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1. 发明授权

US4581166A Method for isolating and purifying antibiotics 失效
标题翻译：分离纯化抗生素的方法
公开(公告)号：US4581166A
公开(公告)日：1986-04-08
申请号：US609204
申请日：1984-05-11
申请人： Siegfried Peter , Hubert Coenen , Rainer Hagen
发明人： Siegfried Peter , Hubert Coenen , Rainer Hagen
IPC分类号： A61K35/74 , A61K38/00 , B01D11/04 , C07D307/94 , C07D499/00 , C07D499/18 , C07D501/12 , C07K1/14 , C12P37/00 , C07C67/58 , C07H15/22
CPC分类号： C07D307/94 , C07D499/00
摘要： A process is proposed for the isolation and purification of antibiotics wherein an antibiotic containing solution is extracted with an extraction agent at a temperature of from 0.degree. to 40.degree. C. and at a pressure which lies between the critical pressure and the ten-fold value of the critical pressure of the extraction agent, with the weight ratio of antibiotic containing solution to the extraction agent being 1:5 to 1:20, wherein the antibiotics are precipitated from the antibiotic containing extraction agent by reducing its density and wherein the extraction agent is recirculated. An entrainer may be added to the extraction agent. The reduction in density of the antibiotic containing extraction agent may be effected by expansion to a pressure of from 30 to 70 bar.
摘要翻译：提出了一种用于分离和纯化抗生素的方法，其中含有抗生素的溶液在0℃至40℃的温度和在临界压力和十倍值之间的压力下用萃取剂萃取的提取剂的临界压力，抗生素含量溶液与提取剂的重量比为1:5至1:20，其中抗生素通过降低其密度从含抗生素的提取剂中沉淀出来，其中提取剂再循环。可以将萃取剂加入到夹带剂中。含抗生素的提取剂的密度降低可以通过膨胀至30至70巴的压力来实现。

2. 发明授权

US5434280A Process for preparing pure monoglycerides, pure diglycerides and/or pure triglycerides 失效
标题翻译：制备纯甘油单酯，纯甘油二酯和/或纯甘油三酯的方法
公开(公告)号：US5434280A
公开(公告)日：1995-07-18
申请号：US155923
申请日：1993-11-22
申请人： Siegfried Peter , Bernd Czech , Ulrich Ender , Eckhard Weidner
发明人： Siegfried Peter , Bernd Czech , Ulrich Ender , Eckhard Weidner
IPC分类号： C07C67/58 , C07C69/30 , C11C1/00 , C11C3/10 , C11B7/00
CPC分类号： C07C67/58
摘要： The invention relates to a process for recovering monoglycerides and optionally diglycerides and/or triglycerides as well as optionally glycerol from mixtures comprising glycerides and glycerol containing glycerides, respectively, by countercurrent extraction with a circulating extraction. As an extractant, forming a separate phase, there is used a hydrocarbon having a density of more than 180 kg/m.sup.3 and/or trifluoromethane having a density of more than 180 kg/m.sup.3.
摘要翻译：本发明涉及通过循环提取的逆流提取来分别回收单甘油酯和任选的甘油二酯和/或甘油三酸酯以及任选的甘油，其包含甘油酯和含甘油的甘油酯的混合物。作为萃取剂，形成分离相，使用密度大于180kg / m 3的烃和/或密度大于180kg / m 3的三氟甲烷。

3. 发明授权

US4345976A Process for separating mixtures of substances of low volatility 失效
标题翻译：分离低挥发性物质混合物的方法
公开(公告)号：US4345976A
公开(公告)日：1982-08-24
申请号：US10143
申请日：1979-02-07
申请人： Siegfried Peter , Gerd Brunner , Rolf Riha
发明人： Siegfried Peter , Gerd Brunner , Rolf Riha
IPC分类号： B01D3/40 , B01D11/04 , C07C51/46 , B01D3/36 , C11C1/10
CPC分类号： C07C51/46 , B01D11/0407 , B01D3/40 , Y02P20/544
摘要： The invention involves a process for substantially separating the components of mixtures of substances at least one of which is of low volatility while the other is of low or no volatility, the process using a compressed gas under supercritical conditions and an entrainer which increases the concentration of said mixture in the gaseous phase as well as the separation factor between the components to be separated. The process operates in two distillation zones the first of which substantially separates the components of low volatility in a process similar to a rectification process while the second distillation zone separates the top product of the first distillation zone from the gas with the aid of the entrainer which is condensed partially and in this state is passed in countercurrent to the gas carrying the separated component of low volatility.
摘要翻译：本发明涉及一种用于基本上分离其中至少一种具有低挥发性，另一种具有低挥发性或不挥发性的物质混合物的组分的方法，该方法在超临界条件下使用压缩气体，并且夹带剂增加了所述气相中的混合物以及要分离的组分之间的分离因子。该方法在两个蒸馏区中操作，其中第一个蒸馏区在类似于精馏过程的过程中基本上分离低挥发性组分，而第二蒸馏区借助于夹带剂将第一蒸馏区的顶部产物与气体分离，被部分冷凝，并且在该状态下与携带低挥发性的分离组分的气体逆流通过。

4. 发明授权

US07468450B2 Process for the transesterification of fats and oils of biological origin by means of alcoholysis using special carbonic acid salts 失效
标题翻译：通过使用特殊的碳酸盐进行醇解来酯交换生物来源的脂肪和油的方法
公开(公告)号：US07468450B2
公开(公告)日：2008-12-23
申请号：US11086267
申请日：2005-03-22
申请人： Siegfried Peter , Eckhard Weidner
发明人： Siegfried Peter , Eckhard Weidner
IPC分类号： C11C1/00
CPC分类号： C11C3/10 , C07C67/03 , C11C3/003 , C07C69/24 , C07C69/52
摘要： The invention relates to a process for the preparation of fatty acid esters from fats and oils of biological origin by transesterification with monohydric alcohols in the presence of basic catalysts, the catalysts being salts of a basic organic compound and carbonic acid.
摘要翻译：本发明涉及一种通过在碱性催化剂存在下通过与一元醇的酯交换从生物来源的脂肪和油制备脂肪酸酯的方法，该催化剂是碱性有机化合物和碳酸的盐。

5. 发明申请

US20060058540A1 Process for the transesterification of fats and oils of biological origin by means of alcoholysis using special carbonic acid salts 失效
标题翻译：通过使用特殊的碳酸盐进行醇解来酯化生物来源的脂肪和油的方法
公开(公告)号：US20060058540A1
公开(公告)日：2006-03-16
申请号：US11086267
申请日：2005-03-22
申请人： Siegfried Peter , Eckhard Weidner
发明人： Siegfried Peter , Eckhard Weidner
IPC分类号： C07C51/43
CPC分类号： C11C3/10 , C07C67/03 , C11C3/003 , C07C69/24 , C07C69/52
摘要： The invention relates to a process for the preparation of fatty acid esters from fats and oils of biological origin by transesterification with monohydric alcohols in the presence of basic catalysts, the catalysts being salts of a basic organic compound and carbonic acid.
摘要翻译：本发明涉及一种通过在碱性催化剂存在下通过与一元醇的酯交换从生物来源的脂肪和油制备脂肪酸酯的方法，该催化剂是碱性有机化合物和碳酸的盐。

6. 发明授权

US4756818A A method for the production of a carbon fiber precursor 失效
标题翻译：一种生产碳纤维前体的方法
公开(公告)号：US4756818A
公开(公告)日：1988-07-12
申请号：US18200
申请日：1987-02-24
申请人： Siegfried Peter , Herbert Beneke , Franz Oeste , Wolfgang Fexer , Wolfgang Jaumann , Manfred Meinbreckse , Joachim Kempfert
发明人： Siegfried Peter , Herbert Beneke , Franz Oeste , Wolfgang Fexer , Wolfgang Jaumann , Manfred Meinbreckse , Joachim Kempfert
IPC分类号： C10C3/02 , C08L95/00 , C10C1/04 , C10C3/04 , C10C3/08 , D01F9/15 , C10C1/18
CPC分类号： C10C1/04 , C10C3/08 , D01F9/15
摘要： A method for the production of a carbon fiber precursor from coal tar pitch comprising extracting coal tar pitch at elevated temperatures and pressures with a mixture of a supercritical gas and an entraining agent to obtain a solution free of quinoline-insoluble components, recovering from the solution by lowering the pressure and/or raising the temperature to obtain at least one fraction selected from the group consisting of quinoline-soluble fraction and toluene-soluble fraction, treating the said fraction(s) at 380.degree. to 450.degree. C. under a non-oxidizing atmosphere at atmosphere pressure until 40 to 65% by volume of the product is converted into pitch containing mesophase, extracting the latter pitch with a mixture of supercritical gas and an entraining agent to remove isotropic pitch and recovering isotropic pitch with a mesophase content of at least 75% by volume, a pyridine-insoluble matter content of 20 to 50% by weight, a mean molecular weight of 900 to 1200 and a melting point of 330.degree. to 360.degree. C. and the isotropic pitch product produced therefrom and carbon fibers made from the isotropic pitch.
摘要翻译：一种从煤沥青沥青生产碳纤维前体的方法，包括在高温和高压下用超临界气体和夹带剂的混合物萃取煤焦油沥青以获得不含喹啉不溶性组分的溶液，从溶液中回收通过降低压力和/或升高温度以获得至少一种选自喹啉可溶级分和甲苯可溶级分的级分，在380-450℃下处理所述级分，在空气压力下的氧化气氛直到产物的40至65体积％转化为含有中间相的沥青，用超临界气体和夹带剂的混合物萃取后者沥青以除去各向同性沥青并回收各向同性沥青，中间相含量为至少75体积％，吡啶不溶物质含量为20〜50重量％，平均分子量为900〜1200，熔点为330〜360℃，由各向同性沥青产物及各向同性沥青制成碳纤维。

7. 发明授权

US06579996B2 Process for removing free fatty acids from fats and oils of biological origin or their steam distillates 失效
标题翻译：从生物来源的油脂或其蒸馏馏分中除去游离脂肪酸的方法
公开(公告)号：US06579996B2
公开(公告)日：2003-06-17
申请号：US10046063
申请日：2001-10-20
申请人： Siegfried Peter , Eckhard Weidner , Martin Drescher , Wolfgang König
发明人： Siegfried Peter , Eckhard Weidner , Martin Drescher , Wolfgang König
IPC分类号： C11B300
CPC分类号： C11B3/06
摘要： A method for removing free fatty acids from fats or oils of biological origin or their steam distillates by extracting the free fatty acids with a mixture of basic organic nitrogen compounds and water as an extraction medium at a temperature below the boiling point of the organic nitrogen compounds. The content of the basic organic nitrogen compounds in the extraction medium is 20-30% by weight. In this manner, the formation of a viscous soapstock which is difficult to remove is prevented. The boiling point of the basic organic nitrogen compounds used is the same as or above boiling point of water and below the boiling point of the fatty acids to be extracted in order to enable simple recovery of the extraction medium.
摘要翻译：通过在低于有机氮化合物的沸点的温度下用碱性有机氮化合物和水的混合物萃取游离脂肪酸作为提取介质，从生物来源的脂肪或油或其蒸汽馏出物中除去游离脂肪酸的方法。萃取介质中碱性有机氮化合物的含量为20-60％（重量）。以这种方式，防止了难以去除的粘性肥皂的形成。使用的碱性有机氮化合物的沸点与水的沸点相同或高于待提取的脂肪酸的沸点，以使得能够简单地回收萃取介质。

8. 发明授权

US06211390B1 Method for producing fatty acid esters 失效
标题翻译：脂肪酸酯的制造方法
公开(公告)号：US06211390B1
公开(公告)日：2001-04-03
申请号：US09269090
申请日：1999-12-03
申请人： Siegfried Peter , Ruth Ganswindt , Eckhard Weidner
发明人： Siegfried Peter , Ruth Ganswindt , Eckhard Weidner
IPC分类号： C07C5100
CPC分类号： C11C3/003 , C07C67/58 , C07C69/52
摘要： The invention concerns a method for producing fatty acid esters from fatty acid triglyceride and in particular from animal or vegetable fats and oils by transesterification with a monovalent low-molecular weight alcohol in the presence of a homogeneous or heterogeneous catalyst. In accordance with the invention, the formed fatty acid ester is extracted from the reaction mixture by means of a near-critical extractant. In this way fatty acid esters are obtained at high yield and excellent purity. As the extractant preferably a low pressure gas having a reduced temperature at 20° C. of about 0.7, preferably of equal to or greater than 0.7, is employed. Preferred extractants are carbon dioxide, propane, butane, dimethyl ether, ethyl acetate or mixtures thereof.
摘要翻译：本发明涉及一种通过在均相或多相催化剂存在下通过与一价低分子量醇的酯交换从脂肪酸甘油三酯，特别是动物或植物脂肪和油制备脂肪酸酯的方法。根据本发明，通过近临界萃取剂从反应混合物中提取形成的脂肪酸酯。以这种方式获得高产率和优异纯度的脂肪酸酯。作为萃取剂，优选使用在20℃下的温度降低约0.7，优选等于或大于0.7的低压气体。优选的萃取剂是二氧化碳，丙烷，丁烷，二甲醚，乙酸乙酯或其混合物。

9. 发明授权

US5597602A Process for de-oiling crude lecithin 失效
标题翻译：粗卵磷脂脱油工艺
公开(公告)号：US5597602A
公开(公告)日：1997-01-28
申请号：US362448
申请日：1995-04-21
申请人： Siegfried Peter , Bernd Czech , Eckard Weidner , Zhenfeng Zhang
发明人： Siegfried Peter , Bernd Czech , Eckard Weidner , Zhenfeng Zhang
IPC分类号： A23J7/00 , C07F9/10 , C11B1/10 , C11B3/00 , C11B7/00 , A23D7/005
CPC分类号： C11B1/104 , A23J7/00
摘要： A process for recovering lecithin from oil- and lecithin-containing mixtures, comprising extracting a lecithin/oil mixture with an extractant selected from the group consisting of a hydrocarbon having 3 carbon atoms, an unbranched hydrocarbon having 4 carbon atoms, a branched hydrocarbon having 4 carbon atoms, and mixtures thereof, at a pressure of from 1 to 8 MPa and a temperature of from 20 to 100.degree. C., which conditions ensure liquid phase extraction with the development of two liquid phases, one of which is an oil enriched liquid hydrocarbon phase and the other of which is a lecithin enriched hydrocarbon phase; separating the two liquid hydrocarbon phases; and recovering substantially lecithin-free oil from the oil-enriched phase and substantially oil-free, pure lecithin from the lecithin-enriched phase.
摘要翻译： PCT No.PCT / EP93 / 01750 Sec。 371日期1995年04月21日 102（e）日期1995年4月21日PCT提交1993年7月6日PCT公布。出版物WO94 / 01004 日期1994年1月20日一种从含有油和含卵磷脂的混合物中回收卵磷脂的方法，包括用选自具有3个碳原子的烃，具有4个碳原子的未分支烃的提取剂萃取卵磷脂/油混合物，具有4个碳原子的支链烃及其混合物，压力为1至8MPa，温度为20至100℃，这些条件确保液相萃取与两个液相的发展，其中之一是富油液相烃相，另一个是富含卵磷脂的烃相; 分离两个液相烃相; 并从富含油脂的相中回收基本上不含卵磷脂的油，并从富含卵磷脂的相中回收基本上无油的纯卵磷脂。

10. 发明申请

US20050020843A1 Process for the transesterification of fat and/or oil by heterogeneous catalysis 审中-公开
标题翻译：通过非均相催化酯交换脂肪和/或油的方法
公开(公告)号：US20050020843A1
公开(公告)日：2005-01-27
申请号：US10887455
申请日：2004-07-08
申请人： Siegfried Peter , Eckhard Weidner , Hans-Peter Neuner
发明人： Siegfried Peter , Eckhard Weidner , Hans-Peter Neuner
IPC分类号： B01J31/02 , C11C3/10 , C07C51/43
CPC分类号： C11C3/003 , C11C3/10
摘要： A process for preparing fat and/or oil with a modified distribution of fatty acids in the glycerides by heterogeneously catalysed transesterification, wherein the process comprises reaction of the fat and/or oil of biological origin to be transesterified in the presence of a catalyst consisting of a metal salt of a basic amino acid or an amino acid derivative. The disadvantages of conventional transesterification processes can be overcome by using this catalyst.
摘要翻译：一种通过异构催化酯交换制备具有脂肪酸在甘油酯中的分布改变的脂肪和/或油的方法，其中所述方法包括将生物来源的脂肪和/或油在催化剂存在下进行酯交换反应，所述催化剂由碱性氨基酸或氨基酸衍生物的金属盐。通过使用该催化剂可以克服常规酯交换方法的缺点。

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