会员体验
专利管家(专利管理)
工作空间(专利管理)
风险监控(情报监控)
数据分析(专利分析)
侵权分析(诉讼无效)
联系我们
交流群
官方交流:
QQ群: 891211   
微信请扫码    >>>
现在联系顾问~
热词
    • 2. 发明申请
    • METHOD FOR PURIFYING CHLOROSILANES
    • 纯化氯霉素的方法
    • US20120121493A1
    • 2012-05-17
    • US13386926
    • 2010-07-07
    • Naoki NagaiTakaaki ShimizuKatsuhiro UeharaTohru Kubota
    • Naoki NagaiTakaaki ShimizuKatsuhiro UeharaTohru Kubota
    • C01B33/107
    • C01B33/10778
    • The present invention provides a method for obtaining high purity chlorosilanes from chlorosilanes containing boron impurities and phosphorus impurities. On the basis of the finding that solid by-product formation in the purification of chlorosilanes by adding an aromatic aldehyde results from a catalytic reaction by iron ions or rust-like iron, a Lewis base having a masking effect is added to chlorosilanes. Examples of the Lewis base include a divalent sulfur-containing compound and an alkoxysilane. The divalent sulfur-containing compound is preferably a compound represented by the formula: R—S—R′ (wherein R is a hydrocarbon group or a carbonyl group; and the sum of the carbon atoms in R and R′ is 7 or more), and the alkoxysilane is preferably a compound represented by the formula: RxSi(OR′)4-x (wherein R and R′ are each an alkyl group having 1 to 20 carbon atoms).
    • 本发明提供从含有硼杂质和磷杂质的氯硅烷中获得高纯度氯硅烷的方法。 基于通过添加芳族醛的氯硅烷纯化产生固体副产物的结果是由铁离子或铁锈铁的催化反应产生的,将具有掩蔽效应的路易斯碱加入到氯硅烷中。 路易碱碱的实例包括二价含硫化合物和烷氧基硅烷。 二价含硫化合物优选为由下式表示的化合物:R-S-R'(其中R为烃基或羰基; R和R'中的碳原子总数为7以上) 烷氧基硅烷优选为下式所示的化合物:RxSi(OR')4-x(式中,R和R'分别为碳原子数为1〜20的烷基)。
    • 3. 发明授权
    • Barcode scanner
    • 扫码机
    • US06811087B2
    • 2004-11-02
    • US10410395
    • 2003-04-10
    • Norio NakamuraNobuyasu GotoTakaaki ShimizuYutaka Ichinohe
    • Norio NakamuraNobuyasu GotoTakaaki ShimizuYutaka Ichinohe
    • G06K710
    • G06K7/10851
    • A barcode scanner comprising a laser driving circuit to drive a laser by a pulse signal generated by an oscillator, a preamplifier to amplify a voltage of a barcode signal from a photodetector corresponding to a reflected light from a barcode scanned by a light output of the laser driven by the pulse signal, a high-pass filter to remove a direct current component contained in an output signal of the preamplifier, a variable gain amplifier which controls an amplification gain of an output signal of the high-pass filter and performs automatic gain control to set an output level almost constant, a synchronous detector to detect a pulse signal contained in an output signal of the variable gain amplifier in synchronization with the output pulse of the oscillator, and a binarization circuit to binarize an output signal of the synchronous detector.
    • 一种条形码扫描器,包括:激光驱动电路,用于通过由振荡器产生的脉冲信号来驱动激光;前置放大器,用于放大来自光电检测器的条形码信号的电压,所述光电检测器对应于来自由激光的光输出扫描的条形码的反射光 由脉冲信号驱动的高通滤波器,去除包含在前置放大器的输出信号中的直流分量;可变增益放大器,其控制高通滤波器的输出信号的放大增益,并执行自动增益控制 为了使输出电平几乎恒定,同步检波器与振荡器的输出脉冲同步地检测包含在可变增益放大器的输出信号中的脉冲信号,以及二值化电路,对同步检波器的输出信号进行二值化。
    • 10. 发明授权
    • Method for the preparation of surface-modified silica particles
    • 表面改性二氧化硅颗粒的制备方法
    • US5013585A
    • 1991-05-07
    • US534450
    • 1990-06-06
    • Takaaki ShimizuTsutomu OgiharaMasatoshi Takita
    • Takaaki ShimizuTsutomu OgiharaMasatoshi Takita
    • B01J20/32C01B33/145C01B33/149C09C1/30C10M113/16
    • B82Y30/00C01B33/145C01B33/149C09C1/3081C10M113/16C01P2002/86C01P2004/64C01P2006/10C01P2006/12C10M2201/14C10M2227/04Y10T428/2995
    • A method for the preparation of a stable silica organosol in a hydrophobic organic solvent is proposed. The method comprises (a) hydrolyzing a tetraalkoxy silane, e.g. tetraethoxy silane, in an alcoholic medium in the presence of a limited amount of water and ammonia as a catalyst under controlled conditions so as to produce a silica alcosol in which the silica particles satisfy the requirements that the alkoxy groups and silanolic hydroxy groups are bonded to the silicon atoms on the surface in densities of at least 3.5 .mu. moles/m.sup.2 and not exceeding 2 .mu. mmoles/m.sup.2, respectively, and the specific surface area S given in m.sup.2 /g and the average particle diameter D given in nm of the silica particles satisfy the relationship of S.times.D.gtoreq.5000, D being 1 nm or larger, and (b) admixing the alcosol of silica particles with an organosilicon compound selected from the group consisting of the compounds represented by the general formula R.sub.4-n SiX.sub.n, (R.sub.3 Si).sub.2 NH, or YO--(--SiR.sub.2 --O--).sub.m --Y, in which each R is, independently from the others, a hydrogen atom or a monovalent hydrocarbon group, X is a hydroxy group or an alkoxy group, Y is a hydrogen atom or an alkyl group, n is 1, 2 or 3 and m is a positive integer not exceeding 20, in an amount, for example, in the range from 0.01 to 10 moles per mole of the silica particles under agitation of the mixture to effect a reaction for the modification of the surface of the silica particles followed by replacement of the alcoholic medium with a desired organic solvent.
    • 提出了一种在疏水性有机溶剂中制备稳定的二氧化硅有机溶胶的方法。 该方法包括(a)水解四烷氧基硅烷,例如 四乙氧基硅烷,在有限量的水和氨作为催化剂的存在下,在控制条件下在醇介质中,以产生二氧化硅颗粒,其中二氧化硅颗粒满足烷氧基和硅烷醇羟基键合的要求 表面上的硅原子的密度分别为至少3.5μmol/ m 2并且不超过2um mmoles / m 2,并且以m2 / g给出的比表面积S和以二氧化硅计的平均粒径D 颗粒满足SxD> / = 5000,D为1nm以上的关系,(b)将二氧化硅粒子的醇溶胶与选自由通式R4-nSiXn表示的化合物的有机硅化合物混合,( R3Si)2NH或YO - ( - SiR2-O-)mY,其中每个R独立地为氢原子或一价烃基,X为羟基或烷氧基,Y为氢 原子或烷基,n为1, 2或3,并且m是不超过20的正整数,其量例如在混合物搅拌下每摩尔二氧化硅颗粒为0.01至10摩尔,以实现改性表面的反应 二氧化硅颗粒,然后用所需的有机溶剂置换醇介质。