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    • 1. 发明申请
    • Submerged sample observation apparatus and method
    • US20040026618A1
    • 2004-02-12
    • US10636564
    • 2003-08-08
    • TOYOTA JIDOSHA KABUSHIKI KAISHA
    • Naoki Nakamura
    • G01N013/10G12B021/00
    • G01Q30/14Y10S977/86
    • An apparatus and a method for observing a submerged sample are disclosed, in which a scanning probe microscope comprises a cantilever with a probe arranged at the forward end thereof, a light source for applying light to the cantilever and a detector for detecting the light reflected from the cantilever, the apparatus further comprising a sample container having a side wall for holding a liquid therein. The probe is placed in closely opposed relation to the sample in the liquid in the sample container, and the relative positions of the probe and the sample are changed, so that based on the interaction between the probe and the sample, a surface image of the sample is produced to observe the sample. A device for preventing volatilization of the liquid having the sample submerged therein is formed on the surface of the liquid. An insulative liquid layer not mixed with the surface of the liquid having the sample submerged therein is formed on the surface of the liquid. Only the forward end of the probe is introduced into the liquid having the sample submerged therein, while the other portion of the probe is covered with the insulative liquid. The light from the light source is applied to the cantilever in the liquid without passing through the interface between the liquid and the atmosphere, and the reflected light is picked up in the liquid.
    • 2. 发明申请
    • Submerged sample observation apparatus and method
    • 浸没式样品观察装置及方法
    • US20020139178A1
    • 2002-10-03
    • US10099986
    • 2002-03-19
    • TOYOTA JIDOSHA KABUSHIKI KAISHA
    • Naoki Nakamura
    • G01B005/28
    • G01Q30/14Y10S977/86
    • An apparatus and a method for observing a submerged sample are disclosed, in which a scanning probe microscope comprises a cantilever with a probe arranged at the forward end thereof, a light source for applying light to the cantilever and a detector for detecting the light reflected from the cantilever, the apparatus further comprising a sample container having a side wall for holding a liquid therein. The probe is placed in closely opposed relation to the sample in the liquid in the sample container, and the relative positions of the probe and the sample are changed, so that based on the interaction between the probe and the sample, a surface image of the sample is produced to observe the sample. A device for preventing volatilization of the liquid having the sample submerged therein is formed on the surface of the liquid. An insulative liquid layer not mixed with the surface of the liquid having the sample submerged therein is formed on the surface of the liquid. Only the forward end of the probe is introduced into the liquid having the sample submerged therein, while the other portion of the probe is covered with the insulative liquid. The light from the light source is applied to the cantilever in the liquid without passing through the interface between the liquid and the atmosphere, and the reflected light is picked up in the liquid.
    • 公开了一种用于观察浸没式样品的装置和方法,其中扫描探针显微镜包括悬臂,其前端具有探针,用于向悬臂施加光的光源和检测器,用于检测从 所述悬臂,所述装置还包括具有用于在其中保持液体的侧壁的样本容器。 将探针放置在样品容器中的液体中与样品紧密相对的关系中,并且改变探针和样品的相对位置,使得基于探针和样品之间的相互作用, 产生样品以观察样品。 在液体的表面上形成有用于防止浸没在其中的样品的液体的挥发的装置。 在液体的表面上形成有与浸没有样品的液体的表面不混合的绝缘性液体层。 只有探头的前端被引入到浸没在其中的样品的液体中,而探针的另一部分被绝缘液覆盖。 来自光源的光被施加到液体中的悬臂,而不通过液体和大气之间的界面,并且反射光在液体中被拾取。
    • 3. 发明申请
    • Submerged sample observation apparatus and method
    • US20040025579A1
    • 2004-02-12
    • US10636565
    • 2003-08-08
    • TOYOTA JIDOSHA KABUSHIKI KAISHA
    • Naoki Nakamura
    • G01N013/10G01B011/30G01B011/00G01N021/49G01N021/47
    • G01Q30/14Y10S977/86
    • An apparatus and a method for observing a submerged sample are disclosed, in which a scanning probe microscope comprises a cantilever with a probe arranged at the forward end thereof, a light source for applying light to the cantilever and a detector for detecting the light reflected from the cantilever, the apparatus further comprising a sample container having a side wall for holding a liquid therein. The probe is placed in closely opposed relation to the sample in the liquid in the sample container, and the relative positions of the probe and the sample are changed, so that based on the interaction between the probe and the sample, a surface image of the sample is produced to observe the sample. A device for preventing volatilization of the liquid having the sample submerged therein is formed on the surface of the liquid. An insulative liquid layer not mixed with the surface of the liquid having the sample submerged therein is formed on the surface of the liquid. Only the forward end of the probe is introduced into the liquid having the sample submerged therein, while the other portion of the probe is covered with the insulative liquid. The light from the light source is applied to the cantilever in the liquid without passing through the interface between the liquid and the atmosphere, and the reflected light is picked up in the liquid.