producing step of processing the organic film with an aqueous solution containing metal (M1) ions, to convert the acid groups to a metal (M1) salt; the metal fixing step of processing the organic film processed with the aqueous solution containing metal (M1) ions with an aqueous metal (M2) ion solution containing metal (M2) ions having lower ionicity than the metal (M1) ions, to convert the metal (M1) salt of the acid groups to a metal (M2) salt; and the reduction step of reducing the metal (M2) ions, to form a metal film on a surface of the organic film. The method therefore efficiently produces a film of metal, especially gold.
摘要翻译：根据本发明的金属膜的制造方法包括：有机膜形成工序，在基材或膜上涂布含有具有三个以上反应性基团的加成聚合性化合物的下层组合物，具有酸基和具有亲水性官能团的聚合性化合物，并使组合物聚合，形成有机膜; 用含有金属（M1）离子的水溶液处理有机膜的金属盐生产步骤，将酸基转化为金属（M1）盐; 金属固定步骤，用含有金属（M1）离子的水溶液处理有机薄膜的金属（M2）离子溶液与金属（M1）离子离子性低的金属（M2）离子处理，以将金属（M1）的盐与金属（M2）盐; 还原金属（M2）离子的还原步骤，以在有机膜的表面上形成金属膜。因此，该方法有效地产生金属膜，特别是金。

6. 发明申请

US20110141568A1 HALF MIRROR AND PROCESS FOR PRODUCING SAME 失效
标题翻译：半透镜及其制造方法
公开(公告)号：US20110141568A1
公开(公告)日：2011-06-16
申请号：US13059718
申请日：2009-09-10
申请人： Seiji Nakajima , Tetsuya Mori , Tetsuo Hayase , Keisuke Oomae
发明人： Seiji Nakajima , Tetsuya Mori , Tetsuo Hayase , Keisuke Oomae
IPC分类号： G02B1/10 , B05D3/10 , B05D5/00 , B05D5/06
CPC分类号： B32B15/08 , C23C18/1658 , C23C18/1893 , C23C18/2086 , C23C18/31 , G02B5/08 , Y10T428/31678 , Y10T428/31681 , Y10T428/31692
摘要： A half mirror has a shape on a substrate and excels in appearance and design and is fabricated by a method. The method includes forming an organic film by applying, onto a transparent substrate or film, a primer composition containing an addition-polymerizable compound having three or more reactive groups, an addition-polymerizable compound having an acidic group, and an addition-polymerizable compound having a hydrophilic functional group, and polymerizing the primer composition. The method includes turning the acidic group into a metal (M1) salt by treating the organic film with an aqueous solution containing metal (M1) ions, and turning the metal (M1) salt into a metal (M2) salt by treating the organic film with a metal (M2) ion aqueous solution containing metal (M2) ions that are lower in ionization tendency than metal (M1) ions, and (d) reducing metal (M2) ions to form a metal film on a surface of the organic film.
摘要翻译：半反射镜在基板上具有形状，外观和设计优异，并且通过一种方法制造。该方法包括通过在透明基板或膜上涂布含有具有三个或更多个反应性基团的可加成聚合化合物的底漆组合物，具有酸性基团的可加成聚合的化合物和可加成聚合的化合物，形成有机薄膜，亲水性官能团，并使底漆组合物聚合。该方法包括通过用含有金属（M1）离子的水溶液处理有机膜，将金属（M1）盐转化为金属（M1）盐，通过处理有机膜与金属（M2）离子的金属（M2）离子水溶液的离子化倾向比金属（M1）离子低，和（d）还原金属（M2）离子以在有机膜的表面上形成金属膜。

7. 发明申请

US20100215979A1 Method of forming metal film and metal wiring pattern, undercoat composition for forming metal film and metal wiring pattern, and metal film 失效
标题翻译：形成金属膜和金属布线图案的方法，用于形成金属膜和金属布线图案的底涂层组合物和金属膜
公开(公告)号：US20100215979A1
公开(公告)日：2010-08-26
申请号：US11917133
申请日：2006-06-06
申请人： Seiji Nakajima , Tetsuya Mori , Hidemi Nawafune
发明人： Seiji Nakajima , Tetsuya Mori , Hidemi Nawafune
IPC分类号： B32B3/00 , B05D5/12 , B05D3/10 , H05H1/24 , B05D3/06 , B32B15/01 , C08K3/08
CPC分类号： C23C18/1658 , C23C18/161 , C23C18/2086 , C23C18/31 , C23C18/44 , C23C18/54 , Y10T428/12396
摘要： A method of forming a metal film and a metal wiring pattern is described a step of forming an organic film by applying and polymerizing an undercoat composition for forming a metal film containing an addition-polymerizable monomer having an acidic group and a polymerization initiator on a substrate or film, a step of converting the acidic group into a metal (M1) salt by treating the organic film with an aqueous solution containing a metal (M1) ion, a step of converting the metal (M1) salt into a metal (M2) salt by treating the organic film with an aqueous solution containing a metal (M2) ion having an ionization tendency lower than the metal (M1) ion, and a step of forming a metal film on the organic film surface by reducing the metal (M2) ion.
摘要翻译：描述了一种形成金属膜和金属布线图案的方法，该方法是通过将含有具有酸性基团和聚合引发剂的可加成聚合单体的金属膜形成的底涂层组合物在基材上进行聚合而形成有机膜或膜，通过用含有金属（M1）离子的水溶液处理有机膜来将酸性基团转化为金属（M1）盐的步骤，将金属（M1）盐转化成金属（M2）的步骤，通过用含有电离倾向低于金属（M1）离子的金属（M2）离子的水溶液处理有机膜，以及通过还原金属（M2）在有机膜表面上形成金属膜的步骤，离子。

8. 发明授权

US09711666B2 Sensor provided with metal oxide film and use thereof 有权
公开(公告)号：US09711666B2
公开(公告)日：2017-07-18
申请号：US14002640
申请日：2011-03-18
申请人： Keisuke Ohmae , Tetsuya Mori , Tetsuo Hayase , Seiji Nakajima , Mariko Nishiguchi
发明人： Keisuke Ohmae , Tetsuya Mori , Tetsuo Hayase , Seiji Nakajima , Mariko Nishiguchi
IPC分类号： B32B15/08 , B32B15/04 , G01N27/04 , H01L31/0248 , G01L9/02 , G01L11/02 , G01N27/12 , G01N33/00
CPC分类号： H01L31/0248 , G01L9/02 , G01L11/02 , G01N27/126 , G01N33/005
摘要： A sensor capable of detecting light, hydrogen gas, and air pressure includes a metal oxide film produced by a process including the steps of: (a) forming an organic film by using a primer composition containing (i) an addition polymerizable compound including three or more reactive groups, (ii) an addition polymerizable compound including an acid group, and (iii) an addition polymerizable compound including a hydrophilic functional group; (b) forming a metal (M1) salt from the acid group; (c) substituting the metal (M1) salt of the acid group with a metal (M2) salt by treating the organic film with a metal (M2) ion aqueous solution; (d) reducing the metal (M2) ion so that a metal film is formed on a surface of the organic film; and (e) oxidizing the metal film.

9. 发明授权

US08071178B2 Method of forming metal film and metal wiring pattern, undercoat composition for forming metal film and metal wiring pattern, and metal film 失效
标题翻译：形成金属膜和金属布线图案的方法，用于形成金属膜和金属布线图案的底涂层组合物和金属膜
公开(公告)号：US08071178B2
公开(公告)日：2011-12-06
申请号：US11917133
申请日：2006-06-06
申请人： Seiji Nakajima , Tetsuya Mori , Hidemi Nawafune
发明人： Seiji Nakajima , Tetsuya Mori , Hidemi Nawafune
IPC分类号： C08F2/48 , C08F2/50
CPC分类号： C23C18/1658 , C23C18/161 , C23C18/2086 , C23C18/31 , C23C18/44 , C23C18/54 , Y10T428/12396
摘要： A method of forming a metal film and a metal wiring pattern is described a step of forming an organic film by applying and polymerizing an undercoat composition for forming a metal film containing an addition-polymerizable monomer having an acidic group and a polymerization initiator on a substrate or film, a step of converting the acidic group into a metal (M1) salt by treating the organic film with an aqueous solution containing a metal (M1) ion, a step of converting the metal (M1) salt into a metal (M2) salt by treating the organic film with an aqueous solution containing a metal (M2) ion having an ionization tendency lower than the metal (M1) ion, and a step of forming a metal film on the organic film surface by reducing the metal (M2) ion.
摘要翻译：描述了一种形成金属膜和金属布线图案的方法，该方法是通过将含有具有酸性基团和聚合引发剂的可加成聚合单体的金属膜形成的底涂层组合物在基材上进行聚合而形成有机膜或膜，通过用含有金属（M1）离子的水溶液处理有机膜来将酸性基团转化为金属（M1）盐的步骤，将金属（M1）盐转化成金属（M2）的步骤，通过用含有电离倾向低于金属（M1）离子的金属（M2）离子的水溶液处理有机膜，以及通过还原金属（M2）在有机膜表面上形成金属膜的步骤，离子。

10. 发明申请

US20100239874A1 PROCESS FOR PRODUCING METAL FILM, PRIMER COMPOSITION, METAL FILM AND USE OF THE METAL FILM 有权
标题翻译：生产金属膜，原料组合物，金属膜和金属膜的使用方法
公开(公告)号：US20100239874A1
公开(公告)日：2010-09-23
申请号：US12675579
申请日：2008-11-14
申请人： Seiji Nakajima , Tetsuo Hayase , Tetsuya Mori
发明人： Seiji Nakajima , Tetsuo Hayase , Tetsuya Mori
IPC分类号： B32B15/08 , G02B5/08 , B05D3/10 , B05D3/06 , B05D5/00 , C08F20/18
CPC分类号： H05K3/387 , C23C18/06 , C23C18/08 , C23C18/14 , C23C18/1667 , C23C18/1678 , C23C18/1893 , C23C18/2086 , C23C18/31 , G02B5/0808 , G02B27/1073 , G02B27/144 , H05K3/181 , H05K2203/1157 , H05K2203/121 , Y10T428/31678 , Y10T428/31681 , Y10T428/31692
摘要： The present invention provides (i) a process for producing a metal film with which process a metal film and a metal pattern can be formed, at low cost, on an arbitrary substrate, (ii) a primer composition, (iii) a metal film, and (iv) use of the metal film. The process includes the steps of: forming an organic film with use of a primer composition which contains (i) an addition polymerizable compound including three or more reactive groups, (ii) an addition polymerizable compound including an acid group, (iii) an addition polymerizable compound including a basic group, and (iv) an addition polymerizable compound including a hydrophilic functional group; form a metal (M1) salt from the acid group; substituting the metal (M1) salt of the acid group with a metal (M2) salt by processing with a metal (M2) ion aqueous solution containing a metal (M2) ion which has a less ionization tendency than the metal (M1) ion; and reducing the metal (M2) ion so that a metal film is formed on a surface of the organic film.
摘要翻译：本发明提供（i）金属膜的制造方法，可以在任意的基材上以低成本形成金属膜和金属图案，（ii）底漆组合物，（iii）金属膜，和（iv）使用金属膜。该方法包括以下步骤：使用底漆组合物形成有机膜，该底漆组合物包含（i）包含三个或更多个反应性基团的加成聚合性化合物，（ii）包含酸基的加聚性化合物，（iii）包含碱性基团的可聚合化合物，和（iv）包含亲水官能团的加成聚合性化合物; 从酸基形成金属（M1）盐; 用含金属（M2）离子的金属（M2）离子水溶液加工，用金属（M2）盐代替金属（M1）盐，电离倾向比金属（M1）离子少; 并且还原金属（M2）离子，使得在有机膜的表面上形成金属膜。

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