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1. 发明授权

US4599112A Recording liquid 失效
标题翻译：记录液体
公开(公告)号：US4599112A
公开(公告)日：1986-07-08
申请号：US666137
申请日：1984-10-31
申请人： Yasumasa Yokoyama , Tomoko Komori , Tsuyoshi Eida , Shoji Koike , Masatsune Kobayashi
发明人： Yasumasa Yokoyama , Tomoko Komori , Tsuyoshi Eida , Shoji Koike , Masatsune Kobayashi
IPC分类号： C09D11/00 , B41M5/00 , C09D11/10 , C09D11/16 , C09D11/02
CPC分类号： C09D11/328
摘要： A recording liquid containing as a coloring component a copper phthalocyanine dye having at least one alkali metal sulfonate substituent is provided. The recording liquid is characterized in that the ratio of the integrated peak areas (A/B) in a liquid chromatogram of said dye is at least 1/6, wherein, provided that the retention time of the main peak is taken as 1.00, A and B represent the integrated peak area of the relative retention time of from 0 to 0.80 and that of from 0.85 to 4.00, respectively.
摘要翻译：提供含有至少一种碱金属磺酸盐取代基的铜酞菁染料作为着色组分的记录液。记录液的特征在于，所述染料的液相色谱图中的积分峰面积（A / B）的比率为至少1/6，其中，如果将主峰的保留时间设为1.00，则A B表示相对保留时间为0至0.80，0.85至4.00的相对保留时间的积分峰面积。

2. 发明授权

US4632703A Recording liquid 失效
标题翻译：记录液体
公开(公告)号：US4632703A
公开(公告)日：1986-12-30
申请号：US592546
申请日：1984-03-23
申请人： Shoji Koike , Tsuyoshi Eida , Masatsune Kobayashi , Yasumasa Yokoyama , Tomoko Komori
发明人： Shoji Koike , Tsuyoshi Eida , Masatsune Kobayashi , Yasumasa Yokoyama , Tomoko Komori
IPC分类号： C09D11/00 , C09B47/24 , C09B47/26 , C09B67/00 , C09D11/02
CPC分类号： C09D11/328 , C09B47/24 , C09B47/26 , C09B67/0032
摘要： A recording liquid comprises a recording agent, water and a water-soluble organic solvent as essential components, wherein said recording agent comprises at least one of the dyes represented by the formula (A) shown below: ##STR1## (wherein [Ph] represents a phthalocyanine skeleton at the center of which a metal atom may be coordinated, X represents an alkali metal or NH.sub.4, a and b each independently represent an integer of 1 to 3 satisfying the relation of 2.ltoreq.a+b.ltoreq.4, Q represents a group --SO.sub.2 OR.sub.1 or a group --SO.sub.2 NR.sub.2 R.sub.3, where R.sub.1 represents an alkyl or an alicyclic group having not more than 15 carbon atoms which may be branched or an aralkyl group having not more than 15 carbon atoms, R.sub.2 and R.sub.3 each independently represent a group --CH.sub.2 CH.sub.2 O).sub.n R.sub.4, a group --CH.sub.2 CHOH).sub.n R.sub.4, a group ##STR2## a straight or cyclic alkyl group having not more than 15 carbon atoms which may be branched or an aralkyl group having not more than 15 carbon atoms or an amino acid salt radical, n means an integer of 0 to 12, and R.sub.4 means H, CH.sub.3 or CH.sub.2 OH).
摘要翻译：记录液体包括记录剂，水和作为必需组分的水溶性有机溶剂，其中所述记录剂包含至少一种由下式（A）表示的染料：（A）（其中[ Ph]表示在其中心处可以配位金属原子的酞菁骨架，X表示碱金属或NH 4，a和b各自独立地表示1〜3的整数，满足2≤a+ b < / = 4，Q表示-SO 2 OR 1或-SO 2 NR 2 R 3基团，其中R 1表示可以是支链或碳原子数15以下的芳烷基的碳原子数不超过15个的烷基或脂环基，R2和 R 3各自独立地表示基团-CH 2 CH 2 O）n R 4，基团-CH 2 CHOH）n R 4，基团，可以是支链或不超过15个碳原子的芳烷基的直链或环状烷基，具有不超过15个碳原子原子或氨基酸盐基，n表示0t的整数 o 12，R 4表示H，CH 3或CH 2 OH）。

3. 发明授权

US4557761A Recording liquid 失效
标题翻译：记录液体
公开(公告)号：US4557761A
公开(公告)日：1985-12-10
申请号：US552794
申请日：1983-11-17
申请人： Masatsune Kobayashi , Tsuyoshi Eida , Shoji Koike , Yasumasa Yokoyama , Tomoko Komori
发明人： Masatsune Kobayashi , Tsuyoshi Eida , Shoji Koike , Yasumasa Yokoyama , Tomoko Komori
IPC分类号： C09B31/08 , C09D11/00 , C09D11/02
CPC分类号： C09D11/328 , C09B31/08 , C09D11/037 , Y10S260/38
摘要： A recording liquid comprising coloring matter, which is an image-forming component, and a liquid medium for dissolving or dispersing the coloring matter, the recording liquid being characterized by containing at least one of the dyes represented by the following general formula (A), as an image-forming component,Q.sup.1 -N=N--Q.sup.2 --N=N--Q.sup.3 (A)wherein Q.sup.1 and Q.sup.3 each represent a substituted phenyl or naphthyl group having at least one SO.sub.3 M substituent and Q.sup.2 represents a substituted naphthyl group having at least one SO.sub.3 M substituent, M being a base selected from Na, K, Li, NH.sub.4, and amine salt cations.A recording liquid comprising coloring matter, which is an image-forming component, and a liquid medium for dissolving or dispersing the coloring matter, the recording liquid being characterized by containing at least one of the dyes represented by the following general formula (B), as an image-forming component, ##STR1## wherein; R represents one member selected from the group consisting --COCH.sub.3, ##STR2## R.sup.7, R.sup.8 and R.sup.9 each being a member selected from the group consisting of H, CH.sub.3, C.sub.2 H.sub.5, Cl, NH.sub.2, OH and OCH.sub.3 : and M represents a base selected from Na, K, Li, NH.sub.4, and amine salt cations.
摘要翻译：包含作为成像成分的着色物质和用于溶解或分散着色剂的液体介质的记录液体，其特征在于含有下述通式（A）表示的至少一种染料，作为成像成分，Q1-N = N-Q2-N = N-Q3（A）其中Q1和Q3各自表示具有至少一个SO3M取代基的取代的苯基或萘基，Q2表示取代的萘基，至少一个SO 3 M取代基，M为选自Na，K，Li，NH 4和胺盐阳离子的碱。包含作为成像成分的着色物质和用于溶解或分散着色剂的液体介质的记录液体，其特征在于含有至少一种由以下通式（B）表示的染料，作为图像形成成分，（B）其中; R表示选自由以下组成的组中的一个：-COCH 3，R 3，R 7，R 8和R 9各自为选自H，CH 3，C 2 H 5，Cl，NH 2，OH和OCH 3的成员：和 M表示选自Na，K，Li，NH 4和胺盐阳离子的碱。

4. 发明授权

US4505749A Method of forming color images 失效
标题翻译：形成彩色图像的方法
公开(公告)号：US4505749A
公开(公告)日：1985-03-19
申请号：US507580
申请日：1983-06-24
申请人： Kazue Kanekiyo , Masatsune Kobayashi , Yasumasa Yokoyama , Tsuyoshi Eida , Tomoko Komori , Shoji Koike
发明人： Kazue Kanekiyo , Masatsune Kobayashi , Yasumasa Yokoyama , Tsuyoshi Eida , Tomoko Komori , Shoji Koike
IPC分类号： B41M1/18 , C09D11/02
CPC分类号： B41M1/18
摘要： In a process for forming color images using more than one kind of color ink including black ink, the dyes in the color ink used have similar chromatographic characteristics. Preferably any difference of the Rf value of paper chromatography between any of the two dyes is not more than 0.30.
摘要翻译：在使用包括黑色墨水的多种彩色墨水形成彩色图像的方法中，所使用的彩色墨水中的染料具有相似的色谱特性。纸张色谱法中任何两种染料之间的任何差值优选不大于0.30。

5. 发明授权

US4627875A Recording liquid 失效
标题翻译：记录液体
公开(公告)号：US4627875A
公开(公告)日：1986-12-09
申请号：US828590
申请日：1986-02-10
申请人： Masatsune Kobayashi , Tsuyoshi Eida , Shoji Koike , Keiko Nakousai
发明人： Masatsune Kobayashi , Tsuyoshi Eida , Shoji Koike , Keiko Nakousai
IPC分类号： C09D11/00 , C09D11/02
CPC分类号： C09D11/17 , C09D11/30 , C09D11/328
摘要： A recording liquid comprises C.I.Acid Red 8 as a recording agent for forming an image and a liquid medium comprising at least(a) a member selected from the group consisting of polyethylene glycol, polyethylene glycol mono methylether and a mixture thereof,(b) a member selected from the group consisting of diethylene glycol, sulfolane and a mixture thereof,(c) a member selected from the group consisting of N-methyl-2-pyrrolidone, 1,3-dimethyl-2-imidazolidinone and a mixture thereof, and(d) water.
摘要翻译：记录液体包含作为形成图像的记录剂的CIAcid Red 8和至少包含（a）选自聚乙二醇，聚乙二醇单甲醚及其混合物的成员的液体介质，（b）选自二甘醇，环丁砜及其混合物的成分，（c）选自N-甲基-2-吡咯烷酮，1,3-二甲基-2-咪唑啉酮及其混合物的成员，以及（d）水。

6. 发明授权

US4661158A Recording liquid 失效
标题翻译：记录液体
公开(公告)号：US4661158A
公开(公告)日：1987-04-28
申请号：US732635
申请日：1985-05-10
申请人： Masatsune Kobayashi , Tsuyoshi Eida , Shoji Koike , Keiko Nakousai
发明人： Masatsune Kobayashi , Tsuyoshi Eida , Shoji Koike , Keiko Nakousai
IPC分类号： B41J2/14 , C09B43/16 , C09D11/00 , C09D11/02 , H01L41/39
CPC分类号： C09D11/328 , C09B43/16
摘要： A recording liquid mainly comprises a recording agent as an image-forming component and a liquid medium containing at least water and a glycol for dissolving or dispersing the recording agent, characterized in that the recording agent contains at least one of dyes represented by the following general formula (A): ##STR1## wherein M represents one element selected from H, Na, Li and K, and 55 mole % or more of total M given in the general formula (A) is Na, Li or K. The recording liquid may additionally contain a water-soluble organic solvent.
摘要翻译：记录液体主要包括作为成像成分的记录剂和至少含有用于溶解或分散记录剂的水和二醇的液体介质，其特征在于，记录剂含有至少一种下列通式式（A）：其中M表示选自H，Na，Li和K中的一种元素，通式（A）中给出的总M的55摩尔％以上为Na，Li或记录液可另外含有水溶性有机溶剂。

7. 发明授权

US5017227A Recording liquid and ink-jet recording process using same 失效
标题翻译：记录使用其的液体和喷墨记录过程
公开(公告)号：US5017227A
公开(公告)日：1991-05-21
申请号：US385153
申请日：1989-07-26
申请人： Shoji Koike , Tsuyoshi Eida , Takao Yamamoto
发明人： Shoji Koike , Tsuyoshi Eida , Takao Yamamoto
IPC分类号： C09D11/00 , C09D11/02
CPC分类号： C09D11/328
摘要： A recording liquid comprising dyes and a liquid medium, wherein the dyes include a black dye and at least one water-soluble dye of a magenta dye and a yellow dye in combination. The black dye is selected from the group, C.I. Food Black 1, C.I. Acid Black 140 and C.I. Acid Black 187.
摘要翻译：一种包含染料和液体介质的记录液体，其中染料包括黑色染料和至少一种品红色染料的水溶性染料和黄色染料的组合。黑色染料选自C.I. 食物黑1，C.I. 酸性黑140和C.I. 酸性黑色187。

8. 发明授权

US5296022A Ink-jet recording method and apparatus employing ink containing halogenated alkanol with 2 to 4 carbon atoms 失效
标题翻译：使用含有2-4个碳原子的卤代烷醇的油墨的喷墨记录方法和装置
公开(公告)号：US5296022A
公开(公告)日：1994-03-22
申请号：US79747
申请日：1993-06-22
申请人： Masatsune Kobayashi , Shoji Koike , Shinichi Tochihara , Kyoko Fukushima , Akira Nagashima , Koromo Shirota , Kumiko Mafune
发明人： Masatsune Kobayashi , Shoji Koike , Shinichi Tochihara , Kyoko Fukushima , Akira Nagashima , Koromo Shirota , Kumiko Mafune
IPC分类号： C09D11/00 , G01D9/00 , G01D15/00
CPC分类号： C09D11/30
摘要： An ink-jet method and apparatus employing an ink comprising a dye and a liquid medium for dissolving or dispersing a dye, wherein the liquid medium comprises an alkyl alcohol having 2 to 4 carbon atoms, in which at least one of the hydrogen atoms is substituted by a halogen atom.
摘要翻译：一种喷墨方法和使用包含染料和用于溶解或分散染料的液体介质的油墨的喷墨方法和装置，其中液体介质包含具有2至4个碳原子的烷基醇，其中至少一个氢原子被取代通过卤素原子。

9. 发明授权

US08506067B2 Ink jet image-forming method, ink jet color image-forming method and ink jet recording apparatus 有权
标题翻译：喷墨成像方法，喷墨彩色成像方法和喷墨记录装置
公开(公告)号：US08506067B2
公开(公告)日：2013-08-13
申请号：US12664084
申请日：2008-07-22
申请人： Shoji Koike , Ryota Kato , Hitoshi Yoshino
发明人： Shoji Koike , Ryota Kato , Hitoshi Yoshino
IPC分类号： C09D11/02
CPC分类号： B41M5/0023 , C09D11/322
摘要： An ink jet image-forming method for forming an image by applying an ink in a fixed amount of 0.5 pl or more to 6.0 pl or less to plain paper. The ink contains a self-dispersion pigment, water, a water-soluble compound having a coefficient of hydrophilicity-hydrophobicity of 0.37 or more as defined by the equation (A) stated in the description and a water-soluble compound having a coefficient of hydrophilicity-hydrophobicity of 0.25 or less, and has a surface tension of 34 mN/m or less. The application of the ink is divided into plural times when an image having a portion where the ink is applied in a duty of 80% or more and an amount of 5.0 μl/cm2 or less in total is formed in a basic matrix for forming the image, and the amount of the ink applied at each of the times divided is 0.7 μl/cm2 or less.
摘要翻译：一种喷墨图像形成方法，用于通过将普通纸的固定量为0.5pl以上至6.0pl以下的墨水进行图像形成。油墨含有自分散颜料，水，具有亲水性 - 疏水性系数的水溶性化合物，如描述中所述的式（A）所定义的0.37以上，具有亲水性系数的水溶性化合物 - 疏水性为0.25以下，表面张力为34mN / m以下。当在具有80％以上的占空比和总共5.0mul / cm 2以下的量施加墨水的部分的图像形成在基本基质中时，油墨的涂布被分成多次，以形成图像，并且在每次分割时施加的油墨量为0.7mul / cm 2以下。

10. 发明授权

US08328926B2 Ink jet recording ink, ink jet image-forming method and ink jet recording apparatus 有权
标题翻译：喷墨记录油墨，喷墨图像形成方法和喷墨记录装置
公开(公告)号：US08328926B2
公开(公告)日：2012-12-11
申请号：US12665065
申请日：2008-07-22
申请人： Shoji Koike , Ryota Kato , Hitoshi Yoshino
发明人： Shoji Koike , Ryota Kato , Hitoshi Yoshino
IPC分类号： C09D11/02
CPC分类号： C09D11/322
摘要： The invention provides an ink jet recording ink containing a self-dispersion pigment having a lactone group and a carboxyl group, an organic carboxylic acid salt, water and a water-soluble substance having a coefficient of hydrophilicity-hydrophobicity of 0.37 or more as defined by the following equation (A), and having a surface tension of 34 mN/m or less. Coefficient of hydrophilicity-hydrophobicity=[(Water activity value of a 20% aqueous solution)−(Molar fraction of water in the 20% aqueous solution)]/ [1−(Molar fraction of water in the 20% aqueous solution)] Equation (A)
摘要翻译：本发明提供一种含有内酯基和羧基的自分散颜料，有机羧酸盐，水和亲水疏水性系数为0.37以上的水溶性物质的喷墨记录油墨，其定义如下：下述式（A），表面张力为34mN / m以下。亲水性 - 疏水性系数= [（20％水溶液的水分活度值） - （20％水溶液中的水的摩尔分数）] / [1-（20％水溶液中的水的摩尔分数）]式（一个）

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