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1. 发明授权

US06503988B1 Polytetrafluoroethylene fine powders and their use 失效
标题翻译：聚四氟乙烯细粉及其用途
公开(公告)号：US06503988B1
公开(公告)日：2003-01-07
申请号：US09051805
申请日：1998-04-23
申请人： Takahiro Kitahara , Kazutaka Hosokawa , Tetsuo Shimizu
发明人： Takahiro Kitahara , Kazutaka Hosokawa , Tetsuo Shimizu
IPC分类号： C08F11418
CPC分类号： C08J3/16 , C08F14/26 , C08J2327/12 , C08L27/18 , C08L101/00 , C09K3/22 , C09K21/14 , C08F2/16 , C08L2666/04
摘要： A polytetrafluoroethylene fine powder excellent in powder flowability which comprises fine particles (the primary particle) having a mean particle diameter of 0.05 to 1 &mgr;m, an apparent density of 0.52 to 0.70 g/ml, a standard specific gravity (SSG) of 2.14 to 2.23, and a secondary mean particle diameter of 100 to 1000 &mgr;m, antidripping agent using the above polytetrafluoroethylene fine powder, flame resistive resin composition containing this powder, and composition for inhibiting dust characteristics containing this powder.
摘要翻译：粉末流动性优异的聚四氟乙烯细粉末，其包含平均粒径为0.05〜1μm的微粒（一次粒子），表观密度为0.52〜0.70g / ml，标准比重（SSG）为2.14〜2.23 ，二次平均粒径为100〜1000μmol，使用上述聚四氟乙烯细粉末的防毒剂，含有该粉末的阻燃树脂组合物和含有该粉末的粉尘特性抑制组合物。

2. 发明授权

US5324785A Polytetrafluoroethylene fine particles and powder 失效
标题翻译：聚四氟乙烯细颗粒和粉末
公开(公告)号：US5324785A
公开(公告)日：1994-06-28
申请号：US133787
申请日：1993-10-08
申请人： Yoshihisa Noda , Kazutaka Hosokawa , Toshio Mizuno , Kiyohiko Ihara , Tetsuo Shimizu
发明人： Yoshihisa Noda , Kazutaka Hosokawa , Toshio Mizuno , Kiyohiko Ihara , Tetsuo Shimizu
IPC分类号： C08J3/02 , C08F2/22 , C08F14/26 , C08F259/08 , C08J3/16 , C08L27/06 , C08L27/18
CPC分类号： C08F259/08 , Y10S525/902
摘要： Colloidal polytetrafluoroethylene fine particles having an average particle size of 0.05 to 1.0 .mu.m and each comprising a core made of polytetrafluoroethylene which has a high molecular weight and can be fibrilled and a shell surrounding the core and made of a low molecular weight polytetrafluoroethylene which is not fibrilled, which has good dispersibility in water or an organic solvent and easily provides an organosol by a phase transfer method.
摘要翻译：平均粒径为0.05〜1.0μm的胶体型聚四氟乙烯微粒，各自包含由聚四氟乙烯制成的芯，该聚四氟乙烯具有高分子量并且可以被纤维化，壳体围绕芯并且由低分子量聚四氟乙烯制成，不是纤维状，其在水或有机溶剂中具有良好的分散性，并且通过相转移法容易地提供有机溶胶。

3. 发明授权

US5284708A Modified polytetrafluoroethylene fine powder and process for preparing the same 失效
标题翻译：改性聚四氟乙烯细粉及其制备方法
公开(公告)号：US5284708A
公开(公告)日：1994-02-08
申请号：US957895
申请日：1992-10-08
申请人： Tetsuo Shimizu , Kazutaka Hosokawa , Masuo Kokumai , Makoto Ono
发明人： Tetsuo Shimizu , Kazutaka Hosokawa , Masuo Kokumai , Makoto Ono
IPC分类号： C08F214/26 , B32B5/16 , C08F116/12
CPC分类号： C08F214/262 , Y10T428/2982
摘要： Modified PTFE fine powder which comprises colloidal particles of a copolymer comprising repeating units derived from tetrafluoroethylene and 0.02 to 0.3 % by weight, preferably 0.03 to 0.2% by weight of repeating units derived from at least one fluoroalkyl vinyl ether selected from compounds of the formula:X(CF.sub.2).sub.n OCF.dbd.CF.sub.2 (I)wherein X is a hydrogen, fluorine or chlorine atom and n is an integer of 1 to 6, andC.sub.3 F.sub.7 (OCF.sub.2 CF.sub.2 CF.sub.2).sub.m [OCF(CF.sub.3)CF.sub.2 ].sub.1 OCF.dbd.CF.sub.2 (II)wherein m and 1 are each an integer of 0 to 4 provided that at least one of them is not zero, which has a number average particle size of 0.05 to 0.6 .mu.m, wherein the copolymer has a specific melt viscosity of from 6.times.10.sup.10 to 30.times.10.sup.10 poise, preferably from 8.0.times.10.sup.10 to 25.times.10.sup.10 poise at 380.degree. C. and a standard specific gravity (SSG, hereinafter defined) of from 2.135 to 2.175, preferably from 2.140 to 2.160 and a paste extruded article of the polymer has a green elongation of at least 400% is provided.
摘要翻译：改性PTFE细粉末，其包含含有衍生自四氟乙烯的重复单元和0.02至0.3重量％，优选0.03至0.2重量％的衍生自至少一种氟代烷基乙烯基醚的重复单元的共聚物的胶体颗粒，所述氟代烷基乙烯基醚选自下式化合物： X（CF 2）n OCF = CF 2（I）其中X为氢，氟或氯原子，n为1至6的整数，C 3 F 7（OCF 2 CF 2 CF 2）m（OCF（CF 3）CF 2） m和1各自为0〜4的整数，条件是它们中的至少一个不为零，其数均粒径为0.05〜0.6（my）m，其中，共聚物的比熔融粘度为6 * 在380℃下优选为1010至30 * 1010泊，优选为8.0 * 1010至25 * 1010泊，标准比重（SSG，以下定义）为2.135至2.175，优选为2.140至2.160，提供聚合物具有至少400％的绿色伸长率。

4. 发明授权

US5118788A Process for preparing polytetrafluoroethylene powder 失效
标题翻译：制备聚四氟乙烯粉的方法
公开(公告)号：US5118788A
公开(公告)日：1992-06-02
申请号：US696194
申请日：1991-05-06
申请人： Kazutaka Hosokawa , Tetsuo Shimizu , Kazuo Ishiwari , Noriyasu Yamane
发明人： Kazutaka Hosokawa , Tetsuo Shimizu , Kazuo Ishiwari , Noriyasu Yamane
IPC分类号： C08J3/12
CPC分类号： C08J3/12 , C08J2327/18
摘要： Polytetrafluoroethylene powder having an average particle size of 1 to 30 .mu.m and a specific surface area of 2 to 6 m.sup.2 /g is prepared by heating unsintered polytetrafluoroethylene powder having a melting point of 313.degree. to 330.degree. C. at a temperature in a range from a temperature 70.degree. C. lower than the melting point to a temperature lower than the melting point and comminuting the heated powder.

5. 发明授权

US06531557B1 Modified polytetrafluoroethylene fine powder and method for the production of the same 有权
标题翻译：改性聚四氟乙烯细粉及其制备方法
公开(公告)号：US06531557B1
公开(公告)日：2003-03-11
申请号：US09242272
申请日：1999-03-12
申请人： Kazutaka Hosokawa , Yoshinori Nanba , Takahisa Aoyama , Tetsuo Shimizu
发明人： Kazutaka Hosokawa , Yoshinori Nanba , Takahisa Aoyama , Tetsuo Shimizu
IPC分类号： C08F21426
CPC分类号： C08F214/262
摘要： A modified polytetrafluoroethylene fine powder containing agglomerates of colloidal particles with an average particle size of from 0.05 to 0.5 &mgr;m which comprise a copolymer of tetrafluoroethylene and an olefin-monomer represented by X(CF2)nOCF═CF2 in which X is a hydrogen atom, a fluorine atom or a chlorine atom, and n is an integer of 1 to 6, and/or C3F7(OCF2CF2CF2)m[OCF(CF3)CF2]pOCF═CF2 in which m and p are independently an integer of 0 to 4, provided that the sum of m and p is not 0 (zero), a content of the olefin monomer being from 0.02 to 0.3 wt. %, wherein the copolymer has a molecular weight distribution Mw/Mn of from 1.5 to 4.5 and a standard specific gravity of from 2.135 to 2.175. This modified polytetrafluoroethylene has good paste extrudability, and provides molded articles having good mechanical properties, in particular, pressure resistance.
摘要翻译：一种改性聚四氟乙烯细粉末，其含有平均粒径为0.05〜0.5μm的胶体粒子的附聚物，其包含由X（CF 2）n OCF = CF 2（其中X为氢原子）表示的四氟乙烯与烯烃单体的共聚物，氟原子或氯原子，n为1〜6的整数，和/或C 3 F 7（OCF 2 CF 2 CF 2）m [OCF（CF 3）CF 2] p OCF = CF 2，其中m和p分别为0〜4的整数， m和p的和不为0（零），烯烃单体的含量为0.02-0.3重量％。％，其中共聚物的分子量分布Mw / Mn为1.5〜4.5，标准比重为2.135〜2.175。该改性聚四氟乙烯具有良好的糊料挤出性，并提供具有良好机械性能，特别是耐压性的模制品。

6. 发明授权

US5143783A Porous film of polytetrafluoroethylene and preparation thereof 失效
标题翻译：聚四氟乙烯多孔薄膜及其制备
公开(公告)号：US5143783A
公开(公告)日：1992-09-01
申请号：US435170
申请日：1989-11-13
申请人： Tetsuo Shimizu , Kazutaka Hosokawa
发明人： Tetsuo Shimizu , Kazutaka Hosokawa
IPC分类号： C08J9/24 , C08J9/28
CPC分类号： C08J9/24 , C08J9/28 , C08J2327/18 , Y10T428/254 , Y10T428/31544
摘要： A polytetrafluoroethylene porous film obtainable by applying an aqueous dispersion of emulsion polymerized polytetrafluoroethylene particles having an average minor particle size of 1 to 500 nm and an average aspect ratio of at least 10 on a substrate, drying the applied dispersion and optionally sintering the dried polytetrafluoroethylene particles on the substrate to obtain the polytetrafluoroethylene porous film, which has a uniform thin thickness.

7. 发明授权

US5176958A Modified polytetrafluoroethylene fine powder and process for preparing the same 失效
标题翻译：改性聚四氟乙烯细粉及其制备方法
公开(公告)号：US5176958A
公开(公告)日：1993-01-05
申请号：US715029
申请日：1991-06-13
申请人： Tetsuo Shimizu , Kazutaka Hosokawa , Masuo Kokumai , Makoto Ono
发明人： Tetsuo Shimizu , Kazutaka Hosokawa , Masuo Kokumai , Makoto Ono
IPC分类号： C08F214/26
CPC分类号： C08F214/262 , Y10T428/2982
摘要： Modified PTFE fine powder which comprises colloidal particles of a copolymer comprising repeating units derived from tetrafluoroethylene and 0.02 to 0.3% by weight, preferably 0.03 to 0.2% by weight of repeating units derived from at least one fluoroalkyl vinyl ether selected from compounds of the formula:X(CF.sub.2).sub.n OCF.dbd.CF.sub.2 (I)wherein X is a hydrogen, fluorine or chlorine atom and n is an integer of 1 to 6, andC.sub.3 F.sub.7 (OCF.sub.2 CF.sub.2 CF.sub.2).sub.m [OCF(CF.sub.3)CF.sub.2 ].sub.l OCF.dbd.CF.sub.2 (II)wherein m and l are each an integer of 0 to 4 provided that at least one of them is not zero, which has a number average particle size of 0.05 to 0.6 .mu.m, wherein the copolymer has a specific melt viscosity of from 6.times.10.sup.10 to 30.times.10.sup.10 poise, preferably from 8.0.times.10.sup.10 to 25.times.10.sup.10 poise at 380.degree. C. and a standard specific gravity (SSG, hereinafter defined) of from 2.135 to 2.175, preferably from 2.140 to 2.160 and a paste extruded article of the polymer has a green elongation of at least 400% is provided.
摘要翻译：改性PTFE细粉末，其包含含有衍生自四氟乙烯的重复单元和0.02至0.3重量％，优选0.03至0.2重量％的衍生自至少一种氟代烷基乙烯基醚的重复单元的共聚物的胶体颗粒，所述氟代烷基乙烯基醚选自下式化合物： X（CF 2）n OCF = CF 2（I）其中X为氢，氟或氯原子，n为1〜6的整数，C 3 F 7（OCF 2 CF 2 CF 2）m [OCF（CF 3）CF 2] m和l各自为0〜4的整数，条件是它们中的至少一个不为零，其数均粒径为0.05至0.6μm，其中共聚物的比熔融粘度为6×10 10至30×10 10泊，优选在380℃下为8.0×10 10至25×10 10泊，标准比重（SSG，以下定义）为2.135至2.175，优选为2.140至2.160，并且聚合物的糊状挤出制品具有至少的绿色伸长率提供400％。

8. 发明授权

US4840998A Modified polytetrafluoroethylene fine powder and production of the same 失效
标题翻译：改性聚四氟乙烯细粉与生产相同
公开(公告)号：US4840998A
公开(公告)日：1989-06-20
申请号：US89766
申请日：1987-08-27
申请人： Tetsuo Shimizu , Kazutaka Hosokawa
发明人： Tetsuo Shimizu , Kazutaka Hosokawa
IPC分类号： C08J3/12 , C08F2/00 , C08F2/18 , C08F214/26
CPC分类号： C08F214/262 , Y10S525/902
摘要： Modified PTFE fine powder which comprises primary particles having an average particle size of 0.1 to 0.6 .mu.m and contains 0.01 to 0.15% by weight, based on the total weight of the particles, of at least one olefinically unsaturated compound selected from the group consisting of a fluoroalkyl vinyl ether of the formula:X(CF.sub.2).sub.n OCF.dbd.CF.sub.2 (I)wherein X is a hydrogen atom, a fluorine atom or a chlorine atom and n is an integer of 1 to 6, and a fluoroalkyl vinyl ether of the formula:C.sub.3 F.sub.7 (OCF.sub.2 CF.sub.2 CF.sub.2).sub.m [OCF(CF.sub.3)CF.sub.2 ].sub.l OCF.dbd.CF.sub.2 (II)wherein m is an integer of 0 to 2 and l is an integer of 0 to 2 mainly in core parts of the particles and 0.04 to 0.25% by weight, based on the total weight of the particles, of chlorotrifluoroethylene in shell parts, which has good paste extrudability and heat stability.
摘要翻译：改性PTFE细粉末，其包含平均粒度为0.1〜0.6μm的一次粒子，以所述粒子的总重量计含有0.01〜0.15重量％的至少一种选自以下的烯属不饱和化合物：具有下式的氟烷基乙烯基醚：X（CF 2）n OCF = CF 2（I）其中X是氢原子，氟原子或氯原子，n是1至6的整数，并且式：C 3 F 7（OCF 2 CF 2 CF 2）m [OCF（CF 3）CF 2] l OCF = CF 2（II）其中m为0〜2的整数，l为0〜2的整数，主要为颗粒的核心部分，0.04〜0.25％重量，基于颗粒的总重量，三氯氟乙烯在壳部分中，其具有良好的浆料挤出性和热稳定性。

9. 发明授权

US06680124B1 Fluorochemical adhesive material and laminate made with the same 有权
标题翻译：氟化合物粘合剂材料和由其制成的层压材料
公开(公告)号：US06680124B1
公开(公告)日：2004-01-20
申请号：US09623571
申请日：2000-11-06
申请人： Takayuki Araki , Takahiro Kitahara , Shigehito Sagisaka , Taketo Kato , Takeshi Inaba , Kazuo Ishiwari , Tetsuo Shimizu , Hidenori Ozaki , Tatsuya Higuchi
发明人： Takayuki Araki , Takahiro Kitahara , Shigehito Sagisaka , Taketo Kato , Takeshi Inaba , Kazuo Ishiwari , Tetsuo Shimizu , Hidenori Ozaki , Tatsuya Higuchi
IPC分类号： B32B2728
CPC分类号： B32B27/08 , B32B1/02 , B32B1/08 , B32B27/28 , B32B27/304 , B32B27/306 , B32B27/308 , B32B27/32 , B32B27/322 , B32B27/34 , B32B27/36 , B32B27/365 , B32B2323/04 , B32B2327/06 , B32B2327/18 , B32B2329/04 , B32B2367/00 , B32B2369/00 , B32B2377/00 , B32B2439/00 , B32B2439/60 , B32B2597/00 , Y10T428/3154 , Y10T428/31544
摘要： A fluorine-containing adhesive material comprising a fluorine-containing ethylenic polymer having a carbonate group and/or a carboxylic halide group at a chain end or a side chain of polymer, wherein a total of a number of the carbonate groups and/or carboxylic halide groups is at least 150 relative to 1×106 main chain carbons, can directly impart the firm adherability to a substrate such as a metal, a glass or a resin while maintaining excellent properties such as resistance to chemicals, resistance to solvent, weatherability and resistance to stain possessed by a fluorine-containing polymer.
摘要翻译：一种含氟粘合剂材料，其包含在聚合物的链端或侧链具有碳酸酯基和/或羧基卤基的含氟乙烯性聚合物，其中总共多个碳酸酯基和/或羧酸卤化物基团相对于1×10 6个主链碳为至少150个，可以直接赋予基底如金属，玻璃或树脂牢固的粘合性，同时保持优异的性能如耐化学性，耐溶剂性，耐候性和含氟聚合物具有的抗污染性。

10. 发明授权

US09127114B2 Curable fluorine-containing polymer composition 有权
标题翻译：可固化含氟聚合物组合物
公开(公告)号：US09127114B2
公开(公告)日：2015-09-08
申请号：US12445354
申请日：2007-10-12
申请人： Katsuhiko Imoto , Tetsuo Shimizu , Tatsuya Morikawa , Masayuki Hayashi , Tomohiro Iimura , Peter Cheshire Hupfield
发明人： Katsuhiko Imoto , Tetsuo Shimizu , Tatsuya Morikawa , Masayuki Hayashi , Tomohiro Iimura , Peter Cheshire Hupfield
IPC分类号： C08G18/81 , C09D127/18 , C09D127/12 , C09D127/20 , C08G18/62 , C08G77/442 , C08L83/04 , C09D131/02 , C08G77/04 , C08G77/12 , C08K5/5419 , C08L27/12 , C08L31/02
CPC分类号： C08G18/8108 , C08G18/6279 , C08G77/045 , C08G77/12 , C08G77/442 , C08K5/5419 , C08L27/12 , C08L31/02 , C08L83/04 , C09D127/12 , C09D127/18 , C09D127/20 , C09D131/02 , C08L2666/04 , C08L2666/14
摘要： There is provided a curable fluorine-containing polymer composition which is quickly cured at relatively low temperatures by hydrosilylation reaction and provides a coating film which has high hardness, excellent solvent resistance and flexibility. The curable fluorine-containing polymer composition comprises a fluorine-containing polymer comprising a fluorinated ethylenic monomer unit and a non-fluorinated ethylenic monomer unit, in which a part or the whole of the non-fluorinated ethylenic monomer units is a unit represented by the formula: wherein R1 is hydrogen or methyl; R2 is a hydrocarbon group having ethylenic C═C; X is —C(O)NH— or —C(O)—; R3 is —O—, —O[CH(R4)]mO—, —(CH2)mO—, —OC(O)—(CH2)mO— or —(CH2)mOC(O)—(CH2)nO—, where R4 is —H, —OH, —CH2OH or —O—X—R2, a siloxane compound having hydrogen atom bonded to silicon atom, and a catalyst for hydrosilylation reaction.
摘要翻译：提供一种通过氢化硅烷化反应在相对低的温度下快速固化的可固化含氟聚合物组合物，并提供具有高硬度，优异的耐溶剂性和柔性的涂膜。可固化含氟聚合物组合物包含含有氟化乙烯性单体单元和非氟化乙烯性单体单元的含氟聚合物，其中一部分或全部未氟化烯属单体单元为式其中R1是氢或甲基; R2是具有烯属C = C的烃基; X是-C（O）NH-或-C（O） - ; R 3是-O-，-O [CH（R 4）] m O - ， - （CH 2）m O - ， - OC（O） - （CH 2）m O-或 - （CH 2）mOC（O） - （CH 2）其中R4是-H，-OH，-CH2OH或-O-X-R2，具有与硅原子键合的氢原子的硅氧烷化合物和氢化硅烷化反应的催化剂。

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