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1. 发明申请

US20070246176A1 Pulp Bleaching Processes 审中-公开
标题翻译：纸浆漂白工艺
公开(公告)号：US20070246176A1
公开(公告)日：2007-10-25
申请号：US11628961
申请日：2005-06-08
申请人： Shoichi Miyawaki , Kazuhiro Kurosu , Takashi Ochi
发明人： Shoichi Miyawaki , Kazuhiro Kurosu , Takashi Ochi
IPC分类号： D21C9/10
CPC分类号： D21C9/1005 , D21C9/1084 , D21C9/16
摘要： The present invention aims to further advance the acid treatment or irradiation technology for pulp to develop a bleaching process using smaller amounts of chlorine chemicals with higher efficiency as compared with conventional bleaching processes. It also aims to provide an excellent high brightness pulp having a low environmental impact and no discoloration as well as a paper containing it. The present invention provides a chlorine-free bleaching process with very high efficiency by irradiating a pulp washed after an acid treatment with UV light and/or visible light at a wavelength of 100-400 nm under alkaline conditions, preferably in a pH range of 10-13. The acid treatment can be performed under conditions of pH 1-6 and a temperature of 80° C. or more. The irradiation treatment can be performed in the presence of at least one compound selected from the group consisting of reducing agents, peroxides, and hydrogen-donating organic compounds. The present invention also provides a high brightness chemical pulp having an ISO brightness of 88% or more and a brightness loss of 1.0% or less in a specific fading test.
摘要翻译：本发明旨在进一步推进纸浆的酸处理或照射技术，与常规漂白方法相比，使用较少量的氯化学品与更高效率开发漂白工艺。它还旨在提供具有低环境影响和不变色的优异的高亮度纸浆以及含有它的纸。本发明通过在碱性条件下，优选在pH范围为10的范围内，用紫外光和/或波长为100-400nm的紫外线和/或可见光照射经过酸洗处理的纸浆，提供了非常高的效率的无氯漂白方法 -13。酸处理可以在pH 1-6和温度为80℃以上的条件下进行。辐射处理可以在至少一种选自还原剂，过氧化物和给氢有机化合物的化合物存在下进行。本发明还提供了在特定的褪色试验中，ISO亮度为88％以上，亮度损失为1.0％以下的高亮度化学纸浆。

2. 发明申请

US20060237153A1 Printing papers 审中-公开
标题翻译：印刷纸
公开(公告)号：US20060237153A1
公开(公告)日：2006-10-26
申请号：US10562788
申请日：2004-06-29
申请人： Takashi Ochi , Shoichi Miyawaki , Akihiko Ouchi
发明人： Takashi Ochi , Shoichi Miyawaki , Akihiko Ouchi
IPC分类号： D21H11/00 , D21H25/00 , D21C9/10
CPC分类号： D21C9/001 , D21H17/63 , D21H25/04
摘要： Printing papers with reduced discoloration are obtained by using a pulp with improved discoloration. Printing papers with remarkably improved discoloration can be obtained by including a pulp consisting of one member or a mixed pulp of two or more members of bleached or unbleached mechanical pulps, semichemical pulps, chemical pulps and deinked pulps irradiated with UV and/or visible light in the presence of at least one additive selected from the group consisting of reducing agents, oxidizing agents and hydrogen-donating organic compounds.
摘要翻译：通过使用具有改进的变色的纸浆获得具有变色变色的印刷纸。可以通过包括由紫外线和/或可见光照射的漂白或未漂白的机械纸浆，半化学纸浆，化学纸浆和脱墨纸浆的两个或更多个成分的一个成员或混合纸浆组成的纸浆来获得显着改善的变色的印刷纸存在至少一种选自还原剂，氧化剂和给氢有机化合物的添加剂。

3. 发明申请

US20060207732A1 Methods for improving discoloration resistance of pulp and pulp improved in discoloration resistance 审中-公开
标题翻译：改善纸浆和纸浆耐变色性的方法提高了耐变色性
公开(公告)号：US20060207732A1
公开(公告)日：2006-09-21
申请号：US10533657
申请日：2003-11-07
申请人： Shoichi Miyawaki , Takashi Ochi , Akihiko Ouchi
发明人： Shoichi Miyawaki , Takashi Ochi , Akihiko Ouchi
IPC分类号： D21C9/00 , D21H11/14
CPC分类号： D21C9/001 , D21C9/1047 , D21H11/20
摘要： The present invention aims to provide a method for improving discoloration in pulp, characterized by a versatile technique adaptable to any type of pulp, a time-saving process, a great and permanent anti-fading effect, environmental friendliness and other properties, as well as a pulp with greatly improved discoloration obtained by said method for improving discoloration. Discoloration in pulp can be greatly improved by adding one or more additives selected from the group consisting of reducing agents, peroxides and hydrogen-donating organic compounds to one of bleached mechanical pulp, semi-chemical pulps, chemical pulp and deinked pulps or a mixture of two or more of them, and irradiating it with UV and/or visible light.
摘要翻译：本发明旨在提供一种改善纸浆变色的方法，其特征在于适用于任何类型纸浆的多用途技术，节省时间的工艺，伟大和永久的防褪色效果，环境友好性等特性，以及通过所述改善变色的方法获得的具有极大改善的变色的纸浆。通过将一种或多种选自还原剂，过氧化物和给氢有机化合物的添加剂添加到漂白机械纸浆，半化学纸浆，化学纸浆和脱墨纸浆中的一种添加剂或混合物中，可以大大提高纸浆中的变色两个或更多个，并用UV和/或可见光照射它们。

4. 发明申请

US20140053828A1 METHOD FOR PRODUCING CELLULOSE NANOFIBERS 有权
标题翻译：生产纤维素纳米纤维的方法
公开(公告)号：US20140053828A1
公开(公告)日：2014-02-27
申请号：US14008682
申请日：2012-03-14
申请人： Shiho Tsuji , Masahiko Fukazawa , Shoichi Miyawaki , Tomoaki Koyanagi
发明人： Shiho Tsuji , Masahiko Fukazawa , Shoichi Miyawaki , Tomoaki Koyanagi
IPC分类号： C08B15/00
CPC分类号： C08B15/00 , C08B15/04 , D01F1/02 , D01F2/02 , D21C9/002 , D21C9/007 , D21H11/18 , D21H11/20
摘要： Cellulose nanofibers are produced by means of a method comprising a step (A) of oxidizing a cellulosic starting material in the presence of an N-oxyl compound and a step (B) of forming the oxidized cellulosic starting material into nanofibers by defibrating the oxidized cellulosic starting material, and a step (C) of performing at least one selected from the following steps: a step (C-1) of treating the cellulosic starting material in water having a hydroxide ion concentration of 0.75 to 3.75 mol/L prior to performing the step (A); and a step (C-2) of subjecting the oxidized cellulosic starting material obtained from the step (A) to hydrolysis in an alkaline solution having a pH between 8 and 14 after performing the step (A) and prior to performing the step (B).
摘要翻译：纤维素纳米纤维通过包括在N-氧基化合物的存在下氧化纤维素原料的步骤（A）的方法和通过将氧化的纤维素纤维素去纤维来形成氧化的纤维素起始材料的步骤（B）起始原料和进行选自以下步骤中的至少一种的步骤（C）：在进行氢氧根离子浓度为0.75〜3.75mol / L的水中处理纤维素原料的工序（C-1）步骤（A）; 以及在进行步骤（A）之后并且在进行步骤（B）之前使由步骤（A）获得的氧化纤维素起始材料在pH为8至14的碱性溶液中水解的步骤（C-2））。

5. 发明申请

US20110112393A1 MAGNETIC RESONANCE IMAGING DEVICE 有权
标题翻译：磁共振成像装置
公开(公告)号：US20110112393A1
公开(公告)日：2011-05-12
申请号：US13054155
申请日：2009-07-22
申请人： Yo Taniguchi , Yoshitaka Bito , Shoichi Miyawaki , Hiroyuki Takeuchi , Suguru Yokosawa
发明人： Yo Taniguchi , Yoshitaka Bito , Shoichi Miyawaki , Hiroyuki Takeuchi , Suguru Yokosawa
IPC分类号： A61B5/055
CPC分类号： G01R33/56518 , A61B5/055 , A61B5/7257 , G01R33/5616 , G01R33/56341 , G01R33/56563
摘要： In the diffusion-weighted imaging, amounts of distortion and amounts of phase offset of k-space data due to a temporally changing magnetic field error induced by eddy currents and vibrations associated with application of a diffusion-weighted gradient magnetic field pulse are corrected with good precision to improve image quality. Characteristic data for correcting distortion of k-space data are calculated for every position in the slice direction as peak shifts of projections observed between the cases of applying and not applying an MPG pulse. As the characteristic data, amounts of distortion in the read-out direction and the phase encoding direction and phase offset amounts in a slice plane are calculated.
摘要翻译：在扩散加权成像中，由于由涡流引起的瞬时变化的磁场误差和与施加扩散加权梯度磁场脉冲相关的振动引起的k空间数据的失真量和相位偏移量被校正为良好精度提高图像质量。针对切片方向上的每个位置计算用于校正k空间数据的失真的特征数据，作为施加和不施加MPG脉冲的情况之间观察到的投影的峰值偏移。作为特征数据，计算读取方向上的失真量和切片平面中的相位编码方向和相位偏移量。

6. 发明授权

US5985367A Process for preparing coated printing paper 失效
标题翻译：涂布印刷纸的制备方法
公开(公告)号：US5985367A
公开(公告)日：1999-11-16
申请号：US152685
申请日：1998-09-14
申请人： Eiji Nishijima , Yuji Sato , Yasunori Nanri , Shoichi Miyawaki
发明人： Eiji Nishijima , Yuji Sato , Yasunori Nanri , Shoichi Miyawaki
IPC分类号： B41M5/52 , C01F11/18 , D21C11/00 , D21H19/38 , B05D3/12 , B05D5/04
CPC分类号： B41M5/5218 , C01F11/18 , D21C11/0078 , D21H19/385 , B41M2205/12 , B41M5/52 , C01P2004/10 , C01P2004/12 , C01P2004/30 , C01P2004/61 , C01P2004/62
摘要： A process for preparing a coated printing paper by applying a coating solution containing a pigment and an adhesive to a base paper, which comprises coating the base paper with the coating solution containing 30 to 90% by weight, based on 100% by weight of pigment components, of rice grain- or spindle-shaped precipitated calcium carbonate as a pigment component, the precipitated calcium carbonate being produced by slaking calcium oxide with a white liquor, followed by causticization with a green liquor, at a causticizing step during pulp production by the sulfate process or the soda process; whereby the coated printing paper free from uneven gloss, mottling, and trapping unevenness, and excellent in ink drying properties and operability with a blade coater is provided.
摘要翻译：一种通过将含有颜料和粘合剂的涂布溶液涂布在原纸上来制备涂布的印刷纸的方法，该方法包括以100重量％的颜料涂覆含有30至90重量％的涂料溶液的原纸作为颜料成分的水稻或锭状沉淀碳酸钙的组分，沉淀的碳酸钙是通过用白液将氧化钙还原，随后用绿液进行苛化，在纸浆生产期间的苛化步骤中通过硫酸盐工艺或苏打工艺; 提供了涂布的印刷纸不受光泽不均匀，斑驳和捕获不均匀性以及油墨干燥性能和刀片涂布机的操作性优异。

7. 发明申请

US20140238626A1 METHOD FOR PRODUCING CELLULOSE NANOFIBERS 有权
标题翻译：生产纤维素纳米纤维的方法
公开(公告)号：US20140238626A1
公开(公告)日：2014-08-28
申请号：US14348791
申请日：2012-09-13
申请人： Shiho Tsuji , Masahiko Fukazawa , Shoichi Miyawaki , Takeshi Iimori
发明人： Shiho Tsuji , Masahiko Fukazawa , Shoichi Miyawaki , Takeshi Iimori
IPC分类号： D21C1/02
CPC分类号： D21C1/02 , C08B15/02 , C08B15/04 , D21C3/02 , D21C3/18 , D21C9/005 , D21C9/007 , D21C9/1036 , D21H11/18 , D21H11/20 , D21H27/10
摘要： Provided is a method which is capable of producing a cellulose nanofiber dispersion liquid that has a low viscosity and excellent fluidity even at a high concentration, while exhibiting excellent transparency. In a method for producing cellulose nanofibers, wherein a cellulosic starting material is oxidized in water using an oxidant in the presence of an N-oxyl compound and a compound that is selected from the group consisting of a bromide, an iodide and a mixture thereof and the thus obtained oxidized cellulose is defibrated and dispersed, pulp which is obtained by carrying out kraft cooking after a hydrolysis process is used as the cellulosic starting material.
摘要翻译：提供一种能够生产即使在高浓度下也具有低粘度和优异流动性同时具有优异透明性的纤维素纳米纤维分散液的方法。在制备纤维素纳米纤维的方法中，其中在N-氧基化合物和选自溴化物，碘化物及其混合物的化合物存在下，使用氧化剂在水中使纤维素原料氧化，由此获得的氧化纤维素被去纤维化和分散，在水解过程之后通过进行硫酸盐蒸煮来获得的纸浆被用作纤维素起始材料。

8. 发明授权

US09365973B2 Method for producing cellulose nanofibers 有权
标题翻译：生产纤维素纳米纤维的方法
公开(公告)号：US09365973B2
公开(公告)日：2016-06-14
申请号：US14348791
申请日：2012-09-13
申请人： Shiho Tsuji , Masahiko Fukazawa , Shoichi Miyawaki , Takeshi Iimori
发明人： Shiho Tsuji , Masahiko Fukazawa , Shoichi Miyawaki , Takeshi Iimori
IPC分类号： D21C9/00 , D21C1/04 , D21C1/02 , D21C9/10 , C08B15/02 , C08B15/04 , D21C3/18 , D21H11/18 , D21H11/20 , D21H27/10 , D21C3/02
CPC分类号： D21C1/02 , C08B15/02 , C08B15/04 , D21C3/02 , D21C3/18 , D21C9/005 , D21C9/007 , D21C9/1036 , D21H11/18 , D21H11/20 , D21H27/10
摘要： Provided is a method which is capable of producing a cellulose nanofiber dispersion liquid that has a low viscosity and excellent fluidity even at a high concentration, while exhibiting excellent transparency. In a method for producing cellulose nanofibers, wherein a cellulosic starting material is oxidized in water using an oxidant in the presence of an N-oxyl compound and a compound that is selected from the group consisting of a bromide, an iodide and a mixture thereof and the thus obtained oxidized cellulose is defibrated and dispersed, pulp which is obtained by carrying out kraft cooking after a hydrolysis process is used as the cellulosic starting material.
摘要翻译：提供一种能够生产即使在高浓度下也具有低粘度和优异流动性同时具有优异透明性的纤维素纳米纤维分散液的方法。在制备纤维素纳米纤维的方法中，其中在N-氧基化合物和选自溴化物，碘化物及其混合物的化合物存在下，使用氧化剂在水中使纤维素原料氧化，由此获得的氧化纤维素被去纤维化和分散，在水解过程之后通过进行硫酸盐蒸煮来获得的纸浆被用作纤维素起始材料。

9. 发明授权

US08865886B2 Method for recovery/reuse of N-oxyl compound 有权
标题翻译： N-氧基化合物的回收/再利用方法
公开(公告)号：US08865886B2
公开(公告)日：2014-10-21
申请号：US13257732
申请日：2010-02-16
申请人： Shoichi Miyawaki , Shiho Katsukawa , Hiroshi Abe , Yuko Iijima , Akira Isogai
发明人： Shoichi Miyawaki , Shiho Katsukawa , Hiroshi Abe , Yuko Iijima , Akira Isogai
IPC分类号： C07D211/00 , C08B16/00 , B01D61/00 , B01D61/42 , C07D211/94 , B01J31/02 , B01J31/40 , C08B15/02
CPC分类号： C07D211/94 , B01J31/0235 , B01J31/40 , B01J2231/70 , C08B15/02 , Y02P20/584
摘要： An effluent produced in oxidation of a cellulosic material with an oxidizing agent in the presence of an N-oxyl compound and a bromide and/or iodide is deionized by electrodialysis to an inorganic salt concentration of less than 0.4%, whereby the N-oxyl compound in the effluent is concentrated and recovered. The N-oxyl compound thus recovered can be reused in oxidation of a cellulosic material. Preferably, the effluent is subjected to reduction treatment and ion exchange resin treatment prior to the electrodialysis.
摘要翻译：在N-氧基化合物和溴化物和/或碘化物的存在下用氧化剂氧化纤维素材料产生的流出物通过电渗析去除，至无机盐浓度小于0.4％，由此N-氧基化合物在流出液中浓缩回收。如此回收的N-氧基化合物可以再次用于纤维素材料的氧化。优选地，在电渗析之前对流出物进行还原处理和离子交换树脂处理。

10. 发明申请

US20120065389A1 METHOD FOR RECOVERY/REUSE OF N-OXYL COMPOUND 有权
标题翻译： N-氧化物的还原/再利用方法
公开(公告)号：US20120065389A1
公开(公告)日：2012-03-15
申请号：US13257732
申请日：2010-02-16
申请人： Shoichi Miyawaki , Shiho Katsukawa , Hiroshi Abe , Yuko Iljima , Akira Isogai
发明人： Shoichi Miyawaki , Shiho Katsukawa , Hiroshi Abe , Yuko Iljima , Akira Isogai
IPC分类号： C07D211/94 , C25B7/00 , C08B16/00
CPC分类号： C07D211/94 , B01J31/0235 , B01J31/40 , B01J2231/70 , C08B15/02 , Y02P20/584
摘要： An effluent produced in oxidation of a cellulosic material with an oxidizing agent in the presence of an N-oxyl compound and a bromide and/or iodide is deionized by electrodialysis to an inorganic salt concentration of less than 0.4%, whereby the N-oxyl compound in the effluent is concentrated and recovered. The N-oxyl compound thus recovered can be reused in oxidation of a cellulosic material. Preferably, the effluent is subjected to reduction treatment and ion exchange resin treatment prior to the electrodialysis.
摘要翻译：在N-氧基化合物和溴化物和/或碘化物的存在下用氧化剂氧化纤维素材料产生的流出物通过电渗析去除，至无机盐浓度小于0.4％，由此N-氧基化合物在流出液中浓缩回收。如此回收的N-氧基化合物可以再次用于纤维素材料的氧化。优选地，在电渗析之前对流出物进行还原处理和离子交换树脂处理。

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