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    • 1. 发明授权
    • Joined metal member and a method and an apparatus for fabricating the same
    • 接合的金属构件及其制造方法和装置
    • US06222150B1
    • 2001-04-24
    • US09153455
    • 1998-09-15
    • Seiji NomuraSatoshi NanbaYukio YamamotoYukihiro SugimotoShinya Shibata
    • Seiji NomuraSatoshi NanbaYukio YamamotoYukihiro SugimotoShinya Shibata
    • B23K2000
    • B23K11/34B23K11/20B23K20/16
    • The present invention provides a method for joining two metal members into a joined metal member. The method comprise steps of; applying a brazing material having a higher melting point than both the members on the surface of a first metal member and heating them to form a brazing material on said surface and a braze-diffusion layer under the brazing material in the surface area of the first member; and, then, pressing the first and another second metal members between which the brazing material is interposed during heating at a higher temperature than said melting point of the brazing material to squeeze the molten brazing material out between both the contact surfaces of both the metal members, therefor the two metal members being joined by the braze diffusion layers formed in both the surfaces into the joined metal member. Particularly, the first metal member may comprise an iron-based alloy and the second metal members may comprise an aluminum-based alloy, and the brazing material may be zinc-containing material such as Zn—Al eutectic alloy.
    • 本发明提供一种将两个金属构件接合到接合的金属构件中的方法。 该方法包括以下步骤: 施加具有比第一金属构件表面上的两个构件更高的熔点的钎焊材料,并加热它们以在所述表面上形成钎焊材料,并且在第一构件的表面区域内的钎焊材料下面的钎焊扩散层 ; 然后在比钎焊材料的熔点高的加热温度下挤压钎焊材料插入其中的第一和第二金属构件,以将两个金属构件的两个接触表面之间挤出熔融钎料 因此,两个金属构件通过形成在两个表面中的钎焊扩散层连接到接合的金属构件中。 特别地,第一金属构件可以包括铁基合金,并且第二金属构件可以包括铝基合金,并且钎焊材料可以是诸如Zn-Al共晶合金的含锌材料。
    • 2. 发明授权
    • Metal welding method and metal bonding structure
    • 金属焊接方法和金属结合结构
    • US06552292B1
    • 2003-04-22
    • US09497193
    • 2000-02-03
    • Seiji NomuraSatoshi NanbaYukihiro SugimotoYukio Yamamoto
    • Seiji NomuraSatoshi NanbaYukihiro SugimotoYukio Yamamoto
    • B23K1100
    • B23K1/19B23K11/002B23K20/16B23K20/2275F01L3/22
    • When a seat (3) (FIG. 6A) on which a wax layer (7) is formed via a melting reaction layer (5) is brought into contact with a head (2) and heated and pressed in this state, a melting reaction layer (6) forms below the wax layer (FIG. 6B). When electric current application and pressing are continued from this state, a wax which has not reacted in the wax layer (7) in the formation of the melting reaction layer (6) is discharged from between the melting reaction layers (5) and (6). When electrical current application and pressing are further continued from this state, the two melting reaction layers (5) and (6) diffuse each other. The result is that a ternary alloy bonding layer (10) containing Fe, Al, and Zn, which constitute the melting reaction layers (5) and (6) is formed between the seat (3) and the head (2) (FIG. 6D).
    • 当通过熔融反应层(5)在其上形成蜡层(7)的座(3)(图6A)与头部(2)接触并在该状态下加热和加压时,熔融反应 层(6)形成在蜡层下方(图6B)。 当从该状态继续进行电流施加和加压时,在形成熔融反应层(6)时在蜡层(7)中没有反应的蜡从熔融反应层(5)和(6)之间排出 )。 当从该状态进一步继续进行电流施加和压制时,两个熔融反应层(5)和(6)彼此扩散。 结果是,在座椅(3)和头部(2)之间形成包含构成熔融反应层(5)和(6)的Fe,Al和Zn的三元合金结合层(10)(图3)。 6D)。
    • 3. 发明授权
    • Joined metal member and method of joining said member
    • 接合的金属构件和连接所述构件的方法
    • US06323458B1
    • 2001-11-27
    • US09277167
    • 1999-03-26
    • Seiji NomuraSatoshi Nanba
    • Seiji NomuraSatoshi Nanba
    • B23K1100
    • F01L3/02B23K1/19B23K20/16B23K20/2275
    • In order to provide a method of joining a cylinder head 2 and a valve seat 3 by press and heat generated on passing an electrical current through both members 2, 3, to achieve satisfactory joining with minimized heat generated inside when the current is supplied, while eliminating the need for an infiltration step and reduce the production cost, inhibiting an increase in thermal conductivity of the valve seat 3 and improving the wear resistance thereof. The valve seat 3 is made of a sintered material made from a powdery material with a high electrical conductivity element such as Cu dispersed therein. The current and the pressure are applied with a first joining surface 3a of the valve seat 3 and a joining surface 2a of the cylinder head body 2 being put into surface contact with each other in advance.
    • 为了提供一种通过压制和气门头3连接气缸盖3和通过两个构件2,3使电流产生的热量的方法,以便在供给电流时内部产生的最小化的热量达到令人满意的接合的同时,同时 消除了渗透步骤的需要并降低了生产成本,抑制了阀座3的导热性的提高并提高了其耐磨性。 阀座3由其中分散有诸如Cu的高导电性元素的粉末材料制成的烧结材料制成。 电流和压力被施加有阀座3的第一接合表面3a,并且气缸盖本体2的接合表面2a预先彼此接触。
    • 4. 发明授权
    • Method of separately collecting optically active amino acid amide and optically active amino acid
    • 分别收集光学活性氨基酸酰胺和光学活性氨基酸的方法
    • US07402695B2
    • 2008-07-22
    • US11587006
    • 2005-04-22
    • Atsushi InoueAkinori TanakaSatoshi Nanba
    • Atsushi InoueAkinori TanakaSatoshi Nanba
    • C07C227/00C07C237/00
    • C07C227/38C07C231/24C12P13/04C07C229/08C07C237/06
    • A method for separately collecting an optically active amino acid amide and an optically active amino acid from an aqueous solution containing same, together with at least one member selected from the group consisting of an acid, a base, and a salt, includes a step of neutralizing an acid or base in the aqueous solution, a desalting step of removing a salt contained in the aqueous solution and/or formed in the neutralization step, and a step of separately collecting the optically active amino acid amide/amino acid separately from the desalted aqueous solution by a process which takes advantage of a difference in solubility between the two components in an organic solvent. The desalting step is preferably performed by electrodialysis, optionally with ammonia added to the aqueous solution. The optically active amino acid amide/amino acid can be separately collected with high efficiency using an organic solvent.
    • 从含有该光学活性氨基酸酰胺和光学活性氨基酸的水溶液中分别收集选自酸,碱和盐中的至少一种的方法,包括以下步骤: 中和水溶液中的酸或碱,除去水溶液中所含的盐和/或中和步骤中形成的盐的脱盐步骤,以及与脱盐的分开收集光学活性氨基酸酰胺/氨基酸的步骤 水溶液,其通过利用有机溶剂中两种组分之间的溶解度差异的方法。 脱盐步骤优选通过电渗析任选地加入到水溶液中进行。 可以使用有机溶剂以高效率单独收集光学活性氨基酸酰胺/氨基酸。
    • 5. 发明申请
    • Method of Separating and Collecting Optically Active Amino Acid Amide
    • 分离收集光活性氨基酸酰胺的方法
    • US20090318730A1
    • 2009-12-24
    • US11912107
    • 2006-04-21
    • Masaki SugitaSatoshi NanbaAkinori Tanaka
    • Masaki SugitaSatoshi NanbaAkinori Tanaka
    • C07C227/40
    • C07C231/24C07B2200/07C07C233/05
    • [Problems] To provide a method for efficiently separating and collecting an optically active amino acid amide and an optically active amino acid which are highly important substances as intermediates in the production of various industrial chemicals, agricultural chemicals, and pharmaceuticals, from an aqueous solution containing the optically active amino acid amide and the optically active amino acid.[Means for Solving Problems] In separating and collecting an optically active amino acid amide from an aqueous solution containing the optically active amino acid amide and an optically active amino acid by a process utilizing a difference in solubility in an organic solvent between the optically active amino acid amide and the optically active amino acid, the separation/collection procedures are carried out, without desalting the aqueous solution or after desalting the same, under such a condition that a ratio (C/A) of the total equivalent (C) of cations to the total equivalent (A) of anions contained in the aqueous solution falls within the range from 0.95 to 1.05 when the aqueous solution is not desalted, and the range from 0.5 to 1.5 when the aqueous solution is desalted.
    • [问题]提供一种高效分离和收集作为制备各种工业化学品,农药和药物的高度重要物质作为中间体的旋光氨基酸酰胺和光学活性氨基酸的方法,该方法含有 光学活性氨基酸酰胺和光学活性氨基酸。 解决问题的手段在通过使用在光学活性氨基酸的有机溶剂中的溶解度差异的方法从含有光学活性氨基酸酰胺和光学活性氨基酸的水溶液中分离并收集光学活性氨基酸酰胺 酸酰胺和光学活性氨基酸,在不脱盐水溶液或脱盐的情况下,在阳离子的总当量(C)的比例(C / A)的条件下进行分离/收集步骤 当水溶液不脱盐时,水溶液中含有的阴离子的总当量(A)为0.95〜1.05,水溶液脱盐时为0.5〜1.5。
    • 9. 发明授权
    • Method of separating and collecting optically active amino acid amide
    • 分离和收集光学活性氨基酸酰胺的方法
    • US08178725B2
    • 2012-05-15
    • US11912107
    • 2006-04-21
    • Masaki SugitaSatoshi NanbaAkinori Tanaka
    • Masaki SugitaSatoshi NanbaAkinori Tanaka
    • C07C237/06
    • C07C231/24C07B2200/07C07C233/05
    • A method for efficiently separating and collecting an optically active amino acid amide and an optically active amino acid from an aqueous solution containing the optically active amino acid amide and the optically active amino acid includes separating and collecting an optically active amino acid amide from an aqueous solution containing the optically active amino acid amide and an optically active amino acid, utilizing a difference in solubility in an organic solvent between the optically active amino acid amide and the optically active amino acid, without desalting the aqueous solution or after desalting the same, under such a condition that a ratio (C/A) of the total equivalent (C) of cations to the total equivalent (A) of anions contained in the aqueous solution falls within the range from 0.95 to 1.05 when the aqueous solution is not desalted, and the range from 0.5 to 1.5 when the aqueous solution is desalted.
    • 从含有光学活性氨基酸酰胺和光学活性氨基酸的水溶液中有效分离和收集光学活性氨基酸酰胺和光学活性氨基酸的方法包括从水溶液中分离和收集光学活性氨基酸酰胺 含有光学活性氨基酸酰胺和光学活性氨基酸,利用光学活性氨基酸酰胺和光学活性氨基酸之间在有机溶剂中的溶解度差异,不脱盐水溶液或脱盐后, 当水溶液不脱盐时,水溶液中含有的阳离子的总当量(C)与阴离子的总当量(A)的比(C / A)在0.95〜1.05的范围内的条件,以及 当水溶液脱盐时,范围为0.5至1.5。