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1. 发明授权

US4395534A Process for producing aromatic polyester carbonate resin 失效
标题翻译：制备芳香族聚酯碳酸酯树脂的方法
公开(公告)号：US4395534A
公开(公告)日：1983-07-26
申请号：US322244
申请日：1981-11-17
申请人： Senzo Shimizu , Isao Nomura , Masahiro Harada , Motohachi Usui , Susumu Taniyama , Shigeo Yanada
发明人： Senzo Shimizu , Isao Nomura , Masahiro Harada , Motohachi Usui , Susumu Taniyama , Shigeo Yanada
IPC分类号： C08G63/64
CPC分类号： C08G63/64
摘要： A process for producing an aromatic polyester carbonate resin in which the molar ratio of the dihydric phenolic compound residue to aromatic dicarboxylic acid residue to carbonate bond is in the range of 2:0.5:1.5-2:1.4:0.6 and these constituent components form an alternating configuration of high regularity, said process comprising a first step wherein in producing a hydroxyl-terminated aromatic oligocarbonate by reacting a dihydric phenolic compound with a halogenated carbonyl compound in a reaction medium consisting of water and a water-immiscible solvent in the presence of a basic inorganic compound, the reaction is carried out by using the basic inorganic compound in an amount of 0.6-1.6 moles per mole of the dihydric phenolic compound and the halogenated carbonyl compound in an amount of 0.3-0.8 mole per mole of the dihydric phenolic compound to form a reaction product mixture consisting predominantly of a phenolic hydroxyl-terminated oligocarbonate of a degree of polymerization of 1-3, and a second step in which an esterification reaction is carried out by reacting the reaction product mixture obtained in the first step with an aromatic dicarboxylic acid dichloride in the presence of a basic inorganic compound in an amount at least sufficient to neutralize the free phenolic hydroxyl groups that remain in the reaction product mixture.
摘要翻译：一种芳族聚酯碳酸酯树脂的制造方法，其中二羟基酚类化合物残基与芳族二羧酸残基与碳酸酯键的摩尔比在2:0.5:1.5-2:1.4:0.6的范围内，并且这些组成成分形成所述方法包括第一步骤，其中通过在由水和水不混溶溶剂组成的反应介质中在二元酚化合物与卤代羰基化合物的反应介质中反应来制备羟基封端的芳族低聚碳酸酯碱性无机化合物，通过使用每摩尔二元酚类化合物和卤代羰基化合物的0.6-1.6摩尔量的碱性无机化合物，其量为每摩尔二羟基酚化合物0.3-0.8摩尔以形成主要由聚合度为酚羟基封端的低聚碳酸酯组成的反应产物混合物为1-3，第二步是在碱性无机化合物存在下使至少足以中和的第一步获得的反应产物混合物与芳族二羧酸二氯化物反应进行酯化反应保留在反应产物混合物中的游离酚羟基。

2. 发明授权

US4278783A Method of curing an organoalkoxysilane compound 失效
标题翻译：固化有机烷氧基硅烷化合物的方法
公开(公告)号：US4278783A
公开(公告)日：1981-07-14
申请号：US72221
申请日：1979-09-04
申请人： Susumu Taniyama , Goro Shimaoka , Shoichi Inoue
发明人： Susumu Taniyama , Goro Shimaoka , Shoichi Inoue
IPC分类号： C08L83/00 , C08G77/00 , C08G77/08 , C08L83/04 , C09D4/00 , C09D183/04 , C08G77/04
CPC分类号： C08G77/08 , C09D4/00
摘要： A method is herein disclosed for curing an organoalkoxysilane compound characterized by using as a catalyst at least one compound selected from the group consisting of a phosphite of the formula:(RO).sub.n P--OH).sub.3-nand a phosphate of the formula: ##STR1## (wherein R is an alkyl group having 1 to 4 carbon atoms and/or an aromatic group; n is an integer of 1 or 2).
摘要翻译：本文公开了一种固化有机烷氧基硅烷化合物的方法，其特征在于使用至少一种选自下式的亚磷酸酯作为催化剂：（RO）n P-OH）3-n的亚磷酸酯和下式的磷酸酯：（其中R为碳原子数为1〜4的烷基和/或芳香族基团，n为1或2的整数）。

3. 发明授权

US4196014A Surface-treating paint for shaped plastic articles 失效
标题翻译：用于成型塑料制品的表面处理涂料
公开(公告)号：US4196014A
公开(公告)日：1980-04-01
申请号：US917025
申请日：1978-06-19
申请人： Susumu Taniyama , Hiromitsu Takanohashi , Shoichi Inoue
发明人： Susumu Taniyama , Hiromitsu Takanohashi , Shoichi Inoue
IPC分类号： C08J7/04 , C09D183/00 , C09D183/04 , C09D183/08 , C09K3/00
CPC分类号： C08J7/047 , C09D183/08 , C08J2483/00
摘要： A surface-treating paint for shaped plastic articles, said paint being the reaction product of(1) 50 to 95 mole % of an epoxyalkylalkoxysilane of the general formula ##STR1## wherein R.sup.1 represents a divalent hydrocarbon group having 1 to 4 carbon atoms, R.sup.2 and R.sup.3 represent a monovalent hydrocarbon group having 1 to 4 carbon atoms, Q represents a glycidoxy or epoxycyclohexyl group, and m is 0 or 1, and(2) 50 to 5 mole % of a fluorinated alcohol of the general formulaH--CF.sub.2 CF.sub.2).sub.p CH.sub.2 OH (II) wherein p is an integer of 1 to 7.The paint may further contain 50 to 5% by weight of the reaction product of (a) 80 to 30 mole % of an epoxyalkylalkoxysilane of general formula (I) with (b) 20 to 70 mole % of an aminoalkylalkoxysilane of the general formula ##STR2## wherein R.sup.1, R.sup.2 and R.sup.3 are as defined with regard to general formula (I), Z represents a hydrogen atom or an aminoalkyl group, and n is 0 or 1, or a partially hydrolyzed product of the reaction product.
摘要翻译：用于成型塑料制品的表面处理涂料，所述涂料是（1）50至95摩尔％的通式为（I）的环氧烷基烷氧基烷氧基硅烷的反应产物，其中R1表示具有1至4个碳原子的二价烃基原子，R2和R3表示碳原子数为1〜4的一价烃基，Q表示缩水甘油氧基或环氧环己基，m为0或1，（2）50〜5摩尔％的通式H的氟化醇 -CF 2 CF 2）p CH 2 OH（II）其中p为1〜7的整数。涂料还可以含有50〜5重量％的（a）80〜30摩尔％的通式（I）的环氧烷基烷氧基烷氧基硅烷的反应产物）与（b）20〜70摩尔％的通式为（III）的氨基烷基烷氧基硅烷，其中R1，R2和R3如通式（I）所定义，Z表示氢原子或氨基烷基，n为0或1，或反应产物的部分水解产物。

4. 发明授权

US4396644A Process for producing aromatic polycarbonate formed articles having coating layer with excellent surface properties 失效
标题翻译：用于制备具有优异表面性质的涂层的芳族聚碳酸酯成型制品的方法
公开(公告)号：US4396644A
公开(公告)日：1983-08-02
申请号：US362261
申请日：1982-03-26
申请人： Susumu Taniyama , Goro Shimaoka , Yukio Maeda , Masuya Ikegami
发明人： Susumu Taniyama , Goro Shimaoka , Yukio Maeda , Masuya Ikegami
IPC分类号： B05D7/02 , C08J7/04 , B05D1/36 , B29D9/00 , B32B27/30 , B32B27/36
CPC分类号： B05D7/02 , B05D7/534 , C08J7/042 , B05D3/0209 , B05D3/0254 , C08J2369/00 , C08J2433/08 , C08J2483/04
摘要： A process for producing a coated aromatic polycarbonate formed article having improved surface properties which comprises forming a primer layer containing a specific thermoplastic acrylic copolymer and an ultraviolet light absorbent on an aromatic polycarbonate formed article, and forming a protective topcoat comprising a thermoset organopolysiloxane on said primed polycarbonate article is disclosed. The coated aromatic polycarbonate formed article has excellent surface properties, such as weather resistance.
摘要翻译：一种制备具有改进的表面性能的涂覆的芳族聚碳酸酯成型制品的方法，包括在芳族聚碳酸酯成型制品上形成含有特定的热塑性丙烯酸共聚物和紫外线吸收剂的底漆层，并在所述涂底漆上形成包含热固性有机聚硅氧烷的保护面漆公开了聚碳酸酯制品。涂覆的芳族聚碳酸酯成型体具有优异的表面性能，如耐候性。

5. 发明授权

US4167537A Surface-treating coating composition for plastic articles 失效
标题翻译：用于塑料制品的表面处理涂料组合物
公开(公告)号：US4167537A
公开(公告)日：1979-09-11
申请号：US869863
申请日：1978-01-16
申请人： Susumu Taniyama , Hiromitsu Takanohashi , Shoichi Inoue
发明人： Susumu Taniyama , Hiromitsu Takanohashi , Shoichi Inoue
IPC分类号： C08J7/04 , C09D161/28 , C09D183/04 , C09D183/08 , C08L61/28 , C08L83/06
CPC分类号： C09D161/28 , C09D183/04 , C09D183/08
摘要： A surface-coating composition for plastic articles, which comprises as a film-forming agent (A) a mixture of the reaction of an aminoalkylalkoxy silane of the general formula ##STR1## WHEREIN R.sup.1 represents a divalent hydrocarbon group containing 1 to 4 carbon atoms, R.sup.2 and R.sup.3 represent a monovalent hydrocarbon group containing 1 to 4 carbon atoms, Z represents a hydrogen atom or an aminoalkyl group, and n is 0 or 1, with an epoxyalkylalkoxy silane of the general formula ##STR2## WHEREIN R.sup.1, R.sup.2 and R.sup.3 are as defined above, Q represents a glycidoxy group ##STR3## or an epoxycyclohexyl group, and m is 0 or 1, and (B) a mixture of an alkyl-modified methylol melamine of the general formula ##STR4## wherein R.sup.4, R.sup.5, R.sup.6, R.sup.7, R.sup.8 and R.sup.9 represent a hydrogen atom or a monovalent hydrocarbon group with 1 to 4 carbon atoms, and an alkyd resin; the amount of component (A) being 45 to 80% by weight, and the amount of component (B) being 20 to 55% by weight, both based on the total amount of components (A) and (B). The composition may further contain (C) an acrylic acid derivative of the general formula ##STR5## wherein R.sup.10 represents a hydrogen atom or a methyl group, and R.sup.11 represents a hydrogen atom, a hydrocarbon group containing 1 to 4 carbon atoms, a hydroxyalkyl group or a glycidyl group, or its polymer of a low degree of polymerization, the amount of component (C) being 5 to 30% by weight based on the total amount of components (A), (B) and (C).
摘要翻译：包括作为成膜剂（A）的通式为“IMAGE”的氨基烷基烷氧基硅烷的反应的混合物的表面涂料组合物，其中R1表示含有1至4个碳原子的二价烃基， R2和R3表示含有1至4个碳原子的一价烃基，Z表示氢原子或氨基烷基，n为0或1，通式为R1，R2和R3的环氧烷基烷氧基硅烷为 Q表示缩水甘油氧基或环氧环己基，m为0或1，（B）通式为“IMAGE”的烷基改性羟甲基三聚氰胺的混合物，其中R4，R5，R6 ，R7，R8和R9表示氢原子或碳原子数为1〜4的一价烃基和醇酸树脂; 组分（A）的量为45至80重量％，组分（B）的量为20至55重量％，均基于组分（A）和（B）的总量。该组合物还可以含有（C）通式“IMAGE”的丙烯酸衍生物，其中R 10表示氢原子或甲基，R 11表示氢原子，含有1至4个碳原子的烃基，羟烷基或缩水甘油基或其低聚合度的聚合物，组分（C）的量相对于组分（A），（B）和（C）的总量为5-30重量％。

6. 发明授权

US4332857A Primer composition and a method for treating a plastics substrate using the same 失效
标题翻译：底漆组合物和使用其的处理塑料基材的方法
公开(公告)号：US4332857A
公开(公告)日：1982-06-01
申请号：US118107
申请日：1980-02-04
申请人： Susumu Taniyama , Goro Shimaoka
发明人： Susumu Taniyama , Goro Shimaoka
IPC分类号： B05D7/02 , C08F299/02 , C08J7/04 , C08J7/16 , C09D183/04 , C12C3/04 , B32B27/30 , C08F220/20
CPC分类号： B05D7/02 , C08F299/026 , C08J7/042 , C08J7/16 , C08J2369/00 , C08J2433/12 , C08J2483/04 , Y10T428/31507 , Y10T428/31663
摘要： A primer composition is prepared by dissolving in an organic solvent one or more diacryloyloxy compounds of the formula: ##STR1## (wherein X is a hydrogen or methyl group; Y is a linear or branched-alkylene group having less than 8 carbon atoms or a binding group selected from the group consisting of ##STR2## n is an integer of from 1 to less than 10). Such primer composition is used as an adhesive inner layer to bond a top-coating finish to a plastic substrate.
摘要翻译：通过在有机溶剂中溶解一种或多种下式的双丙酰氧基化合物制备底漆组合物：其中X为氢或甲基; Y为直链或支链亚烷基， 8个碳原子或选自 n的结合基团是1至小于10的整数）。这种底漆组合物用作粘合剂内层以将顶涂层结合到塑料基材上。

7. 发明授权

US4241116A Method of treating the surfaces of shaped articles of polycarbonate resins 失效
标题翻译：处理聚碳酸酯树脂成型制品表面的方法
公开(公告)号：US4241116A
公开(公告)日：1980-12-23
申请号：US76802
申请日：1979-09-17
申请人： Susumu Taniyama , Goro Shimaoka , Shoichi Inoue
发明人： Susumu Taniyama , Goro Shimaoka , Shoichi Inoue
IPC分类号： B32B27/36 , C08J7/04 , C09D183/00 , C09D183/04 , C09D183/08 , B05D3/02
CPC分类号： C08J7/04 , C09D183/08 , C08J2369/00 , Y10T428/31507 , Y10T428/31511
摘要： A method of treating the surface of a shaped article of a polycarbonate resin, which comprises coating the shaped article of the polycarbonate resin with a specific pre-treating solution (I), air-drying the coated article, then coating the article with a specific coating composition (II), and heat-curing the coated article. The pre-treating solution (I) contains a bisphenol type epoxy resin in a mixed solvent of a lower alcohol and an alkyl ether of ethylene glycol, and the coating composition (II) comprises (A) a reaction mixture of an aminoalkylalkoxy silane of the formula (1) with an epoxyalkylalkoxy silane of the formula (2); (B) a mixture of an alkyl-modified methylol melamine of the formula (3) with an alkyd resin; and (C) an acrylic acid derivative of the formula (5) or its polymer of a low degree of polymerization, the formulas (1), (2), (3) and (5) being given in the claim.
摘要翻译：一种处理聚碳酸酯树脂成型制品表面的方法，包括用特定的预处理溶液（I）涂覆聚碳酸酯树脂的成型制品，将涂覆的制品进行空气干燥，然后用特定的涂料组合物（II），并且对涂覆的制品进行热固化。预处理溶液（I）在低级醇和乙二醇的烷基醚的混合溶剂中含有双酚型环氧树脂，涂料组合物（II）包含（A）氨基烷基烷氧基硅烷的反应混合物式（1）与式（2）的环氧烷基烷氧基硅烷; （B）式（3）的烷基改性羟甲基三聚氰胺与醇酸树脂的混合物; 和（C）式（5）的丙烯酸衍生物或其低聚合度的聚合物，式（1），（2），（3）和（5）在权利要求中给出。

8. 发明授权

US4150068A Flame retardant for synthetic resins 失效
标题翻译：合成树脂阻燃剂
公开(公告)号：US4150068A
公开(公告)日：1979-04-17
申请号：US892026
申请日：1978-03-31
申请人： Susumu Taniyama , Masami Taniguchi
发明人： Susumu Taniyama , Masami Taniguchi
IPC分类号： C07F9/14 , C08G79/04 , C08K5/51 , C08L101/00 , C08K5/49
CPC分类号： C08K5/51 , C07F9/1406 , C08G79/04 , C08L101/00
摘要： Flame retardant for synthetic resins comprising an oligomer having the following structural formula: ##STR1## wherein Y is ##STR2## wherein R.sub.1, R.sub.2, R.sub.3, R.sub.4, R.sub.5 and R.sub.6 are independently H or alkyl of C.sub.1 -C.sub.3, X and X' are independently Br or Cl, A is H or a residue of a terminator selected from the group consisting of phenol, alkylphenol, halo-nucleus-substituted phenol, halo-nucleus-substituted alkylphenol, aniline or halo-nucleus-substituted aniline, B is OH or said residue, m is 1 or 2, and l is integer of from 1 to 10.
摘要翻译：包含具有以下结构式的低聚物的合成树脂的阻燃剂：其中Y是其中R 1，R 2，R 3，R 4，R 5和R 6独立地是H或C 1 -C 3，X和X' 独立地是Br或Cl，A是H或选自苯酚，烷基酚，卤代 - 核取代的苯酚，卤代 - 核 - 取代的烷基酚，苯胺或卤代 - 核 - 取代的苯胺的终止剂的残基，B是 OH或所述残基，m为1或2，l为1至10的整数。

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