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    • 3. 发明授权
    • Toner for developing electrostatic images and process for production
thereof
    • 用于显影静电图像的调色剂及其生产方法
    • US5840459A
    • 1998-11-24
    • US662081
    • 1996-06-12
    • Manabu OhnoSatoshi MitsumuraNobuyuki OkuboYoshinori Tsuji
    • Manabu OhnoSatoshi MitsumuraNobuyuki OkuboYoshinori Tsuji
    • G03G9/08G03G9/087G03G9/097
    • G03G9/0821G03G9/08711G03G9/08782G03G9/08797G03G9/09783
    • A toner for developing electrostatic images, includes toner particles and 10-500 isolated low-molecular weight wax particles per 10,000 toner particles. The toner has a melt index as measured at 125.degree. C. under a load of 98 N of at least 10. The toner particles comprise at least a binder resin, a colorant and the low-molecular weight wax. The low-molecular weight wax comprises a compound represented by the formula of: R--Y, wherein R denotes a hydrocarbon group, and Y denotes a hydroxyl group, carboxyl group, alkyl ether group or alkyl ester group. The low-molecular weight wax has a thermal property providing a DSC curve as measured by a differential scanning calorimeter exhibiting: (i) a maximum heat-absorption peak having a peak temperature in a temperature range of 70.degree.-130.degree. C.; (ii) a heat-absorption peak including the maximum heat-absorption peak showing an onset temperature of at least 50.degree. C., and (iii) a maximum heat-evolution peak in a range of .+-.15.degree. C. from the peak temperature of the maximum hat-absorption peak. The toner shows a good fixability while retaining a good productivity through the melt-kneading-pulverization process.
    • 用于显影静电图像的调色剂包括每10,000个调色剂颗粒中的调色剂颗粒和10-500个分离的低分子量蜡颗粒。 该调色剂在125℃负载下测定的熔体指数为98N至少为10.调色剂颗粒至少包含粘合剂树脂,着色剂和低分子量蜡。 低分子量蜡包括由下式表示的化合物:R-Y,其中R表示烃基,Y表示羟基,羧基,烷基醚基或烷基酯基。 低分子量蜡具有提供通过差示扫描量热计测量的DSC曲线的热性质,其显示出:(i)峰值温度在70℃-130℃的最大吸热峰; (ii)包括显示起始温度至少为50℃的最大吸热峰的热吸收峰,和(iii)在+/- 15℃范围内的最大放热峰 最高帽吸收峰的峰值温度。 调色剂通过熔融捏合粉碎过程保持良好的生产率,显示出良好的定影性。
    • 4. 发明授权
    • Surface treating apparatus for solid particles, surface treating method
therefor and method for producing toner
    • 固体颗粒表面处理装置及其表面处理方法及调色剂的制造方法
    • US5865381A
    • 1999-02-02
    • US902327
    • 1997-07-29
    • Satoshi MitsumuraToshinobu OhnishiYoshinori Tsuji
    • Satoshi MitsumuraToshinobu OhnishiYoshinori Tsuji
    • G03G9/087B01J2/00B01J2/10B02C13/18B02C13/282G03G9/08B02C13/00B02C13/28
    • B01J2/10B01J2/006G03G9/0802
    • An apparatus for treating the surfaces of solid particles has at least a first cylindrical treating chamber and a rotary shaft and a first rotor having two or more blades on its front face, contained in the first cylindrical treating chamber. A powder charging aperture for introducing the solid particles into the first cylindrical treating chamber together with gas is provided at the center of the front wall of the first cylindrical treating chamber, opposed to the front face of the first rotor. A first powder discharging aperture for discharging the treated solid particles is provided at the center of the rear wall of the first cylindrical treating chamber, opposed to the rear face of the first rotor. The first rotor is connected with the rotary shaft and rotated by the rotation of the rotary shaft. The height H.sub.a of the blades, the gap L.sub.1a between the tip of each of the blades and the front wall, the largest diameter R.sub.1a of the first rotor and the gap L.sub.2a between the blades and the sidewall of the first cylindrical treating chamber satisfy the following conditions:0.1.ltoreq.L.sub.1a /H.sub.a .ltoreq.5.0, 50.times.10.sup.-3 .ltoreq.H.sub.a /R.sub.1a .ltoreq.400.times.10.sup.-3 and 1.0.times.10.sup.-3 .ltoreq.L.sub.2a /R.sub.1a .ltoreq.95.times.10.sup.-3.
    • 用于处理固体颗粒表面的装置具有至少第一圆柱形处理室和旋转轴以及在其前表面上具有两个或更多个叶片的第一转子,该第一转子包含在第一圆柱形处理室中。 在与第一转子的前表面相对的第一圆柱形处理室的前壁的中心处设置用于将固体颗粒与气体一起引入第一圆柱形处理室的粉末填充孔。 在第一圆筒形处理室的后壁的与第一转子的后表面相对的中心处设置有用于排出经处理的固体颗粒的第一粉末排放孔。 第一转子与旋转轴连接并通过旋转轴的旋转而旋转。 叶片的高度Ha,每个叶片的前端和前壁之间的间隙L1a,第一转子的最大直径R1a和叶片与第一圆柱形处理室的侧壁之间的间隙L2a满足以下 条件:0.1
    • 7. 发明授权
    • Pneumatic impact pulverizer and process for producing toner
    • 气动冲击式粉碎机及其制造方法
    • US5934575A
    • 1999-08-10
    • US995901
    • 1997-12-22
    • Toshinobu OhnishiSatoshi MitsumuraYoshinori Tsuji
    • Toshinobu OhnishiSatoshi MitsumuraYoshinori Tsuji
    • B02C19/06
    • B02C19/066
    • A pneumatic impact pulverizer is disclosed which has a nozzle for feeding high-pressure gas, a tube for transporting and accelerating a pulverizing material, a pulverization chamber, and an impact member for pulverizing the material. The impact member is opposed to an outlet of the accelerating tube and has at least a first impact face projecting toward the accelerating tube side and a second impact face sloped toward the downstream side. The pulverization chamber has at least a first sidewall positioned on the side more upstream than the outermost edge of the second impact face and a second sidewall positioned on the downstream side of the first sidewall. The pulverization chamber is enlarged at its part on the side more upstream than the outermost edge of the second impact face so that the cross-sectional area of the inside of the chamber at that part is larger than that of the inside of the chamber corresponding to the outermost edge of the second impact face. The tip of the first impact face is positioned on the side more upstream than the downstream side edge of the first sidewall. The pulverization can be conducted in a very high efficiency with the pulverizer. Also, a process for producing a toner for developing electrostatic images using the pulverizer is disclosed.
    • 公开了一种气动冲击式粉碎机,其具有用于供给高压气体的喷嘴,用于输送和加速粉碎材料的管,粉碎室和用于粉碎材料的冲击构件。 撞击构件与加速管的出口相对,并且至少具有朝向加速管侧突出的第一冲击面和朝向下游侧倾斜的第二冲击面。 粉碎室具有至少第一侧壁,其位于比第二冲击面的最外边缘更上游的一侧,以及位于第一侧壁的下游侧的第二侧壁。 粉碎室在其比第二冲击面的最外边缘更上游的一侧的部分被扩大,使得该部分的室内部的横截面面积大于对应于室的室的内部的横截面积 第二冲击面的最外边缘。 第一冲击面的尖端位于比第一侧壁的下游侧边缘更上游的一侧。 粉碎机可以以非常高的效率进行粉碎。 此外,公开了使用粉碎机制造用于显影静电图像的调色剂的方法。
    • 10. 发明授权
    • Process for producing toner
    • 生产调色剂的方法
    • US06309788B1
    • 2001-10-30
    • US09433559
    • 1999-11-04
    • Yoshinori TsujiAtsushi KuboMinoru OhmuraHitoshi KandaTakeshi Tsujino
    • Yoshinori TsujiAtsushi KuboMinoru OhmuraHitoshi KandaTakeshi Tsujino
    • G03G908
    • G03G9/0806B01F7/00816
    • A process for producing a toner. The process has the steps of dispersing a fine-particle colorant in a liquid monomer mixture containing at least a liquid polymerizable monomer, dispersing the resulting colorant-dispersed liquid monomer mixture in an aqueous dispersion medium to form particles of a polymerizable monomer composition, and polymerizing polymerizable monomers present in the particles in the aqueous dispersion medium to form toner particles. In the dispersion step, a media particle agitation type wet-dispersion machine is used as a dispersion means. The dispersion machine has a cylindrical vessel having a first wall surface having a liquid-feed opening and a second wall surface having a liquid-discharge opening. The vessel is inside provided with an inner chamber and an outer chamber which are partitioned with a cylindrical separator having slits, a rotor set in the inner chamber rotatably by the rotary drive motion of a drive shaft, and a plurality of spherical media particles held in the inner chamber.
    • 调色剂的制造方法。 该方法具有以下步骤:将细颗粒着色剂分散在至少含有液体可聚合单体的液体单体混合物中,将得到的着色剂分散液体单体混合物分散在水性分散介质中以形成可聚合单体组合物的颗粒,并聚合 存在于水分散介质中的颗粒中的可聚合单体以形成调色剂颗粒。 在分散步骤中,使用介质颗粒搅拌型湿式分散机作为分散装置。 分散机具有圆柱形容器,其具有具有供液口的第一壁表面和具有排液口的第二壁表面。 内部具有内室和外室,其分隔开具有狭缝的圆柱形分离器,通过驱动轴的旋转驱动运动可旋转地设置在内室中的转子和保持在 内室。