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    • 1. 发明授权
    • Edging mill for section rolling
    • 磨边机用于轧制
    • US5295380A
    • 1994-03-22
    • US928435
    • 1992-08-12
    • Takeshi HiokiToru IkezakiYasushi HoriuchiKazufumi HiroseYoshun YamamotoMasanori Fujiwara
    • Takeshi HiokiToru IkezakiYasushi HoriuchiKazufumi HiroseYoshun YamamotoMasanori Fujiwara
    • B21B1/08B21B27/02B21B31/26B21B31/16
    • B21B1/0886B21B27/028B21B31/26
    • An edging mill for section rolling has a pair of horizontal rolls, each horizontal roll including a pair of axially spaced horizontal roll segments supported by driven horizontal roll shafts. Eccentric rings are disposed between the two horizontal roll segments making up each horizontal roll and are rotatably mounted on the horizontal roll shaft. The eccentric rings are eccentric to the horizontal rolls. Web-restraining ring rolls each comprise a pair of web-restraining roll segments rotatably fitted over the periphery of the eccentric rings concentrically thereto. A web-restraining ring roll positioning device rotates the eccentric rings. While the horizontal rolls roll the flange edges of the section, the web-restraining ring rolls hold the web of the section therebetween. The position of the web-restraining ring rolls with respect to the horizontal rolls changes with the rotating angle of the eccentric rings. The position of the web-restraining ring rolls is adjusted according to the flange thickness of the section.
    • 用于截面轧制的磨边机具有一对水平辊,每个水平辊包括由从动水平辊轴支撑的一对轴向间隔开的水平辊段。 偏心环设置在构成每个水平辊的两个水平辊段之间并且可旋转地安装在水平辊轴上。 偏心环与水平辊偏心。 卷筒纸限制环卷每一个包括一对卷筒纸限制卷筒部分,其可旋转地装配在与其同心的偏心环的周边上。 卷筒纸限定环辊定位装置使偏心环旋转。 当横向辊滚动该部分的凸缘边缘时,幅材限制环辊保持该部分的腹板。 卷筒纸限制环相对于水平卷筒的位置随偏心环的旋转角度而变化。 纤维网限制环辊的位置根据截面的凸缘厚度进行调整。
    • 4. 发明授权
    • Radiation-sensitive positive resist composition
    • 辐射敏感正光刻胶组合物
    • US5792585A
    • 1998-08-11
    • US217892
    • 1994-03-25
    • Ayako IdaHaruyoshi OsakiTakeshi HiokiYasunori DoiYasunori UetaniRyotaro Hanawa
    • Ayako IdaHaruyoshi OsakiTakeshi HiokiYasunori DoiYasunori UetaniRyotaro Hanawa
    • C07C39/15G03F7/004G03F7/022G03F7/023H01L21/027H01L21/30
    • G03F7/022C07C39/15G03F7/0226G03F7/0236
    • A positive resist composition comprising 1,2-quinonediazide compound and, as an alkali-soluble resin, an alkali-soluble resin (A) which comprises a resin (I) obtainable through a condensation reaction of a mixture of m-cresol, 2,3,5-trimethylphenol and optionally p-cresol with an aldehyde and a low molecular weight novolak (II) having a weight average molecular weight of 200 to 2000 as converted to polystyrene, an alkali-soluble resin (B) which comprises a resin (I) and a compound of the general formula (III): ##STR1## wherein R.sub.1, R.sub.2 and R.sub.3 are respectively a C.sub.1 -C.sub.5 alkyl group or a C.sub.1 -C.sub.5 alkoxy group, 1, m and n are respectively a number of 0 to 3, R' is a hydrogen atom or a C.sub.1 -C.sub.3 alkyl group, or an alkali-soluble resin (C) which comprises a resin (IV) obtainable through a condensation reaction of a mixture of m-methoxyphenol and 2,3,5-trimethylphenol in a molar ratio of 80:20 to 30:70 with an aldehyde, which has good sensitivity, improved resolution and heat resistance.
    • 包含1,2-醌二叠氮化合物的正性抗蚀剂组合物和作为碱溶性树脂的碱溶性树脂(A),其包含可通过间甲酚,2,5-二氯苯的混合物的缩合反应获得的树脂(I) 3,5-二甲基苯酚和任选的具有醛和低分子量酚醛清漆(II)的对甲酚,其重均分子量为200至2000,转化为聚苯乙烯,碱溶性树脂(B)包含树脂( I)和通式(III)的化合物:其中R 1,R 2和R 3分别是C 1 -C 5烷基或C 1 -C 5烷氧基,m和n分别为0〜 3,R'是氢原子或C1-C3烷基,或碱溶性树脂(C),其包含可通过间 - 甲氧基苯酚和2,3,5-三羟基苯酚的混合物的缩合反应获得的树脂(IV) - 三甲基苯酚与摩尔比为80:20至30:70的醛,其具有良好的灵敏度,改进的分辨率和耐热性。
    • 5. 发明授权
    • Process for producing O,O-di-lower-alkylchlorothiophosphate
    • O,O-二低级烷基氯代硫代磷酸酯的制备方法
    • US4769494A
    • 1988-09-06
    • US11009
    • 1987-02-05
    • Motomasa OhsuKoichi KamemotoManabu YahataTooru TokumaruTakeshi HiokiHiroshi Ueda
    • Motomasa OhsuKoichi KamemotoManabu YahataTooru TokumaruTakeshi HiokiHiroshi Ueda
    • C07F9/20C07F9/02
    • C07F9/20
    • A continuous process for producing O,O-di-lower alkylchlorothiophosphate very important as an intermediate for organo-phosphate series agricultural chemicals which comprises continuously reacting phosphorus sulfochloride with a lower alcohol in the presence of caustic soda according to a multi-stage reaction form comprising from 3 to 8 stages in which the following conditions are satisfied:(1) The amounts of caustic soda and a lower alcohol used shall be from 2 to 2.2 moles and 10 moles or more, respectively, based on 1 mole of phosphorus sulfochloride.(2) Caustic soda, water and the lower alcohol shall be used as a caustic soda/water/lower alcohol solution, and besides the caustic soda concentration of the aqueous caustic soda in said solution shall be from 30.0 to 99.5 wt.%.(3) To the 1st reaction stage shall be continuously supplied the whole amount of phosphorus sulfochloride required and from 45 to 85 wt.% each of the amounts of caustic soda and the lower alcohol required; and to the 2nd and subsequent reaction stages shall be continuously supplied the residual caustic soda and lower alcohol in divided portions so that the substantial amounts supplied become successively small toward the final reaction stage.(4) The temperature of the reaction system shall be -5.degree. C. or lower.(5) The residence time in the reaction system shall be within 4 hours.
    • 一种用于生产作为有机磷酸酯系农药的中间体非常重要的O,O-二低级烷基氯硫代磷酸酯的连续方法,其包括在苛性钠存在下,根据多阶段反应形式连续地使磷酰氯与低级醇反应,包括 从3到8个阶段,其中满足以下条件:(1)基于1摩尔磷酰氯,苛性钠和低级醇的用量分别为2至2.2摩尔和10摩尔或更多。 (2)苛性钠,水和低级醇应用作苛性钠/水/低级醇溶液,除了所述溶液中的苛性钠水溶液的苛性钠浓度外还应为30.0至99.5重量%。 (3)向第一反应阶段连续供应所需的全部硫磺磷酸盐和每一种苛性钠和所需的低级醇的45至85重量%; 并且连续向第二和随后的反应阶段连续地供应残留的苛性钠和低级醇,使得所供应的实质量向着最终反应阶段依次小。 (4)反应体系的温度应在-5℃以下。 (5)反应体系中的停留时间应在4小时内。
    • 7. 发明授权
    • Cyan dye-donor element used in thermal transfer and thermal transfer
sheet using it
    • CYAN DYE-DONOR元件用于热转印和热转印片使用它
    • US5077264A
    • 1991-12-31
    • US451318
    • 1989-12-15
    • Yoshiaki HayashiTaira FujitaTakehiro KusumotoTakeshi Hioki
    • Yoshiaki HayashiTaira FujitaTakehiro KusumotoTakeshi Hioki
    • B41M5/035B41M5/26B41M5/385B41M5/39
    • B41M5/3858B41M5/3852B41M5/3854B41M5/39Y10S428/913Y10S428/914
    • A cyan dye-donor element which gives good printed images to a thermal-transfer sheet and a thermal-transfer sheet comprising a substrate sheet and a layer containing said cyan dye-donor and being laid on one side of the substrate sheet are provided. The cyan dye-donor element comprises cyan dyes dispersed or dissolved in a polymeric binder wherein said cyan dyes comprise: ##STR1## wherein R.sub.1 and R.sub.2 each represents a hydrogen atom or a C.sub.1 -C.sub.6 alkyl group; at least one dye represented by the following formula (II): ##STR2## wherein R.sub.3 and R.sub.4 each represents a hydrogen atom or a C.sub.1 -C.sub.6 alkyl group which may be substituted, and R.sub.5 represents a hydrogen atom or a C.sub.1 -C.sub.6 alkyl group; and at least one dye selected from the group consisting of dyes represented by the following formula (III): ##STR3## wherein R.sub.6 and R.sub.7 each represents a hydrogen atom or a C.sub.1 -C.sub.6 alkyl group which may be substituted, R.sub.8 represents a hydrogen atom, a C.sub.1 -C.sub.6 alkyl group which may be substituted, an alkoxy group which may be substituted or an acylamino group which may be substituted and R.sub.9 represents a hydrogen atom, a C.sub.1 -C.sub.6 alkyl group which may be substituted or an aryl group which may be substituted, dyes represented by the following formula (IV): ##STR4## wherein R.sub.10 represents a hydrogen atom, a C.sub.1 -C.sub.6 alkyl group which may be substituted, an aryl group which may be substituted or a cyclohexyl group, R.sub.11 -R.sub.13 each represents a hydrogen atom or a C.sub.1 -C.sub.6 alkyl group which may be substituted, and R.sub.14 represents a hydrogen atom or a C.sub.1 -C.sub.6 alkyl group which may be substituted or an alkoxy group which may be substituted, and dyes represented by the following formula (V): ##STR5## wherein R.sub.15 and R.sub.16 each represents a hydrogen atom or a C.sub.1 -C.sub.6 alkyl group which may be substituted.
    • 8. 发明授权
    • Method of producing photoresist
    • 光致抗蚀剂的制造方法
    • US07264912B2
    • 2007-09-04
    • US10117248
    • 2002-04-08
    • Takeshi HiokiKota TokuharaYukio Hanamoto
    • Takeshi HiokiKota TokuharaYukio Hanamoto
    • G03C1/73G03F7/00
    • G03F7/0045G03F7/022G03F7/0392
    • Provided are a method of producing a photoresist comprising a process of filtrating a raw resist solution containing resist constituent components and a resist solvent dissolving them, using a filter made of at least one resin selected from fluorine-based resins and polyolefins, wherein this filter has been used for filtration of the same or different kind of other raw resist solution and has been washed with a solvent containing the resist solvent toward the reverse direction to the filtration direction, and a method of sequentially producing two or more photoresists using the same production apparatus, wherein this production apparatus is washed with the resist solvent, a solvent other than this resist solvent capable of dissolving or decomposing the resist constituent components, and the resist solvent, in this order, after production of the photoresist and before production of the subsequent photoresist.
    • 提供一种光致抗蚀剂的制造方法,其特征在于,使用由选自氟系树脂和聚烯烃中的至少一种树脂制成的过滤器,过滤由含有抗蚀剂构成成分的原始抗蚀剂溶液和溶解了抗蚀剂溶剂的抗蚀剂溶剂的方法, 用于过滤相同或不同种类的其他原始抗蚀剂溶液,并且已经用含有抗蚀剂溶剂的溶剂朝向与过滤方向相反的方向进行过滤,以及使用相同的生产设备依次生产两个或更多个光致抗蚀剂的方法 其中,该制造装置在制造光致抗蚀剂之后并且在制造后续的光致抗蚀剂之前,依次用抗蚀剂溶剂,除了能够溶解或分解抗蚀剂构成成分的抗蚀剂溶剂之外的溶剂和抗蚀剂溶剂洗涤 。