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1. 发明授权

US5463149A 1-halo-cis-3-tetradecenes and processes for the preparation of cis-olefin compounds by using same 失效
标题翻译： 1-卤代 - 顺式-3-十四碳烯和通过使用它们制备顺式烯烃化合物的方法
公开(公告)号：US5463149A
公开(公告)日：1995-10-31
申请号：US274139
申请日：1994-07-12
申请人： Takehiko Fukumoto , Daisuke Iwai , Shigeo Okano , Hiroshi Suzuki , Mitsuyoshi Oshima
发明人： Takehiko Fukumoto , Daisuke Iwai , Shigeo Okano , Hiroshi Suzuki , Mitsuyoshi Oshima
IPC分类号： A01N27/00 , C07C1/32 , C07C11/02 , C07C17/16 , C07C21/04 , C07C21/14 , C07C21/17 , C07F1/02 , C07F3/02 , C07C19/08
CPC分类号： C07C11/02 , C07C17/16 , C07C21/04 , C07C21/14 , C07C21/17
摘要： Disclosed are compounds suitable for use as raw materials which enable cis-olefin compounds useful as physiologically active substances such as the sex pheromones of various insects, or as intermediates for the synthesis thereof to be prepared on an industrial scale at a reasonable cost, and processes for the preparation of cis-olefin compounds by using the same. For this purpose, novel compounds (i.e., 1-halo-cis-3-tetradecenes) of the general formula (I)CH.sub.3 (CH.sub.2).sub.9 CH.dbd.CH(CH.sub.2).sub.2 X (I)wherein X is a halogen atom, are used as raw materials for the preparation of cis-olefin compounds.
摘要翻译：公开了适合用作原料的化合物，其使得可用作诸如各种昆虫的性信息素的生理活性物质的顺式烯烃化合物或其合成成本的工业规模的合成中间体，以及方法用于通过使用它们制备顺式烯烃化合物。为此，将通式（I）CH（CH 2）9 CH = CH（CH 2）2 X（I）的新化合物（即1-卤代 - 顺式-3-十四碳烯）其中X为卤素原子用作用于制备顺式烯烃化合物的原料。

2. 发明授权

US5714649A 1-Halo-cis-3-tetradecenes and processes for the preparation of cis-Olefin compounds by using same 失效
标题翻译： 1-顺 - 顺-3-十四碳烯和通过使用它们制备顺式烯烃化合物的方法
公开(公告)号：US5714649A
公开(公告)日：1998-02-03
申请号：US575333
申请日：1995-12-20
申请人： Takehiko Fukumoto , Daisuke Iwai , Shigeo Okano , Hiroshi Suzuki , Mitsuyoshi Oshima
发明人： Takehiko Fukumoto , Daisuke Iwai , Shigeo Okano , Hiroshi Suzuki , Mitsuyoshi Oshima
IPC分类号： A01N27/00 , C07C1/32 , C07C11/02 , C07C17/16 , C07C21/04 , C07C21/14 , C07C21/17 , C07F1/02 , C07F3/02 , C07C19/08
CPC分类号： C07C11/02 , C07C17/16 , C07C21/04 , C07C21/14 , C07C21/17
摘要： Disclosed are compounds suitable for use as raw materials which enable cis-olefin compounds useful as physiologically active substances such as the sex pheromones of various insects, or as intermediates for the synthesis thereof to be prepared on an industrial scale at a reasonable cost, and processes for the preparation of cis-olefin compounds by using the same. For this purpose, novel compounds (i.e., 1-halo-cis-3-tetradecenes) of the general formula (I) CH.sub.3 (CH.sub.2).sub.9 CH.dbd.CH(CH.sub.2).sub.2 X (I) wherein X is a halogen atom, are used as raw materials for the preparation of cis-olefin compounds.
摘要翻译：公开了适合用作原料的化合物，其使得可用作诸如各种昆虫的性信息素的生理活性物质的顺式烯烃化合物或其合成成本的工业规模的合成中间体，以及方法用于通过使用它们制备顺式烯烃化合物。为此，将通式（I）CH（CH 2）9 CH = CH（CH 2）2 X（I）的新化合物（即1-卤代 - 顺式-3-十四碳烯）其中X为卤素原子用作用于制备顺式烯烃化合物的原料。

3. 发明授权

US5162596A Z-12-heptadecen-1-yne 失效
标题翻译： Z-12-HEPTADECEN-1-YNE
公开(公告)号：US5162596A
公开(公告)日：1992-11-10
申请号：US837025
申请日：1992-02-14
申请人： Takehiko Fukumoto , Akira Yamamoto , Mitsuyoshi Oshima
发明人： Takehiko Fukumoto , Akira Yamamoto , Mitsuyoshi Oshima
IPC分类号： C07C11/28
CPC分类号： C07C11/28
摘要： Disclosed is a novel ene-yne compound Z-12-heptadecen-1-yne expressed by the structural formula CH.sub.3 (CH.sub.2).sub.3 CH.sup.(Z) =CH(CH.sub.2).sub.9 C=CH, which is useful as an intermediate in the synthetic preparation of several diene compounds having activity as a sex pheromone of the insects belonging to the lepidopteran order, such as E,Z-2,13-octadecadienyl acetate and E,Z-2,13-octadecadienal, having two double bonds at the 2- and 13-positions. The inventive compound can be synthesized by the reaction of 1-bromo-Z-10-pentadecene with sodium acetylide dispersed in an organic solvent in the presence of liquid ammonia.
摘要翻译：公开了由结构式CH 3（CH 2）3 CH（Z）= CH（CH 2）9 C = CH表示的新型烯类化合物Z-12-十七碳烯-1-炔，其可用作合成制剂中的中间体具有属于鳞翅目类昆虫的性信息素的几种二烯化合物，例如E，Z-2,13-十八碳二烯酸乙酯和E，Z-2,13-十八碳二烯醛，在2-和 13个职位。本发明化合物可以通过在液氨存在下分散在有机溶剂中的1-溴代-Z-十五碳烯与乙炔化钠的反应来合成。

4. 发明授权

US5880318A Process for the preparation of .alpha.-bromo, .omega.-chloroalkanes 失效
标题翻译：制备α-溴，ω-氯代烷烃的方法
公开(公告)号：US5880318A
公开(公告)日：1999-03-09
申请号：US906816
申请日：1997-08-06
申请人： Takehiko Fukumoto , Hiroshi Suzuki , Kinya Ogawa , Kazushi Hirokawa
发明人： Takehiko Fukumoto , Hiroshi Suzuki , Kinya Ogawa , Kazushi Hirokawa
IPC分类号： C07C17/20 , C07C19/075 , C07C19/00
CPC分类号： C07C17/202
摘要： Described is a process for easily preparing an .alpha.-bromo,.omega.-chloroalkane which is high in purity represented by the formula: Br(CH.sub.2).sub.n Cl in which n stands for an integer of 4 to 12. The process comprises reacting in an organic solvent an .alpha.,.omega.-dichloroalkane with an .alpha..omega.-dibromoalkane. As the organic solvent, an aprotic nitrogen-containing or sulfur-containing organic solvent having a dielectric constant at 20.degree. C. of 20 or larger, for example, N,N-dimethylformamide, N,N-dimethylacetamide or N,N-dimethylimidazolidinone is preferred.
摘要翻译：描述了一种易于制备由式Br（CH 2）n Cl表示的纯度高的α-溴，ω-氯烷烃的方法，其中n表示4至12的整数。该方法包括在有机溶剂具有αω-二溴烷烃的α，ω-二氯烷烃。作为有机溶剂，在20℃下介电常数为20以上的非质子性含氮或含硫有机溶剂，例如N，N-二甲基甲酰胺，N，N-二甲基乙酰胺或N，N-二甲基咪唑烷酮是优选的。

5. 发明授权

US5532421A Method for the isomerization of cis-alkenyl compounds 失效
标题翻译：顺式 - 烯基化合物的异构化方法
公开(公告)号：US5532421A
公开(公告)日：1996-07-02
申请号：US275753
申请日：1994-07-19
申请人： Takanobu Terauchi , Toyohisa Sakurada , Takehiko Fukumoto , Hiroshi Suzuki
发明人： Takanobu Terauchi , Toyohisa Sakurada , Takehiko Fukumoto , Hiroshi Suzuki
IPC分类号： B01J27/24 , C07B35/08 , C07B61/00 , C07C5/22 , C07C11/02 , C07C11/107 , C07C17/358 , C07C21/04 , C07C29/56 , C07C33/025 , C07C51/353 , C07C51/62 , C07C57/12 , C07C57/66 , C07C67/293 , C07C67/333 , C07C69/007 , C07C69/145 , C07C69/533 , C07C69/58 , C07C5/27
CPC分类号： C07C5/2206 , C07B35/08 , C07C29/56 , C07C33/025 , C07C51/353 , C07C51/62 , C07C67/333 , C07B2200/09 , C07C2527/25
摘要： An object of the present invention is to provide a method for the preparation of geometrical isomers which are important as constituents of synthetic pheromones, synthetic perfumes, terpenes and the like (i.e., a method for the isomerization of cis-alkenyl compounds to their trans-isomers). In this method, the above-described object is accomplished by reacting a cis-alkenyl compound in the presence of nitric acid used as the sole catalyst.
摘要翻译：本发明的目的是提供一种制备作为合成信息素，合成香料，萜烯等的成分重要的几何异构体的方法（即将顺式 - 链烯基化合物异构化成其反式 - 异构体）。在该方法中，上述目的是通过使用作为唯一催化剂的硝酸存在下的顺式链烯基化合物进行。

6. 发明授权

US09545102B2 Sustained release pheromone preparation targeting insect pest having carboxylic acid as pheromone substance 有权
标题翻译：以具有羧酸为信息素物质的昆虫害虫的缓释信息素制剂
公开(公告)号：US09545102B2
公开(公告)日：2017-01-17
申请号：US13325838
申请日：2011-12-14
申请人： Tatsuya Fujii , Tatsuya Hojo , Naoki Ishibashi , Ryuichi Saguchi , Takehiko Fukumoto
发明人： Tatsuya Fujii , Tatsuya Hojo , Naoki Ishibashi , Ryuichi Saguchi , Takehiko Fukumoto
IPC分类号： A01N25/10 , A01N37/02 , A01N25/18
CPC分类号： A01N25/18 , A01N25/10 , A01N25/22 , A01N37/02 , A01N37/06
摘要： Targeting an insect pest having a carboxylic acid compound as a pheromone substance, provided is a sustained release pheromone preparation enabling a high amount of pheromone to be released during the control period. More specifically, provided is a sustained release pheromone preparation, comprising: a carboxylic acid compound to be released, and an ethylene-vinyl acetate copolymer membrane through which the carboxylic acid compound can permeate, wherein the preparation is targeted for an insect pest having the carboxylic acid compound as a pheromone substance.
摘要翻译：提供了具有羧酸化合物作为信息素物质的害虫，其是提供在控制期间能够释放大量信息素的缓释信息素制剂。更具体地，提供了一种缓释信息素制剂，其包含：待释放的羧酸化合物和羧酸化合物可以渗透的乙烯 - 乙酸乙烯酯共聚物膜，其中所述制剂靶向具有羧酸的害虫酸化合物作为信息素物质。

7. 发明申请

US20100069664A1 METHOD FOR PREPARING (E3,Z5)-3,5-ALKADIENYL ACETATE 有权
标题翻译：制备（E3，Z5）-3,5-亚氨基乙酸酯的方法
公开(公告)号：US20100069664A1
公开(公告)日：2010-03-18
申请号：US12620981
申请日：2009-11-18
申请人： Miyoshi Yamashita , Takehiko Fukumoto
发明人： Miyoshi Yamashita , Takehiko Fukumoto
IPC分类号： C07C43/30 , C07C41/48 , C07C67/24
CPC分类号： C07C41/48 , C07C29/10 , C07C41/50 , C07C67/08 , C07C69/007 , C07C69/145 , C07C33/02 , C07C43/30
摘要： Provided is a method for preparing (E3,Z5)-3,5-alkadienyl acetate and (E3,Z5)-3,5-dodecadienyl acetate which is a sex pheromone of Brazilian apple leafminer. Specifically, provided is a method for preparing (E3,Z5)-3,5-alkadienyl acetate, comprising steps of hydrolyzing 5,5-diethoxy-(Z3)-3-pentenyl methoxymethyl ether in the presence of an acid to obtain 4-formyl-(E3)-butenyl methoxymethyl ether; reacting the 4-formyl-(E3)-butenyl methoxymethyl ether with alkylidene triphenylphosphorane in accordance with the Wittig reaction to obtain (E3,Z5)-3,5-alkadienyl methoxymethyl ether; and obtaining (E3,Z5)-3,5-alkadienyl acetate using the (E3,Z5)-3,5-alkadienyl methoxymethyl ether as a starting substance.
摘要翻译：提供一种制备（E3，Z5）-3,5-链二烯酸乙酸酯和（E3，Z5）-3,5-十二烷基乙酸酯的方法，其是巴西苹果叶片的性信息素。具体地说，提供了制备（E3，Z5）-3,5-链二烯基乙酸酯的方法，包括在酸存在下水解5,5-二乙氧基 - （Z 3）-3-戊烯基甲基甲基醚的步骤，得到4- 甲酰基 - （E3） - 丁烯基甲氧基甲基醚; 根据Wittig反应使4-甲酰基 - （E3） - 丁烯基甲氧基甲基醚与亚烷基三苯基正膦反应，得到（E3，Z5）-3,5-二甲氧基甲基醚; 并使用（E3，Z5）-3,5-链二烯基甲氧基甲基醚作为起始物质获得（E3，Z5）-3,5-链二烯酸乙酯。

8. 发明申请

US20050209344A1 Behavior-disrupting agent and behavior-disrupting method of Argentine ant 有权
标题翻译：阿根廷蚂蚁的行为破坏剂和行为破坏方法
公开(公告)号：US20050209344A1
公开(公告)日：2005-09-22
申请号：US11063900
申请日：2005-02-23
申请人： Sadahiro Tatsuki , Mamoru Terayama , Yasutoshi Tanaka , Takehiko Fukumoto
发明人： Sadahiro Tatsuki , Mamoru Terayama , Yasutoshi Tanaka , Takehiko Fukumoto
IPC分类号： A01N49/00 , A01N35/00 , A01N35/02
CPC分类号： A01N35/02
摘要： Provided are a behavior-disrupting agent of Argentine ants for controlling them or suppressing their reproduction is a safer and more effective manner, and the behavior-disrupting method of them. More specifically, a behavior-disrupting agent of Argentine ants comprising Z-9-hexadecenal, and a behavior-disrupting method of Argentine ants comprising a step of using the behavior-disrupting agent are provided based on the finding that the behavior of Argentine ants is disrupted by emission of Z-9-hexadecenal, which is a trail pheromone, into the atmosphere.
摘要翻译：阿根廷蚂蚁的行为破坏剂是控制它们或抑制其繁殖是一种更安全和更有效的方式，以及它们的行为破坏方法。更具体地，基于以下发现提供了包含Z-9-十六烯醛的阿根廷蚂蚁的行为破坏剂和包含使用行为破坏剂的步骤的阿根廷蚂蚁的行为破坏性方法，其发现：阿根廷蚂蚁的行为为通过尾气信息素的Z-9-十六烯醛的排放而破坏了大气。

9. 发明授权

US06562331B1 Mating disruption methods for the control of insect pests 失效
标题翻译：用于控制害虫的交配破坏方法
公开(公告)号：US06562331B1
公开(公告)日：2003-05-13
申请号：US09635905
申请日：2000-08-10
申请人： Tatsuya Ito , Takehiko Fukumoto , Kinya Ogawa , Fumiaki Mochizuki
发明人： Tatsuya Ito , Takehiko Fukumoto , Kinya Ogawa , Fumiaki Mochizuki
IPC分类号： A01N2500
CPC分类号： A01N35/02 , A01N25/00 , A01N25/18 , A01N25/22 , A01N37/02 , A01N2300/00
摘要： A mating disruption method for the control of insect pests comprises releasing a sex pheromone in a field wherein an adsorption of the sex pheromone to a soil in the field is decreased.
摘要翻译：用于控制害虫的交配破坏方法包括在场中的性信息素吸附到土壤中的场中释放性信息素。

10. 发明授权

US08900611B2 Sustained releaser comprising sex pheromone substances 有权
标题翻译：持续释放者包括性信息素物质
公开(公告)号：US08900611B2
公开(公告)日：2014-12-02
申请号：US11226588
申请日：2005-09-14
申请人： Tatsuya Hojo , Kinya Ogawa , Noboru Aiba , Takehiko Fukumoto
发明人： Tatsuya Hojo , Kinya Ogawa , Noboru Aiba , Takehiko Fukumoto
IPC分类号： A01N25/00 , A01N37/02 , A01N35/00 , A01N35/02 , A01N25/18 , A01N31/02
CPC分类号： A01N25/18 , A01N37/02 , A01N35/02 , A01N31/02 , A01N2300/00
摘要： Provided are a sustained releaser of sex pheromone substances and a method for controlling insect pest by using the releaser, each enabling to control the simultaneous release of a mixture of sex pheromone substances having different chemical structures of one insect pest or a mixture of sex pheromone substances of insect pests, and each enabling to release the sex pheromone substances at a fixed rate or greater during the infestation period or periods of the respective insect pest or pests. More specifically, provided is a sustained releaser of sex pheromone substances comprising one or more first sex pheromone substances selected from linear aliphatic aldehyde having 10 to 18 carbon atoms, one or more second sex pheromone substances selected from aldehyde-free aliphatic derivatives having 7 to 20 carbon atoms, and first and second chambers each made of polymer material, wherein all of the first sex pheromone substances or all of the first sex pheromone substances and some of the second sex pheromone substances are enclosed in the first chamber and the remainder of the sex pheromone substances is enclosed in the second chamber.
摘要翻译：提供性信息素物质的持续释放者和通过使用释放剂来控制害虫的方法，每种能够控制同时释放具有不同化学结构的一种害虫或性信息素物质混合物的性信息素物质的混合物的虫害，并且每个能够在相应的害虫或害虫的感染期或期间以固定的速率或更高的速率释放性信息素物质。更具体地，提供了包含一种或多种选自具有10至18个碳原子的直链脂族醛的一种或多种第一性信息素物质的性信息素物质的持续释放剂，一种或多种选自不含醛的脂族衍生物的第二性别信息素物质，其具有7至20 碳原子，以及由聚合物材料制成的第一和第二室，其中所有第一性别信息素物质或所有第一性信息素物质和一些第二性信息素物质被封闭在第一室中，其余的性别信息素物质被封闭在第二个室中。

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