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1. 发明授权

US4652625A N-aminopropyl derivatives of 2,4-diamino-2-methylpentane as epoxy curing agents 失效
标题翻译：作为环氧固化剂的2,4-二氨基-2-甲基戊烷的N-氨基丙基衍生物
公开(公告)号：US4652625A
公开(公告)日：1987-03-24
申请号：US830143
申请日：1986-02-18
申请人： Terry L. Renken , George P. Speranza , Harold G. Waddill
发明人： Terry L. Renken , George P. Speranza , Harold G. Waddill
IPC分类号： C08G59/50
CPC分类号： C08G59/5006
摘要： N-aminopropyl derivatives of 2,4-diamino-2-methylpentane show rapid curing when used to cure epoxy resins.
摘要翻译：当用于固化环氧树脂时，2,4-二氨基-2-甲基戊烷的N-氨基丙基衍生物显示快速固化。

2. 发明授权

US5250632A Heimd-containing polyetheramine curative for flexible, toughened products 失效
标题翻译：含Heimd的聚醚胺固化剂用于柔性，增韧的产品
公开(公告)号：US5250632A
公开(公告)日：1993-10-05
申请号：US928583
申请日：1992-08-13
申请人： Harold G. Waddill , Wei-Yang Su , Michael Cuscurida , Terry L. Renken
发明人： Harold G. Waddill , Wei-Yang Su , Michael Cuscurida , Terry L. Renken
IPC分类号： C08G59/50 , C08L63/00 , C08G59/40 , C08G59/62 , C08G65/00
CPC分类号： C08G59/5073 , C08L63/00
摘要： Disclosed is a novel polyetherdiamine comprising an aminated, alkoxylated 1-2'-hydroxyethyl-2-imidazolidone represented by the formula: ##STR1## where R is H or an alkyl group of from 1 to 16 carbon atoms and a+b=n, wherein n is a number from about 2 to 80, and to its use in epoxy resin curing systems to produce compositions having improved strength and flexibility properties compared with currently available polyoxyalkylenediamine curatives of equivalent weight.
摘要翻译：公开了一种新型的聚醚二胺，其包含由下式表示的胺化的烷氧基化的1-2'-羟乙基-2-咪唑烷酮：其中R是H或具有1至16个碳原子的烷基和a + b = n，其中n为约2至80的数，并且在环氧树脂固化体系中用于生产具有相当于目前可获得的当量聚氧化亚烷基二胺固化剂的具有改善的强度和柔软性的组合物。

3. 发明授权

US4735746A Long lasting detergent bar containing a polyamide or polyester polymer 失效
标题翻译：持久的洗涤剂棒含有聚酰胺或聚酯聚合物
公开(公告)号：US4735746A
公开(公告)日：1988-04-05
申请号：US29111
申请日：1987-03-23
申请人： George P. Speranza , Terry L. Renken
发明人： George P. Speranza , Terry L. Renken
IPC分类号： C11D3/37 , C11D17/00 , C11D9/30 , C11D11/04
CPC分类号： C11D3/3715 , C11D17/006 , C11D3/3719
摘要： A water-soluble polyamide or polyester is prepared or melted in the presence of a surface active agent. The polyamide or polyester is present in an amount of 5 to 95 wt % with the surfactant as the major portion of the balance. The composition is molded or shaped into long lasting detergent bars.In the specified range, compositions with more surface active agent are more suitable for detergent bars. Compositions with more polymer are more suitable for toys or shaped or molded articles.
摘要翻译：在表面活性剂的存在下制备或熔融水溶性聚酰胺或聚酯。以表面活性剂作为余量的主要部分，聚酰胺或聚酯的存在量为5〜95重量％。该组合物被模塑或成型为长久的洗涤剂条。在特定范围内，具有更多表面活性剂的组合物更适用于洗涤剂条。具有更多聚合物的组合物更适用于玩具或成形或模制品。

4. 发明授权

US5247078A Synthesis of diaza crown ethers 失效
标题翻译：二氮冠醚的合成
公开(公告)号：US5247078A
公开(公告)日：1993-09-21
申请号：US694706
申请日：1991-05-02
申请人： Donald H. Champion , George P. Speranza , Terry L. Renken
发明人： Donald H. Champion , George P. Speranza , Terry L. Renken
IPC分类号： C07D273/00 , C07D273/08
CPC分类号： C07D273/00
摘要： Poly(ethyleneoxy)amines, such as those having the structure:H.sub.2 N--(CH.sub.2).sub.a --(OCH.sub.2 CH.sub.2).sub.b --NH--(CH.sub.2 CH.sub.2 O).sub.c --(CH.sub.2).sub.d --Rwhere a and d are independently 2 to 3; b and c are independently 1 to 4 and R is --OH or --NH.sub.2, may be reacted over a transition metal catalyst such as one containing nickel to produce diaza crown ethers, such as, for example 4,13-diaza-18-crown-6. If the poly(ethyleneoxy)amine is a diamine having a hydroxyl group of the above formula, the reaction may produce the corresponding triamine in the presence of ammonia. These triamines also readily form diaza crown ethers at near complete conversions simply from nickel, platinum, and palladium metal catalysts alone or with other transition metals such as copper and/or chromium. The process avoids tedious, multiple step procedures and the high dilutions that accompany prior diaza crown ether preparations.
摘要翻译：聚（乙烯氧基）胺，例如具有以下结构的那些：H 2 N - （CH 2）a - （OCH 2 CH 2）b -NH-（CH 2 CH 2 O）c - （CH 2）d -R，其中a和d独立地为2至3; b和c独立地为1至4并且R为-OH或-NH 2，可以在过渡金属催化剂如含镍的反应物上反应以制备二氮杂冠醚，例如4,13-二氮杂-18-冠 -6。如果聚（乙烯氧基）胺是具有上式的羟基的二胺，则反应可在氨的存在下产生相应的三胺。这些三胺也可以简单地从镍，铂和钯金属催化剂单独或与其它过渡金属如铜和/或铬接近完全转化形成二氮冠醚。该过程避免了繁琐的多步骤程序和伴随以前的碳酸乙醚制备的高稀释度。

5. 发明申请

US20110009670A1 CYCLOHEXANEDIMETHANAMINE BY DIRECT AMINATION OF CYCLOHEXANEDIMETHANOL 审中-公开
标题翻译：环己烷二甲胺通过环己烷二甲醇的直接胺化
公开(公告)号：US20110009670A1
公开(公告)日：2011-01-13
申请号：US12919435
申请日：2009-03-09
申请人： Terry L. Renken , Howard P. Klein
发明人： Terry L. Renken , Howard P. Klein
IPC分类号： C07C209/04
CPC分类号： C07C209/16 , C07C2601/14 , C07C211/18
摘要： Embodiments of the present invention include methods for producing a cyclohexanedimethanamine by a reductive amination process.
摘要翻译：本发明的实施方案包括通过还原胺化方法制备环己烷二甲胺的方法。

6. 发明授权

US5352835A Supported catalysts for amination 失效
标题翻译：用于胺化的支持催化剂
公开(公告)号：US5352835A
公开(公告)日：1994-10-04
申请号：US14583
申请日：1993-02-08
申请人： Pei-Shing E. Dai , Terry L. Renken , Laurence D. Neff
发明人： Pei-Shing E. Dai , Terry L. Renken , Laurence D. Neff
IPC分类号： C07C213/02 , C07C209/16
CPC分类号： C07C213/02
摘要： Disclosed is a process for the amination of polyols to form primary amines which comprises reacting a polyoxyalkylene alcohol or polyol having a molecular weight of from about 230 to 5000 and ammonia in the presence of hydrogen over a catalyst consisting essentially of 10 to 35 wt % nickel, 1 to 20 wt % copper and 0.1 to 2.0 wt % optionally chromium or molybdenum promoter impregnated onto a .theta.-alumina support at a temperature of 100.degree. C. to 300.degree. C. and a pressure of 1000 psig to 3000 psig wherein the .theta.-alumina support results from calcining .gamma.-alumina or pseudo-boehmite for 2-4 hours at 900.degree.-1100.degree. C.
摘要翻译：公开了一种用于胺化多元醇以形成伯胺的方法，其包括在氢气存在下使分子量为约230至5000的聚氧化烯醇或多元醇与氨反应，催化剂基本上由10至35重量％的镍，1至20重量％的铜和0.1至2.0重量％的任选的铬或钼助催化剂，其在100℃至300℃的温度和1000psig至3000psig的压力下浸渍在θ-氧化铝载体上，其中θ 氧化铝载体的结果是在900℃-1100℃煅烧γ-氧化铝或假勃姆石2-4小时。

7. 发明授权

US4766245A Process for the preparation of polyoxyalkylene polyamines 失效
标题翻译：聚氧化烯多胺的制备方法
公开(公告)号：US4766245A
公开(公告)日：1988-08-23
申请号：US707126
申请日：1985-03-01
申请人： John M. Larkin , Terry L. Renken
发明人： John M. Larkin , Terry L. Renken
IPC分类号： C08G65/32 , C08G65/325 , C07C85/02 , C07C85/06
CPC分类号： C08G65/3255
摘要： An improved method for the manufacture of high molecular weight polyoxyalkylene amines wherein a hydroxy-terminated polyoxyalkylene compound having a molecular weight of at least 500 is reacted with ammonia in the presence of hydrogen and Raney nickel/aluminum under anhydrous reductive amination conditions to provide the corresponding polyoxyalkylene amine in good yield and selectivity.The Raney nickel/aluminum is a nickel/aluminum alloy treated with a base, such as sodium hydroxide, so as to only partially leach the aluminum from the alloy, such that the final product contains from about 60 wt. % to about 75 wt. % of nickel and, correspondingly, from about 25 wt. % to about 40 wt. % of aluminum and is preferably used in nugget form.
摘要翻译：制备高分子量聚氧化烯胺的改进方法，其中分子量至少为500的羟基封端的聚氧化烯化合物在无水还原胺化条件下在氢和阮内镍/铝的存在下与氨反应，以提供相应的聚氧亚烷基胺具有良好的收率和选择性。阮内镍/铝是用碱如氢氧化钠处理的镍/铝合金，以便仅从合金中部分浸出铝，使得最终产物含有约60wt。％至约75wt。的镍，相应地为约25wt。％至约40wt。铝的百分比，优选以熔核形式使用。

8. 发明授权

US4642303A Catalyst composition 失效
标题翻译：催化剂组成
公开(公告)号：US4642303A
公开(公告)日：1987-02-10
申请号：US813884
申请日：1985-12-27
申请人： Terry L. Renken
发明人： Terry L. Renken
IPC分类号： B01J23/86 , C07D295/023 , B01J23/72
CPC分类号： C07D295/023 , B01J23/868
摘要： The present invention is directed to catalyst compositions containing nickel, copper, chromium and iron which are useful for promoting reductive amination reactions, such as the conversion of feedstocks containing one or more hydroxyl groups to corresponding amine compounds including acyclic, cyclic and heterocyclic amines. For example, the catalyst compositions of the present invention may be utilized to convert monoethanolamine to ethylenediamine and piperazine, for the conversion of diethylene glycol to morpholine and diglycolamine, etc.
摘要翻译：本发明涉及含有镍，铜，铬和铁的催化剂组合物，其可用于促进还原胺化反应，例如将含有一个或多个羟基的原料转化成包括无环，环状和杂环胺的相应胺化合物。例如，本发明的催化剂组合物可用于将单乙醇胺转化为乙二胺和哌嗪，以将二甘醇转化为吗啉和二甘醇胺等。

9. 发明授权

US4517374A Cycloalkane epoxides produced by air oxidation of cycloalkenes over oxide catalysts 失效
标题翻译：通过环氧烯烃在氧化物催化剂上空气氧化制备的环烷烃环氧化物
公开(公告)号：US4517374A
公开(公告)日：1985-05-14
申请号：US510142
申请日：1983-07-01
申请人： John R. Sanderson , Lewis W. Watts, Jr. , Terry L. Renken
发明人： John R. Sanderson , Lewis W. Watts, Jr. , Terry L. Renken
IPC分类号： B01J23/86 , C07D301/06 , C07D303/04
CPC分类号： B01J23/868 , C07D301/06 , C07D303/04
摘要： A process for the production of cycloalkane epoxides from cycloalkenes in the presence of an oxide catalyst, oxygen and a carboxylate ion source via air oxidation is described. The oxide catalyst may have as a cation boron, chromium, iron, nickel, copper, zinc or terbium or mixtures thereof. Combination catalysts such as ferric oxide/zinc oxide and nickel oxide/copper oxide/chromium oxide/boric oxide complexes are also found to be useful. The reaction is conducted at a temperature in the range of 50.degree. to 150.degree. C. and a pressure of one atmosphere or greater. Cycloalkane epoxides are useful in the preparation of resins, plasticizers, etc.
摘要翻译：描述了在氧化物催化剂，氧气和羧酸根离子源通过空气氧化存在下从环烯烃制备环烷烃环氧化物的方法。氧化物催化剂可以具有阳离子硼，铬，铁，镍，铜，锌或铽或其混合物。还发现组合催化剂如氧化铁/氧化锌和氧化镍/氧化铜/氧化铬/氧化硼络合物是有用的。该反应在50℃至150℃的温度和一个或多于一个气压的压力下进行。环烷烃环氧化物可用于制备树脂，增塑剂等

10. 发明授权

US09067865B2 Etheramines and their use as intermediates for polymer synthesis 有权
标题翻译：醚胺及其作为聚合物合成中间体的用途
公开(公告)号：US09067865B2
公开(公告)日：2015-06-30
申请号：US13516879
申请日：2010-12-21
申请人： Howard P. Klein , Terry L. Renken , Martin J. Renner , Bruce L. Burton , Katty Darragas
发明人： Howard P. Klein , Terry L. Renken , Martin J. Renner , Bruce L. Burton , Katty Darragas
IPC分类号： C07C217/42 , C07C213/02 , C08G59/50 , C08G59/56 , C08G18/08 , C08G18/32
CPC分类号： C07C217/42 , C07C213/02 , C08G18/08 , C08G18/32 , C08G59/5006 , C08G59/56
摘要： The present invention relates to an etheramine mixture containing a monoether diamine and its method of production by alkoxylating an initiator with an alkylene oxide to produce a precursor polyol and reductively aminating the precursor polyol to form the etheramine mixture. The etheramine mixture may be used in variety of applications including as a curing agent for an epoxy resin or as a reactant in the production of polyurea.
摘要翻译：本发明涉及一种含有单醚二胺的醚胺混合物及其制备方法，其通过使烯化氧烷氧基化引发剂以制备前体多元醇并还原胺化前体多元醇以形成醚胺混合物。醚胺混合物可用于多种应用，包括作为环氧树脂的固化剂或作为制备聚脲的反应物。

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