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1. 发明授权

US4880877A Method for producing rubber modified thermoplastic resins 失效
标题翻译：橡胶改性热塑性树脂的制造方法
公开(公告)号：US4880877A
公开(公告)日：1989-11-14
申请号：US946058
申请日：1986-12-24
申请人： Teruhiko Sugimori , Noriyuki Tajiri , Fumio Suzuki , Hideaki Habara , Yutaro Fukuda , Haruki Sato
发明人： Teruhiko Sugimori , Noriyuki Tajiri , Fumio Suzuki , Hideaki Habara , Yutaro Fukuda , Haruki Sato
IPC分类号： C08J3/00 , C08L51/04
CPC分类号： C08J3/005 , C08L51/04
摘要： Disclosed is a method for producing a rubber modified thermoplastic resin which comprises carrying out all or a part of the following steps (I)-(VI):(I) a setp of mixing the following (A), (B), (C) and thermoplastic resin (2):(A) a latex of gfart rubber polymer (1),(B) an organic agent which is capable of dissolving thermoplastic resin (2) and has a solubility in water of 5% by weight or less t a temperature at which (A), (B), (C) and thermoplastic resin (2) are mixed, amount of the organic agent being 10-600% by weight of polymer (4) which is the sum of graft rubber polymer (1) and thermoplastic resin (2) and(C) a warer soluble agent capable of coagulating latex (A), amount of this agent being 10% by weight or less of graft rubber polymer (1),(II) a step of separating and removing aqueous phase from a two-phase mixture obtained in the mixing step (I),(III) a step of mixing the mixture from which the aqueous phase hsa been removed at step (II) and the whole or a part of thermoplastic resin (3),(IV) a step of removing a part or the whole of ogranic agent (B) and remaining water from the mixture obtained at step (III) by a thermal means,(V) a step of mixing the remainder of thermoplastic resin (3) in case a part of thermoplastic resin (3) has been mixed at step (III), and(VI) a step of removing the remainder of organic agent (B) in case only a part of organic agent (B) has been removed at step (IV).
摘要翻译：公开了一种橡胶改性热塑性树脂的制造方法，其特征在于，进行以下（I）〜（VI）的全部或一部分步骤（I）：（I）将下述（A），（B），（C ）和热塑性树脂（2）：（A）gfart橡胶聚合物（1）的胶乳，（B）能够溶解热塑性树脂（2）并且在水中的溶解度为5重量％以下的有机试剂（A），（B），（C）和热塑性树脂（2）混合时，有机试剂的量为聚合物（4）的10-600重量％，其为接枝橡胶聚合物 1）和热塑性树脂（2）和（C）能够凝固胶乳（A）的较易溶解剂，该试剂的量为接枝橡胶聚合物（1）的10重量％以下，（II）分离步骤以及从混合步骤（I），（III）中获得的两相混合物中除去水相的步骤是将在步骤（II）中除去水相hsa的混合物与热塑性树脂的全部或部分混合的步骤苯乙烯树脂（3），（Ⅳ）通过加热方法从步骤（III）获得的混合物中除去部分或全部异味剂（B）和剩余水的步骤，（Ⅴ）在热塑性树脂（3）的一部分已经在步骤（III）中混合的情况下，热塑性树脂（3）的热塑性树脂（3），和（VI）在仅有一部分有机试剂的情况下去除剩余的有机试剂（B）的步骤 B）已经在步骤（IV）被去除。

2. 发明授权

US4992510A Method for producing rubber modified thermoplastic resins 失效
标题翻译：橡胶改性热塑性树脂的制造方法
公开(公告)号：US4992510A
公开(公告)日：1991-02-12
申请号：US394720
申请日：1989-08-16
申请人： Teruhiko Sugimori , Noriyuki Tajiri , Fumio Suzuki , Hideaki Habara , Yutaro Fukuda , Haruki Sato
发明人： Teruhiko Sugimori , Noriyuki Tajiri , Fumio Suzuki , Hideaki Habara , Yutaro Fukuda , Haruki Sato
IPC分类号： C08J3/00 , C08L51/04
CPC分类号： C08J3/005 , C08L51/04
摘要： Disclosed is method for producing a rubber modified thermoplastic reins which comprises carrying out all or a part of the following setps (I) - (VI):(I) a step of mixing the following (A), (B), (C) and thermoplastic resin (2):(A) a latex of graft rubber polymer (1),(B) an organic agent which is capable of dissolving thermoplastic resin (2) and has a solubility in water of 5% by weight or less at a temperature at which (A), (B), (C) and thermoplastic resin (2) are mixed, amount of the organic agent being 10-600% by weight of polymer (4) which is the sum of graft rubber polymer (1) and thermoplastic resin (2) and(C) a water soluble agent capable of coagulating latex (A), amount of this agent being 10% by weight or less of graft rubber polymer (1),(II) a step of separating and removing aqueous phase from a two-phase mixture obtained in the mixing step (I),(III) a step of mixing the mixture from which the aqueous phase has been removed at step (II) and the whole or a part of thermoplastic resin (3),(IV) a step of removing a part or the whole of organic agent (B) and remaining water from the mixture obtained at step (III) by a thermal means,(V) a step of mixing the remainder of thermoplastic resin (3) in case a part of thermoplastic resin (3) has been mixed at step (III), and(VI) a step of removing the remainder of organic agent (B) in case only a part of organic agent (B) has been removed at step (IV).

3. 发明授权

US4690975A Method for producing rubber modified thermoplastic resins 失效
标题翻译：橡胶改性热塑性树脂的制造方法
公开(公告)号：US4690975A
公开(公告)日：1987-09-01
申请号：US867204
申请日：1986-05-27
申请人： Teruhiko Sugimori , Noriyuki Tajiri , Yutaro Fukuda
发明人： Teruhiko Sugimori , Noriyuki Tajiri , Yutaro Fukuda
IPC分类号： C08J3/00 , C08L101/00 , C08L51/00
CPC分类号： C08J3/005 , C08L101/00
摘要： Disclosed is a method for producing a rubber modified thermoplastic resin excellent in surface appearance and various properties and high in commercial values which comprises removing an aqueous phase from a two-phase mixture comprises a graft rubber polymer latex (1) obtained by graft polymerization of vinyl monomer on a rubber latex, a thermoplastic resin (2) and an organic agent in an amount of 0.2 to 6 times the weight of all the polymers (3) which is capable of dissolving said thermoplastic resin (2) and has a solubility in water of 5 to 50% by weight at 25.degree. C. and then removing said organic agent and remaining water from the remaining organic phase by a thermal means.
摘要翻译：公开了一种表面外观和各种性能和商业价值高的橡胶改性热塑性树脂的制造方法，其包括从两相混合物中除去水相，包括通过乙烯基接枝聚合获得的接枝橡胶聚合物胶乳（1）橡胶胶乳上的单体，热塑性树脂（2）和有机试剂的量为所有能够溶解所述热塑性树脂（2）的所有聚合物（3）的重量的0.2至6倍，并且在水中具有溶解度在25℃下为5至50重量％，然后通过热方法从剩余的有机相中除去所述有机物和剩余的水。

4. 发明授权

US4910850A Method for coagulation of a polymer latex 失效
标题翻译：凝聚聚合物胶乳的方法
公开(公告)号：US4910850A
公开(公告)日：1990-03-27
申请号：US226526
申请日：1988-08-01
申请人： Teruhiko Sugimori , Noriyuki Tajiri , Akio Hironaka , Hideaki Habara
发明人： Teruhiko Sugimori , Noriyuki Tajiri , Akio Hironaka , Hideaki Habara
IPC分类号： B29B9/06 , B29B15/02 , B29B15/04
CPC分类号： B29B9/06 , B29B15/02 , B29B15/04 , Y10T29/53687
摘要： A method for coagulation of a polymer latex by feeding the polymer latex to an extruder having a base plate and a plurality of fine tubes fixed to said base plate and extending therefrom, said fine tubes being mutually spaced by at least 1 mm and protruding from said base plate by at least 3 mm, and discharging said polymer latex through said fine tubes into a coagulation solution to coagulate the latex.

5. 发明授权

US4921909A Method for producing thermoplastic resins 失效
标题翻译：热塑性树脂的制造方法
公开(公告)号：US4921909A
公开(公告)日：1990-05-01
申请号：US946057
申请日：1986-12-24
申请人： Teruhiko Sugimori , Noriyuki Tajiri , Yutaro Fukuda
发明人： Teruhiko Sugimori , Noriyuki Tajiri , Yutaro Fukuda
IPC分类号： C08J3/00 , C08L51/04
CPC分类号： C08J3/005 , C08L51/04
摘要： Emulsion polymerization type thermoplastic resin of high performance can be produced by the following methods: namely, a method which comprises removing an aqueous phase from a two-phase mixture comprising a latex of polymer (1) produced by emulsion polymerization, a water soluble agent (2) in an amount of 10% by weight or less of said polymer (1) which is capable of coagulating the latex of polymer (1) and an organic agent (3) in an amount of 0.1 to 6 times the weight of said polymer (1) which is capable of dissolving both an uncrosslinked polymer contained in said polymer (1) and thermoplastic polymer (4) mentioned hereinbelow and has a solubility in water of 5% by weight or less at 25.degree. C., then melt-mixing molten polymer which has been subjected to a first devolatilization by a thermal means with thermoplastic resin (4) and then subjecting the mixture to a second devolatilization; and a method which comprises removing an aqueous phase from a two-phase mixture comprising a latex of polymer (1) produced by emulsion polymerization, a water soluble agent ( 2) in an amount of 10% by weight or less of said polymer (1) which is capable of coagulating the latex of polymer (1) and an organic agent (3) in an amount of 0.1 to 6 times the weight of said polymer (1) which is capable of dissolving an uncrosslinked polymer contained in said polymer (1) and has a solubility in water of 5% by weight or less at 25.degree. C. and then melt-mixing the molten polymer from which volatile component has been devolatilized by a thermal means with thermoplastic polymer (4').
摘要翻译：可以通过以下方法制备高性能的乳液聚合型热塑性树脂：即包括从包含通过乳液聚合制备的聚合物（1）的胶乳的两相混合物中除去水相的方法，水溶性试剂（ 2）的量为所述聚合物（1）的10重量％以下，其能够将聚合物（1）和有机试剂（3）的胶乳凝集为所述聚合物的重量的0.1至6倍（1），其能够溶解所述聚合物（1）中所含的未交联的聚合物和下述热塑性聚合物（4），并且在25℃下在水中的溶解度为5重量％以下，然后熔融混合熔融聚合物，其已经用热塑性树脂（4）进行了第一次脱挥发分化，然后使混合物进行第二脱挥发分; 以及包括从包含通过乳液聚合制备的聚合物（1）的胶乳的两相混合物中除去水相的方法，所述聚合物（1）的10重量％以下的水溶性试剂（2）），其能够将聚合物（1）的胶乳和有机试剂（3）的量以能够溶解在所述聚合物（1）中所含的未交联的聚合物的所述聚合物（1）的重量的0.1至6倍的量），并且在25℃下在水中的溶解度为5重量％以下，然后将熔融聚合物熔融混合，其中挥发性组分已经通过热方式与热塑性聚合物（4'）脱挥发分。

6. 发明授权

US4690974A Method for producing rubber modified thermoplastic resins 失效
标题翻译：橡胶改性热塑性树脂的制造方法
公开(公告)号：US4690974A
公开(公告)日：1987-09-01
申请号：US864868
申请日：1986-05-20
申请人： Teruhiko Sugimori , Noriyuki Tajiri , Yutaro Fukuda
发明人： Teruhiko Sugimori , Noriyuki Tajiri , Yutaro Fukuda
IPC分类号： C08J3/00 , C08L51/04 , C08L101/00 , C08L51/00
CPC分类号： C08L51/04 , C08J3/005 , C08L101/00
摘要： Disclosed is a method for producing a rubber modified thermoplastic resin excellent in surface appearance and various properties and high in commercial values which comprises removing an aqueous phase from a two-phase mixture comprising a graft rubber polymer latex (1) obtained by graft polymerization of vinyl monomer on a rubber latex, a thermoplastic resin (2), an organic agent in an amount of 0.1 to 6 times the weight of all the polymers (3) which is capable of dissolving said thermoplastic resin (2) and has a solubility in water of 5% by weight or less at 25.degree. C. and a water soluble agent in an amount of 10% by weight or less of said graft rubber polymer which can coagulate said latex and then removing said organic agent and remaining water from the remaining organic phase by a thermal means.
摘要翻译：公开了一种表面外观和各种性能和商业价值高的橡胶改性热塑性树脂的制造方法，其包括从包含通过乙烯基接枝聚合获得的接枝橡胶聚合物胶乳（1）的两相混合物中除去水相，橡胶胶乳上的单体，热塑性树脂（2），能够溶解所述热塑性树脂（2）的所有聚合物（3）的重量的0.1至6倍并且在水中具有溶解度的有机试剂在25℃下为5重量％以下的水溶性试剂和10重量％以下的所述接枝橡胶聚合物的水溶性试剂，其可以凝结所述胶乳，然后从剩余的有机物中除去所述有机试剂和剩余的水通过热方式进行相。

7. 发明授权

US4744744A Extrusion nozzle for coagulation of polymer latices 失效
标题翻译：用于聚合物胶乳凝结的挤出喷嘴
公开(公告)号：US4744744A
公开(公告)日：1988-05-17
申请号：US592365
申请日：1984-03-22
申请人： Teruhiko Sugimori , Noriyuki Tajiri , Akio Hironaka , Hideaki Habara
发明人： Teruhiko Sugimori , Noriyuki Tajiri , Akio Hironaka , Hideaki Habara
IPC分类号： B29B9/06 , B29B15/02 , B29B15/04 , B29C47/30
CPC分类号： B29B9/06 , B29B15/02 , B29B15/04 , Y10T29/53687
摘要： Apparatus for coagulation of a polymer latex by feeding the polymer latex to an extruder having a base plate and a plurality of fine tubes fixed to said base plate and extending therefrom, said fine tubes being mutually spaced by at least 1 mm and protruding from said base plate by at least 3 mm, and discharging said polymer latex through said fine tubes into coagulation solution to coagulate the latex and an extruder used for carrying out said method.
摘要翻译：一种通过将聚合物胶乳输送到具有底板的挤出机和固定到所述基板并从其延伸的多个细管的聚合物胶乳凝结的装置，所述细管相互间隔开至少1mm并从所述底部突出将所述聚合物胶乳通过所述细管排出到凝固溶液中以使胶乳和用于实施所述方法的挤出机凝结。

8. 发明授权

US4752522A Electrostatic recording material 失效
标题翻译：静电记录材料
公开(公告)号：US4752522A
公开(公告)日：1988-06-21
申请号：US847525
申请日：1986-04-03
申请人： Teruhiko Sugimori , Fumio Suzuki , Naoyuki Fukabori , Hideaki Habara
发明人： Teruhiko Sugimori , Fumio Suzuki , Naoyuki Fukabori , Hideaki Habara
IPC分类号： G03G5/02 , B32B3/00 , B32B5/16 , D21F11/00
CPC分类号： G03G5/0208 , Y10T428/24934 , Y10T428/25 , Y10T428/31895 , Y10T428/31899 , Y10T428/31902 , Y10T428/31906
摘要： An electrostatic recording material comprising a substrate treated for low electric resistance and a dielectric layer formed on the substrate and composed of a composition comprising an insulating resin having a volume specific resistance of at least 10.sup.12 .OMEGA.cm and a powder of an acrylonitrile-type polymer having a copolymerized acrylonitrile content of at least 95% by weight and containing substantially no ionic groups, said powder having a volume average particle size of from 1.5 to 4 .mu.m and a content of particles having a size exceeding 8 .mu.m as measured by a particle size distribution measuring apparatus, being at most 0.02% by number.
摘要翻译：一种静电记录材料，包括用于低电阻处理的基底和形成在基底上的电介质层，该电介质层由包含体积电阻率为至少1012欧米亚厘米的绝缘树脂和丙烯腈型聚合物的粉末组成的组合物组成，共聚丙烯腈含量为至少95重量％且基本上不含离子基团，所述粉末具有1.5至4μm的体积平均粒度和通过颗粒测量的尺寸超过8μm的颗粒含量尺寸分布测量装置，数量至多0.02％。

9. 发明授权

US4977241A Particulate polymer and preparation process thereof 失效
标题翻译：微粒聚合物及其制备方法
公开(公告)号：US4977241A
公开(公告)日：1990-12-11
申请号：US140670
申请日：1987-12-24
申请人： Teruhiko Sugimori , Fumio Suzuki , Hideaki Habara , Hiromasa Inada
发明人： Teruhiko Sugimori , Fumio Suzuki , Hideaki Habara , Hiromasa Inada
IPC分类号： C08F6/00 , C08C1/065 , C08F6/18 , C08J3/12 , C08J3/16
CPC分类号： C08C1/065 , C08F6/18 , C08J3/12 , C08J3/16 , C08J2321/02
摘要： Disclosed herein is a particulate polymer prepared by the agglomeration of polymer particles contained in a polymer latex. The particulate polymer is composed of primary particles having particle sizes of at least 20 .mu.m and/or secondary particles formed by the agglomeration of at least some of the primary particles and is in the form of a compact mass substantially free of voids. The particulate polymer is prepared by coagulating the polymer latex in the presence of a coagulant and an organic liquid having low solubility in water. The particulate polymer has a high bulk specific gravity and contains few fine particles. It is thus easy to handle and allows the consumption of energy to be reduced in the drying step.

10. 发明授权

US4874841A Particulate polymer and preparation process thereof 失效
标题翻译：微粒聚合物及其制备方法
公开(公告)号：US4874841A
公开(公告)日：1989-10-17
申请号：US898018
申请日：1986-08-19
申请人： Teruhiko Sugimori , Fumio Suzuki , Hideaki Habara , Hiromasa Inada
发明人： Teruhiko Sugimori , Fumio Suzuki , Hideaki Habara , Hiromasa Inada
IPC分类号： C08F6/00 , C08C1/065 , C08F6/18 , C08J3/12 , C08J3/16
CPC分类号： C08C1/065 , C08F6/18 , C08J3/12 , C08J3/16 , C08J2321/02
摘要： Disclosed herein is a particulate polymer prepared by the agglomeration of polymer particles contained in a polymer latex. The particulate polymer is composed of primary particles having particle sizes of at least 20 .mu.m and/or secondary particles formed by the agglomeration of at least some of the primary particles and is in the form of a compact mass substantially free of voids. The particulate polymer is prepared by coagulating the polymer latex in the presence of a coagulant and an organic liquid having low solubility in water. The particulate polymer has a high bulk specific gravity and contains few fine particles. It is thus easy to handle and allows the consumption of energy to be reduced in the drying step.
摘要翻译：本文公开了通过聚合物胶乳中包含的聚合物颗粒的聚集制备的颗粒聚合物。颗粒状聚合物由至少20μm的粒径的一次粒子和/或由至少一些初级粒子附聚形成的二次粒子组成，并且呈基本上不含空隙的致密质量的形式。颗粒聚合物通过在凝结剂和在水中溶解度低的有机液体存在下使聚合物胶乳凝结来制备。颗粒聚合物具有高堆积比重并且几乎没有细颗粒。因此，易于处理并允许在干燥步骤中减少能量的消耗。

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