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1. 发明授权

US5976752A Toner and image forming method 有权
标题翻译：调色剂和成像方法
公开(公告)号：US5976752A
公开(公告)日：1999-11-02
申请号：US135167
申请日：1998-08-18
申请人： Satoshi Matsunaga , Koichi Tomiyama , Yuichi Mizoh , Keita Nozawa , Minekazu Endo , Tadashi Doujo , Yoshihiro Ogawa , Nene Shibayama
发明人： Satoshi Matsunaga , Koichi Tomiyama , Yuichi Mizoh , Keita Nozawa , Minekazu Endo , Tadashi Doujo , Yoshihiro Ogawa , Nene Shibayama
IPC分类号： G03G9/087 , G03G9/097 , G03G13/22
CPC分类号： G03G9/08755 , G03G9/087 , G03G9/08702 , G03G9/08711 , G03G9/08728 , G03G9/08797
摘要： An electrophotographic toner is composed of at least a binder resin, a colorant, and a wax. The binder resin (a) comprises a polyester resin, a vinyl resin and a hybrid resin component comprising a polyester unit and a vinyl polymer unit, (b) has a THF (tetrahydrofuran)-soluble content (W1) of 50-85 wt. % and a THF-insoluble content (W2) of 5-50 wt. %, an ethyl acetate-soluble content (W3) of 40-98 wt. % and an ethyl acetate-insoluble content (W4) of 2-60 wt. %, a chloroform-soluble content (W5) of 55-90 wt. % and a chloroform-insoluble content (W6) of 10-45 wt. %, respectively after 10 hours of Soxhlet extraction with respective solvents, giving a ratio W4/S6 of 1.1-4.0, and contains a THF-soluble content providing a GPC (gel permeation chromatography) chromatogram exhibiting a main peak in a molecular weight range of 4000-9000, including 35.0-65.0% (A1) of a component haing molecular weights in a range of 500 to below 1.times.10.sup.4, 25.0-45.0% (A2) of a component having molecular weights in a range of 1.times.10.sup.4 to below 1.times.10.sup.5 and 10.0-30.0% (A3) of a component having molecular weights of at least 1.times.10.sup.5 giving a ratio A1/A2 of 1.05-2.00. The binder resin shows good dispersibility of wax and colorant.
摘要翻译：电子照相调色剂由至少粘合剂树脂，着色剂和蜡组成。粘合剂树脂（a）包括聚酯树脂，乙烯基树脂和包含聚酯单元和乙烯基聚合物单元的混合树脂组分，（b）具有50-85重量％的THF（四氢呋喃） - 可溶成分（W1）％和THF不溶物含量（W2）为5-50wt。％，40-98重量％的乙酸乙酯可溶物含量（W3）％，乙酸乙酯不溶物含量（W4）为2-60wt。％，55-90重量％的氯仿可溶物含量（W5）％，氯仿不溶物含量（W6）为10-45wt。％，分别用各自的溶剂提取索氏提取10小时后，得到比例W4 / S6为1.1-4.0，并含有THF可溶性成分，提供在分子量范围内显示主峰的GPC（凝胶渗透色谱）色谱图 4000-9000，包括分子量在500至低于1×10 4范围内的分子量为35.0-65.0％（A1），分子量为1×104至低于1×10 5的组分的25.0-45.0％（A2）和10.0 -30.0％（A3）的分子量为至少1×10 5的组分，其A1 / A2比为1.05-2.00。粘合剂树脂表现出良好的蜡和着色剂的分散性。

2. 发明授权

US06232027B1 Toner having negative triboelectric chargeability and image forming method 有权
标题翻译：具有负摩擦带电性和图像形成方法的调色剂
公开(公告)号：US06232027B1
公开(公告)日：2001-05-15
申请号：US09318776
申请日：1999-05-26
申请人： Satoshi Matsunaga , Toshiaki Nakahara , Yuichi Mizoh , Hirohide Tanikawa , Minekazu Endo , Tadashi Doujo , Nene Shibayama
发明人： Satoshi Matsunaga , Toshiaki Nakahara , Yuichi Mizoh , Hirohide Tanikawa , Minekazu Endo , Tadashi Doujo , Nene Shibayama
IPC分类号： G03G9087
CPC分类号： G03G9/09783 , G03G9/08755 , G03G9/08782 , G03G9/08793 , G03G9/09741 , G03G9/0975
摘要： A toner having a negative triboelectric chargeability is constituted by at least a binder resin, a colorant and an organic metal compound. The toner is characterized by: (a) the organic metal compound is an organic zirconium compound comprising a coordination or/and a bonding of zirconium and an aromatic compound as a ligand or/and an acid source selected from the group consisting of aromatic diols, aromatic hydroxycarboxylic acids, aromatic monocarboxylic acids, and aromatic polycarboxylic acids, (b) the binder resin is a resin selected from the group consisting of (i) a polyester resin and (ii) a hybrid resin component comprising a polyester unit and a vinyl polymer unit, (c) the binder resin has an acid value of 2-50 mgKOH/g, and (d) the toner contains a TFT (tetrahydrofuran)-soluble content providing a GPC (gel permeation chromatography) chromatogram exhibiting a main peak in a molecular weight range of 3,000-20,000 and including 3-25% of a component having molecular weights of at least 5×105.
摘要翻译：具有负摩擦带电性的调色剂至少由粘合剂树脂，着色剂和有机金属化合物构成。调色剂的特征在于：（a）有机金属化合物是一种有机锆化合物，其包含锆和作为配体的芳族化合物的配位或/和键合，和/或选自芳族二醇，（b）粘合剂树脂是选自（i）聚酯树脂和（ii）包含聚酯单元和乙烯基聚合物的杂化树脂组分的树脂中的一种树脂单元，（c）粘合剂树脂的酸值为2-50mgKOH / g，（d）调色剂含有提供GPC（凝胶渗透色谱）色谱的TFT（四氢呋喃） - 可溶性含量，分子量范围为3,000-20,000，并且包括3-25％的分子量至少为5×10 5的成分。

3. 发明授权

US06593052B2 Toner, image forming method and process cartridge 有权
公开(公告)号：US06593052B2
公开(公告)日：2003-07-15
申请号：US09915331
申请日：2001-07-27
申请人： Junko Yoshikawa , Yuichi Mizoo , Satoshi Matsunaga , Tadashi Dojo , Nene Shibayama , Ryota Kashiwabara
发明人： Junko Yoshikawa , Yuichi Mizoo , Satoshi Matsunaga , Tadashi Dojo , Nene Shibayama , Ryota Kashiwabara
IPC分类号： G03G9087
CPC分类号： G03G9/08797 , G03G9/08704 , G03G9/08708 , G03G9/08711 , G03G9/08755 , G03G9/08771 , G03G9/08784 , G03G9/08795
摘要： A toner containing toner particles and an inorganic fine powder; the toner particles containing at least a binder resin, a colorant, a sulfur-containing resin, and a wax; the binder resin containing a hybrid resin component containing a vinyl type polymer unit and a polyester unit, and the sulfur-containing resin being a resin selected from the group consisting of sulfur-containing polymers and sulfur-containing copolymers

4. 发明授权

US06703176B2 Toner, process for producing toner image forming method and apparatus unit 有权
标题翻译：调色剂，调色剂成像方法和设备单元的制造方法
公开(公告)号：US06703176B2
公开(公告)日：2004-03-09
申请号：US10152776
申请日：2002-05-23
申请人： Takeshi Naka , Yuichi Mizoo , Satoshi Matsunaga , Masami Azuma , Takashige Kasuya , Tadashi Dojo , Tsuneo Nakanishi , Nene Shibayama , Katsuhisa Yamazaki , Yusuke Hasegawa
发明人： Takeshi Naka , Yuichi Mizoo , Satoshi Matsunaga , Masami Azuma , Takashige Kasuya , Tadashi Dojo , Tsuneo Nakanishi , Nene Shibayama , Katsuhisa Yamazaki , Yusuke Hasegawa
IPC分类号： G03G9087
CPC分类号： G03G9/0827 , G03G9/0802 , G03G9/081 , G03G9/0817 , G03G9/0819
摘要： A toner contains at least a bonding resin and a coloring agent, and has a weight mean particle size from 5 &mgr;m to 12 &mgr;m; not less than 90% by number of particles not less than 3 &mgr;m have a circularity “a” not less than 0.900; a cut ratio Z and a weight mean size X of the toner are related as: cut ratio Z≦5.3×X; and a relationship of particles Y having a circularity of not less than 0.950 and a weight mean size X is Y≧e5.51×X−0.645 where X is 5 to 12 &mgr;m.
摘要翻译：调色剂至少含有粘合树脂和着色剂，其重均粒径为5〜12μm; 不少于90％的不小于3μm的颗粒具有不小于0.900的圆形度“a”。调色剂的切割比Z和重量平均尺寸X相关：切割比Z <= 5.3×X; 并且具有不小于0.950的圆形度和重量平均尺寸X的颗粒Y的关系为Y> = e <5.51> xX <-0.645>其中X为5至12μm。

5. 发明授权

US06586151B1 Toner, process for producing toner image forming method and apparatus unit 有权
标题翻译：调色剂，调色剂成像方法和设备单元的制造方法
公开(公告)号：US06586151B1
公开(公告)日：2003-07-01
申请号：US09679554
申请日：2000-10-06
申请人： Takeshi Naka , Yuichi Mizoo , Satoshi Matsunaga , Masami Azuma , Takashige Kasuya , Tadashi Dojo , Tsuneo Nakanishi , Nene Shibayama , Katsuhisa Yamazaki , Yusuke Hasegawa
发明人： Takeshi Naka , Yuichi Mizoo , Satoshi Matsunaga , Masami Azuma , Takashige Kasuya , Tadashi Dojo , Tsuneo Nakanishi , Nene Shibayama , Katsuhisa Yamazaki , Yusuke Hasegawa
IPC分类号： G03G908
CPC分类号： G03G9/0827 , G03G9/0802 , G03G9/081 , G03G9/0817 , G03G9/0819
摘要： A toner manufacturing method includes grinding and classification to produce a toner containing a binder resin and a colorant with a weight mean particle size of 5 microns to 12 microns and sharp particle density distribution. The toner has a specific circularity, relationship between cut ratio and weight mean size, and relationship between circularity and weight mean size as disclosed in the specification.
摘要翻译：调色剂制造方法包括研磨和分级以产生包含粘合剂树脂和着色剂的调色剂，其重均粒径为5微米至12微米，并具有尖锐的颗粒密度分布。调色剂具有特定的圆形度，切割比和重量平均尺寸之间的关系以及圆形度和重量平均尺寸之间的关系，如说明书中所公开的。

6. 发明授权

US06613490B2 Toner, image forming method and process-cartridge 有权
公开(公告)号：US06613490B2
公开(公告)日：2003-09-02
申请号：US09984118
申请日：2001-10-29
申请人： Satoshi Matsunaga , Yuichi Mizoh , Junko Yoshikawa , Ryota Kashiwabara
发明人： Satoshi Matsunaga , Yuichi Mizoh , Junko Yoshikawa , Ryota Kashiwabara
IPC分类号： G03G908
CPC分类号： G03G9/0821 , G03G9/08704 , G03G9/08755 , G03G9/08782 , G03G9/08795 , G03G9/08797 , G03G9/09716 , G03G9/09725
摘要： A toner exhibiting good balance of low-temperature fixability, an anti-offset characteristic and a developing performance in continuous image formation is formed of at least a binder resin, a colorant and a wax. The toner exhibits a dielectric loss tangent showing a maximum of 6.0×10−2 to 10.0×10−2 in a temperature range of 90 to 125° C. The toner provides a DSC curve showing at least one heat-absorption peak or shoulder in a temperature range of 85 to 140° C. on temperature increase according to differential scanning calorimetry (DSC). The binder resin comprises a hybrid resin having a vinyl polymer unit and a polyester unit.

7. 发明授权

US6040103A Toner for developing electrostatic image and image forming method 失效
标题翻译：用于显影静电图像和图像形成方法的调色剂
公开(公告)号：US6040103A
公开(公告)日：2000-03-21
申请号：US921565
申请日：1997-09-02
申请人： Manabu Ohno , Takeshi Ohtake , Satoshi Matsunaga , Tadashi Doujo
发明人： Manabu Ohno , Takeshi Ohtake , Satoshi Matsunaga , Tadashi Doujo
IPC分类号： G03G9/087 , G03G9/097 , G03G13/22
CPC分类号： G03G9/08782
摘要： A toner for developing an electrostatic image is composed of toner particles each containing at least a binder resin, a colorant, and a wax. The wax satisfies conditions of:(a) showing a maximum heat-absorption peak in a region of 50-130.degree. C. on temperature increase on a DSC (differential scanning calorimeter) curve, and(b) giving a .sup.13 C-NMR (nuclear magnetic resonance) spectrum showing a total peak area S in a range of 0-50 ppm, a total peak area S1 in a range of 36-42 ppm and a total peak area S2 in a range of 10-17 ppm satisfying:1.0.ltoreq.(S1/S).times.100.ltoreq.10, 1.5.ltoreq.(S2/S).times.100.ltoreq.15, and S1
摘要翻译：用于显影静电图像的调色剂由至少包含粘合剂树脂，着色剂和蜡的调色剂颗粒组成。蜡满足以下条件：（a）在DSC（差示扫描量热计）曲线上升温时，在50-130℃区域显示最大吸热峰，（b）给出13 C-NMR（核磁共振）光谱，其总峰面积S在0-50ppm的范围内，总峰面积S1在36-42ppm范围内，总峰面积S2在10-17ppm的范围内满足：1.0 < 满足上述条件的蜡具有适当分支的长链结构，并且提供了（S1 / S）×100

8. 发明授权

US5955234A Toner for developing electrostatic image, and image forming method 失效
标题翻译：用于显影静电图像的调色剂和图像形成方法
公开(公告)号：US5955234A
公开(公告)日：1999-09-21
申请号：US947273
申请日：1997-10-08
申请人： Satoshi Matsunaga , Manabu Ohno , Tadashi Doujo
发明人： Satoshi Matsunaga , Manabu Ohno , Tadashi Doujo
IPC分类号： C08F257/00 , C08F265/06 , G03G9/08 , G03G9/087
CPC分类号： C08F257/00 , C08F265/06 , G03G9/081 , G03G9/08711 , G03G9/08782 , G03G9/08788 , G03G9/08795 , G03G9/08797
摘要： A toner for developing an electrostatic image is comprised of a binder resin, a colorant and a wax. The toner has the following rheological characteristics: (a) a temperature at which the ratio of a loss elastic modulus to a storage elastic modulus (G"/G'=tan .delta.) comes to be 1.0 is present in a temperature range of from 55.degree. C. to 70.degree. C., with an elastic modulus being 1.5.times.10.sup.8 Pa or below; (b) the ratio of the storage elastic modulus at a temperature of 40.degree. C. (G'.sub.40) to the storage elastic modulus at a temperature of 50.degree. C. (G'.sub.50), G'.sub.40 /G'.sub.50, is from 1.5 to 5.0; (c) the ratio of the storage elastic modulus at a temperature of 50.degree. C. (G'.sub.50) to the storage elastic modulus at a temperature of 60.degree. C. (G'.sub.60), G'.sub.50 /G'.sub.60, is from 3 to 20; (d) the ratio of the storage elastic modulus at a temperature of 70.degree. C. (G'.sub.70) to the storage elastic modulus at a temperature of 100.degree. C. (G'.sub.100), G'.sub.70 /G'.sub.100, is from 50 to 250; and (e) the ratio of the storage elastic modulus at a temperature of 110.degree. C. (G'.sub.110) to the storage elastic modulus at a temperature of 140.degree. C. (G'.sub.140), G'.sub.110 /G'.sub.140, is from 2 to 20.
摘要翻译：用于显影静电图像的调色剂由粘合剂树脂，着色剂和蜡组成。调色剂具有以下流变特性：（a）在下述的温度范围内存在损耗弹性模量与储能弹性模量（G“/ G'=tanδ）的比率为1.0的温度 55℃至70℃，弹性模量为1.5×10 8 Pa或更低; （b）在温度为40℃（G'40）下的储能弹性模量与50℃温度（G'50），G'40 / G'50，为1.5〜5.0; （c）温度为50℃（G'50）的储能弹性模量与60℃温度（G'60），G'50 / G'60，从3到20; （d）温度为70℃（G'70）时的储能弹性模量与100℃（G'100），G'70 / G'100的储能弹性模量的比率，从50到250; 和（e）温度为110℃（G'110）时的储能弹性模量与140℃温度下的储能弹性模量（G'140），G'110 / G'140 是从2到20。

9. 发明授权

US6156470A Toner having negative triboelectric chargeability and image forming method 有权
标题翻译：具有负摩擦带电性和图像形成方法的调色剂
公开(公告)号：US6156470A
公开(公告)日：2000-12-05
申请号：US362221
申请日：1999-07-28
申请人： Satoshi Matsunaga , Hirohide Tanikawa , Minekazu Endo
发明人： Satoshi Matsunaga , Hirohide Tanikawa , Minekazu Endo
IPC分类号： G03G9/087 , G03G9/097 , G03G13/22
CPC分类号： G03G9/09783 , G03G9/08795
摘要： A toner having a negative triboelectric chargeability is constituted by at least a binder resin, a colorant, a wax and an organic metal compound. The toner is characterized in that: (a) the toner has an acid value of 5-35 mgKOH/g, (b) the binder resin comprises a vinyl polymer, (c) the binder resin in the toner contains a chloroform-insoluble content in an amount of 3-50 wt. %, (d) the toner contains a THF (tetrahydrofuran)-soluble content providing a GPC (gel permeation chromatography) chromatogram exhibiting a main peak in a molecular weight range of 5,000-30,000 and at least one sub-peak and/or shoulder in a molecular weight range of 2.times.10.sup.5 -15.times.10.sup.5 and including 15-70% of a component having molecular weights of 1.times.10.sup.4 -10.times.10.sup.4, and (e) the organic metal compound is an organic zirconium compound comprising a coordination or/and a bonding of zirconium and an aromatic compound as a ligand or/and an acid source selected from the group consisting of aromatic diols, aromatic hydroxycarboxylic acids, aromatic monocarboxylic acids, and aromatic polycarboxylic acids.
摘要翻译：具有负摩擦带电性的调色剂至少由粘合剂树脂，着色剂，蜡和有机金属化合物构成。调色剂的特征在于：（a）调色剂的酸值为5-35mgKOH / g，（b）粘合剂树脂包含乙烯基聚合物，（c）调色剂中的粘合剂树脂含有氯仿不溶物含量其量为3-50wt。％，（d）调色剂含有THF（四氢呋喃） - 可溶成分，其提供GPC（凝胶渗透色谱）色谱图，其显示分子量范围为5,000-30,000的主峰和至少一个亚峰和/或肩峰分子量范围为2×105-15×105，包括15-70％的分子量为1×10 4 -10×10 4的组分，和（e）有机金属化合物是一种有机锆化合物，其包含锆和/ 芳族化合物作为配体或/和选自芳族二醇，芳族羟基羧酸，芳族一元羧酸和芳族多元羧酸的酸源。

10. 发明授权

US5710965A Developer for developing electrostatic images and image forming method 失效
标题翻译：用于显影静电图像和图像形成方法的显影剂
公开(公告)号：US5710965A
公开(公告)日：1998-01-20
申请号：US515327
申请日：1995-08-15
申请人： Keita Nozawa , Tsutomu Kukimoto , Satoshi Matsunaga , Kazuyoshi Hagiwara
发明人： Keita Nozawa , Tsutomu Kukimoto , Satoshi Matsunaga , Kazuyoshi Hagiwara
IPC分类号： G03G9/08 , G03G9/097 , G03G13/09 , G03G13/16 , G03G15/16
CPC分类号： G03G13/09 , G03G13/16 , G03G9/09708 , G03G9/09716
摘要： A developer for developing electrostatic images has a toner and an aggregate of fine particles. The aggregate holds a silicone compound selected from the group consisting of a silicone oil and a silicone varnish, in an amount of from 20% by weight to 90% by weight.
摘要翻译：用于显影静电图像的显影剂具有调色剂和细颗粒的聚集体。聚集体含有选自硅油和有机硅清漆的硅氧烷化合物，其量为20重量％至90重量％。

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