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1. 发明申请

US20120309906A1 POLYMERS FUNCTIONALIZED WITH HALOSILANES CONTAINING AN AMINO GROUP 有权
标题翻译：聚合物与含有氨基酸的半胱氨酸官能化
公开(公告)号：US20120309906A1
公开(公告)日：2012-12-06
申请号：US13588033
申请日：2012-08-17
申请人： Terrence E. Hogan , Steven Luo , Yoichi Ozawa , Matsushita Junko , Nakagawa Ryuji , Suzuki Eiju , Ken Tanaka
发明人： Terrence E. Hogan , Steven Luo , Yoichi Ozawa , Matsushita Junko , Nakagawa Ryuji , Suzuki Eiju , Ken Tanaka
IPC分类号： C08F236/06 , C08F8/32
CPC分类号： C08C19/44 , C08F8/42 , C08L15/00 , C08L19/006 , C08F297/04
摘要： A method for preparing a functionalized polymer, the method comprising the steps of preparing a reactive polymer, and reacting the reactive polymer with a halosilane compound containing an amino group.
摘要翻译：一种制备官能化聚合物的方法，该方法包括如下步骤：制备反应性聚合物，并使反应性聚合物与含有氨基的卤代硅烷化合物反应。

2. 发明授权

US08258332B2 Polymers functionalized with halosilanes containing an amino group 有权
标题翻译：用含有氨基的卤代硅烷官能化的聚合物
公开(公告)号：US08258332B2
公开(公告)日：2012-09-04
申请号：US12665539
申请日：2008-06-18
申请人： Terrence E. Hogan , Steven Luo , Yoichi Ozawa , Junko Matsushita , Ryuji Nakagawa , Eiju Suzuki , Ken Tanaka
发明人： Terrence E. Hogan , Steven Luo , Yoichi Ozawa , Junko Matsushita , Ryuji Nakagawa , Eiju Suzuki , Ken Tanaka
IPC分类号： C08F4/44 , C08F8/32 , C07F7/02 , C09K3/00
CPC分类号： C08C19/44 , C08F8/42 , C08L15/00 , C08L19/006 , C08F297/04
摘要： A method for preparing a functionalized polymer, the method comprising the steps of preparing a reactive polymer, and reacting the reactive polymer with a halosilane compound containing an amino group.
摘要翻译：一种制备官能化聚合物的方法，该方法包括如下步骤：制备反应性聚合物，并使反应性聚合物与含有氨基的卤代硅烷化合物反应。

3. 发明授权

US08809464B2 Polymers functionalized with halosilanes containing an amino group 有权
标题翻译：用含有氨基的卤代硅烷官能化的聚合物
公开(公告)号：US08809464B2
公开(公告)日：2014-08-19
申请号：US13588033
申请日：2012-08-17
申请人： Terrence E. Hogan , Steven Luo , Yoichi Ozawa , Junko Matsushita , Ryuji Nakagawa , Eiju Suzuki , Ken Tanaka
发明人： Terrence E. Hogan , Steven Luo , Yoichi Ozawa , Junko Matsushita , Ryuji Nakagawa , Eiju Suzuki , Ken Tanaka
IPC分类号： C08F236/06 , C08F8/32
CPC分类号： C08C19/44 , C08F8/42 , C08L15/00 , C08L19/006 , C08F297/04
摘要： A method for preparing a functionalized polymer, the method comprising the steps of preparing a reactive polymer, and reacting the reactive polymer with a halosilane compound containing an amino group.
摘要翻译：一种制备官能化聚合物的方法，该方法包括如下步骤：制备反应性聚合物，并使反应性聚合物与含有氨基的卤代硅烷化合物反应。

4. 发明申请

US20100016496A1 PROCESS FOR PRODUCTION OF MODIFIED CONJUGATED DIENE POLYMERS, MODIFIED CONJUGATED DIENE POLYMERS PRODUCED BY THE PROCESS, RUBBER COMPOSITIONS, AND TIRES 有权
标题翻译：生产改性共轭二烯聚合物的方法，由工艺生产的改性的共混二烯聚合物，橡胶组合物和轮胎
公开(公告)号：US20100016496A1
公开(公告)日：2010-01-21
申请号：US12446799
申请日：2007-10-25
申请人： Ken Tanaka , Kouji Masaki , Yoichi Ozawa , Eiji Suzuki , Christine M. Rademacher , Terrence E. Hogan , Takuo Sone , Takaomi Matsumoto
发明人： Ken Tanaka , Kouji Masaki , Yoichi Ozawa , Eiji Suzuki , Christine M. Rademacher , Terrence E. Hogan , Takuo Sone , Takaomi Matsumoto
IPC分类号： C08L83/04 , C08G77/08
CPC分类号： C08C19/25 , B60C1/0016 , B60C1/0025 , C08C19/44 , C08K3/04 , C08K3/36 , C08L9/00 , C08L15/00 , C08L21/00 , C08L2666/08
摘要： The invention provides a process for producing a modified conjugated diene based polymer which attains favorable interaction between a rubber component and carbon black and/or silica, thereby improving dispersibility of the fillers, and which exhibits excellent properties such as heat-buildup-suppressing performance, fracture characteristics, and wear resistance; a modified conjugated diene based polymer produced through the process; a rubber composition containing the diene polymer; and a tire produced from the rubber composition and exhibiting the above properties. The process for producing a modified conjugated diene based polymer includes a step (a) of reacting a silicon compound with a conjugated diene based polymer having an active end so that the reaction takes place at the active end, the silicon compound having a protected primary amino group in the molecule thereof and a bi-functional silicon atom to which a hydrocarbyloxy group and a reactive group are bonded, to thereby modify the active end, and a step (b) of performing condensation reaction which involves the compound having a bi-functional silicon atom, in the presence of a titanium compound serving as a titanium-based condensation-accelerating agent.
摘要翻译：本发明提供了一种制备改性共轭二烯系聚合物的方法，其在橡胶组分与炭黑和/或二氧化硅之间具有良好的相互作用，从而提高填料的分散性，并且具有优异的性能如发热抑制性能，断裂特性和耐磨性; 通过该方法制备的改性共轭二烯基聚合物; 含有二烯聚合物的橡胶组合物; 以及由橡胶组合物制成并具有上述特性的轮胎。改性共轭二烯系聚合物的制造方法包括使硅化合物与具有活性末端的共轭二烯系聚合物反应的步骤（a），使得反应在活性末端进行，具有被保护的伯氨基在其分子中具有烃氧基和反应性基团键合的双功能硅原子，从而改变活性末端，以及进行缩合反应的步骤（b），其涉及具有双官能团的化合物硅原子，在用作钛基缩合促进剂的钛化合物的存在下。

5. 发明申请

US20080103261A1 Process for producing modified conjugated diene based polymer, modified conjugated diene based polymer produced by the process, rubber composition, and tire 审中-公开
标题翻译：制造改性共轭二烯系聚合物，通过该方法制造的改性共轭二烯系聚合物，橡胶组合物和轮胎的方法
公开(公告)号：US20080103261A1
公开(公告)日：2008-05-01
申请号：US11585810
申请日：2006-10-25
申请人： Ken Tanaka , Koji Masaki , Yoichi Ozawa , Eiju Suzuki , Christine M. Rademacher , Terrence E. Hogan
发明人： Ken Tanaka , Koji Masaki , Yoichi Ozawa , Eiju Suzuki , Christine M. Rademacher , Terrence E. Hogan
IPC分类号： C08F136/00
CPC分类号： C08C19/25 , B60C1/0016 , B60C1/0025 , C08C19/44 , C08K3/04 , C08K3/36 , C08L9/00 , C08L15/00 , C08L21/00 , C08L2666/08
摘要： The invention provides a process for producing a modified conjugated diene based polymer which attains favorable interaction between a rubber component and carbon black and/or silica, thereby improving dispersibility of the fillers, and which exhibits excellent properties such as heat-buildup-suppressing performance, fracture characteristics, and wear resistance; a modified conjugated diene based polymer produced through the process; a rubber composition containing the diene polymer; and a tire produced from the rubber composition and exhibiting the above properties. The process for producing a modified conjugated diene based polymer includes a step (a) of reacting a silicon compound with a conjugated diene based polymer having an active end so that the reaction takes place at the active end, the silicon compound having a protected primary amino group in the molecule thereof and a bi-functional silicon atom to which a hydrocarbyloxy group and a reactive group including a hydrocarbyloxy group are bonded, to thereby modify the active end, and a step (b) of performing condensation reaction which involves the compound having a bi-functional silicon atom, in the presence of a titanium compound serving as a titanium-based condensation-accelerating agent.
摘要翻译：本发明提供了一种制备改性共轭二烯系聚合物的方法，其在橡胶组分与炭黑和/或二氧化硅之间具有良好的相互作用，从而提高填料的分散性，并且具有优异的性能如发热抑制性能，断裂特性和耐磨性; 通过该方法制备的改性共轭二烯基聚合物; 含有二烯聚合物的橡胶组合物; 以及由橡胶组合物制成并具有上述特性的轮胎。改性共轭二烯系聚合物的制造方法包括使硅化合物与具有活性末端的共轭二烯系聚合物反应的步骤（a），使得反应在活性末端进行，具有被保护的伯氨基在其分子中具有烃氧基和含有烃氧基的反应性基团键合的双官能硅原子，从而改变活性末端，和进行缩合反应的步骤（b），其包括具有在用作钛基缩合促进剂的钛化合物存在下，是双功能硅原子。

6. 发明授权

US09056925B2 Process for production of modified conjugated diene polymers, modified conjugated diene polymers produced by the process, rubber compositions, and tires 有权
标题翻译：改性共轭二烯聚合物的制备方法，通过该方法制备的改性共轭二烯聚合物，橡胶组合物和轮胎
公开(公告)号：US09056925B2
公开(公告)日：2015-06-16
申请号：US12446799
申请日：2007-10-25
申请人： Ken Tanaka , Kouji Masaki , Yoichi Ozawa , Eiji Suzuki , Christine M. Rademacher , Terrence E. Hogan , Takuo Sone , Takaomi Matsumoto
发明人： Ken Tanaka , Kouji Masaki , Yoichi Ozawa , Eiji Suzuki , Christine M. Rademacher , Terrence E. Hogan , Takuo Sone , Takaomi Matsumoto
IPC分类号： C08L83/00 , C08C19/25 , B60C1/00 , C08C19/44 , C08L15/00 , C08L21/00
CPC分类号： C08C19/25 , B60C1/0016 , B60C1/0025 , C08C19/44 , C08K3/04 , C08K3/36 , C08L9/00 , C08L15/00 , C08L21/00 , C08L2666/08
摘要： A process for producing a modified conjugated diene based polymer includes a step (a) of reacting a silicon compound with a conjugated diene based polymer having an active end so that the reaction takes place at the active end, the silicon compound having a protected primary amino group in the molecule thereof and a silicon atom to which a hydrocarbyloxy group and a reactive group are bonded, to thereby modify the active end, and a step (b) of performing condensation reaction, in the presence of a titanium compound serving as a titanium-based condensation-accelerating agent. A rubber composition contains the modified diene polymer, and a tire is produced from the rubber composition.
摘要翻译：改性共轭二烯系聚合物的制造方法包括使硅化合物与具有活性末端的共轭二烯系聚合物反应以使反应在活性末端进行的工序（a），具有被保护的伯氨基在其分子中具有烃氧基和反应性基团键合的硅原子，从而改变活性末端，以及在用作钛的钛化合物的存在下进行缩合反应的步骤（b）的缩合促进剂。橡胶组合物含有改性二烯聚合物，由橡胶组合物制成轮胎。

7. 发明授权

US07598322B1 Functionalized polymers and improved tires therefrom 有权
标题翻译：官能化聚合物和改良的轮胎
公开(公告)号：US07598322B1
公开(公告)日：2009-10-06
申请号：US11189891
申请日：2005-07-26
申请人： Christine Rademacher , Steven Luo , Terrence E. Hogan
发明人： Christine Rademacher , Steven Luo , Terrence E. Hogan
IPC分类号： C08C19/34 , C08C19/00
CPC分类号： C08C19/44 , B60C1/0016 , C08K3/013 , C08L15/00
摘要： A tire component comprising a vulcanized rubber deriving from a functionalized polymer defined by the formula I where π is a polymer chain, B is a boron atom, R1 is a bond or a divalent organic group, and each υ is independently selected from alkoxy groups (—OR), thioalkoxy groups (—SR), amino groups (—NR2), or phosphino groups (—PR2), where each R is independently selected from monovalent organic groups or two R groups form a divalent organic group, which forms a cyclic structure.
摘要翻译：一种轮胎组件，其包含衍生自由式I定义的官能化聚合物的硫化橡胶，其中p 1是聚合物链，B是硼原子，R 1是键或二价有机基团，并且各自独立地选自烷氧基（ -OR），硫代烷氧基（-SR），氨基（-NR2）或膦基（-PR2），其中每个R独立地选自一价有机基团或两个R基团形成二价有机基团，其形成环状结构体。

8. 发明授权

US08399570B2 Functionalized polymers and improved tires therefrom 有权
标题翻译：官能化聚合物和改良的轮胎
公开(公告)号：US08399570B2
公开(公告)日：2013-03-19
申请号：US12555843
申请日：2009-09-09
申请人： Christine Rademacher , Steven Luo , Terrence E. Hogan
发明人： Christine Rademacher , Steven Luo , Terrence E. Hogan
IPC分类号： C08C19/00 , C08C19/22
CPC分类号： C08C19/44 , B60C1/0016 , C08K3/013 , C08L15/00
摘要： A tire component comprising a vulcanized residue of a functionalized polymer defined by the formula I where π is a rubbery polymer chain, B is a boron atom, R1 is a bond or a divalent organic group, and each υ is independently selected from thioalkoxy groups (—SR), amino groups (—NR2), or phosphino groups (—PR2), where each R is independently selected from monovalent organic groups or two R groups form a divalent organic group, which forms a cyclic structure.
摘要翻译：一种轮胎组件，其包含由式I定义的官能化聚合物的硫化残余物，其中pgr; 是橡胶状聚合物链，B是硼原子，R1是键或二价有机基团，每个υ独立地选自硫代烷氧基（-SR），氨基（-NR2）或膦基（-PR2）其中每个R独立地选自一价有机基团或两个R基团形成二价有机基团，其形成环状结构。

9. 发明申请

US20090326161A1 FUNCTIONALIZED POLYMERS AND IMPROVED TIRES THEREFROM 有权
标题翻译：功能化的聚合物和改进的轮胎
公开(公告)号：US20090326161A1
公开(公告)日：2009-12-31
申请号：US12555843
申请日：2009-09-09
申请人： Christine Rademacher , Steven Luo , Terrence E. Hogan
发明人： Christine Rademacher , Steven Luo , Terrence E. Hogan
IPC分类号： C08F30/06
CPC分类号： C08C19/44 , B60C1/0016 , C08K3/013 , C08L15/00
摘要： A tire component comprising a vulcanized residue of a functionalized polymer defined by the formula I where π is a rubbery polymer chain, B is a boron atom, R1 is a bond or a divalent organic group, and each υ is independently selected from thioalkoxy groups (—SR), amino groups (—NR2), or phosphino groups (—PR2), where each R is independently selected from monovalent organic groups or two R groups form a divalent organic group, which forms a cyclic structure.
摘要翻译：一种轮胎组件，其包含由式I定义的官能化聚合物的硫化残余物，其中p1是橡胶状聚合物链，B是硼原子，R 1是键或二价有机基团，并且各自独立地选自硫代烷氧基（ -SR），氨基（-NR2）或膦基（-PR2），其中每个R独立地选自一价有机基团或两个R基团形成二价有机基团，其形成环状结构。

10. 发明授权

US08822620B2 Method for making alkoxy-modified silsesquioxanes 有权
标题翻译：制备烷氧基改性倍半硅氧烷的方法
公开(公告)号：US08822620B2
公开(公告)日：2014-09-02
申请号：US13030611
申请日：2011-02-18
申请人： William L. Hergenrother , James H. Pawlow , Terrence E. Hogan , Ashley S. Hilton
发明人： William L. Hergenrother , James H. Pawlow , Terrence E. Hogan , Ashley S. Hilton
IPC分类号： C08G77/08
CPC分类号： C08G77/08 , B60C1/00 , C08G77/18 , C08G77/28 , C08K3/013 , C08L9/00 , C08L21/00 , C08L83/06 , C08L83/08 , Y02P20/584 , C08L83/00
摘要： A method is presented for making alkoxy-modified silsesquioxanes (AMS) or co-alkoxy-modified silsesquioxanes (co-AMS,) comprising the steps of (a) combining as a reaction mixture (i) water, (ii) an acid-stable solvent for the water, (iii) a solid strong cationic hydrolysis and condensation catalyst, and (iv) a trialkoxysilane compound, (b) allowing the reaction mixture to react for about 0.5 hours to about 200 hours to form the alkoxy-modified silsesquioxanes; and (c) recovering the alkoxy-modified silsesquioxanes from the reaction mixture. The use of solid strong cationic catalysts in this reaction system is advantageous because they remain as solids throughout the reaction, allowing simplified separation of the solid catalyst from the soluble AMS or co-AMS products, resulting in total or near total recovery of the AMS or co-AMS products, the products being free of, or substantially free of residual acid catalyst, as well as virtual total recovery of the catalyst for recycling. The improved AMS and co-AMS compounds, vulcanizable rubber compounds containing them, and a pneumatic tire having a component made from the vulcanized rubber compounds are also presented.
摘要翻译：提出了制备烷氧基改性倍半硅氧烷（AMS）或共 - 烷氧基改性倍半硅氧烷（co-AMS）的方法，该方法包括以下步骤：（a）将反应混合物（i）和（ii）酸稳定溶剂，（iii）固体强阳离子水解和缩合催化剂，和（iv）三烷氧基硅烷化合物，（b）使反应混合物反应约0.5小时至约200小时以形成烷氧基改性倍半硅氧烷; 和（c）从反应混合物中回收烷氧基改性的倍半硅氧烷。在该反应系统中使用固体强阳离子催化剂是有利的，因为它们在整个反应中保持固体，允许固体催化剂与可溶性AMS或共AMS产物的简单分离，导致AMS或共AMS产品，产品没有或基本上没有残留的酸催化剂，以及用于再循环的催化剂的虚拟总回收。还提出了改进的AMS和共AMS化合物，含有它们的可硫化橡胶化合物和具有由硫化橡胶化合物制成的组分的充气轮胎。

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